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US3899450A Expired / Lapsed US ⏱️ 0.0 years remaining

Dye penetrant composition containing a volatile degreaser-type solvent

Assignee: Boeing North American Inc
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Filing: 1973-10-03
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Granted: 1975-08-12
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Expires: 1993-10-03
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Abstract

Abstract A liquid dye penetrant composition for detecting cracks and flaws in a specimen surface, consisting essentially of an Nalkyl-2-pyrrolidone, a dye soluble in said pyrrolidone and about 50 to 97 percent by volume of said composition of a volatile halogenated hydrocarbon solvent.

Inventors

  • 👤 Orlando G Molina

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 19:33
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/84; G01N21/88; G01N21/91; Y; Y10; Y10S; Y10S252/00; Y10S252/96

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 119 words
A LIQUID DYE PENETRANT COMPOSITION FOR USE IN NONDESTRUCTIVE TESTING FOR DETECTING CRACKS AND FLAWS IN A SPECIMEN SURFACE, WHICH CONSISTS ESSENTIALLY OF ABOUT 0.2% TO ABOUT 45% BY VOLUME OF AN N-ALKYL-2-PYRROLIDONE, SAID ALKYL GROUP CONTAINING FROM 1 TO 4 CARBON ATOMS, A DYE WHICH IS SOLUBLE IN SAID PYRROLIDONE, THE RATIO OF SAID DYE TO SAID PYRROLIDONE IN SAID COMPOSITION RANGING FROM ABOUT 1 PART OF DYE TO ABOUT 25 PARTS OF PYRROLIDONE, TO ABOUT 2 PARTS OF SAID DYE TO ABOUT 1 PARTS OF PYRROLIDONE, BY VOLUME, AND ABOUT 50 TO ABOUT 97% BY VOLUME OF SAID DYE PENETRANT COMPOSITION, OF A VOLATILE SOLVENT SELECTED FROM THE GROUP CONSISTING OF 1,1,1-TRICHLOROETHANE, TRICHLOROETHYLENE, 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE, TRICHLOROFLUOROMETHANE AND BROMOTRIFLUOROMETHANE.
Claim 2
Dependent Claim 119 words
A LIQUID DYE PENETRANT COMPOSITION FOR USE IN NONDESTRUCTIVE TESTING FOR DETECTING CRACKS AND FLAWS IN A SPECIMEN SURFACE, WHICH CONSISTS ESSENTIALLY OF ABOUT 0.2% TO ABOUT 45% BY VOLUME OF AN N-ALKYL-2-PYRROLIDONE, SAID ALKYL GROUP CONTAINING FROM 1 TO 4 CARBON ATOMS, A DYE WHICH IS SOLUBLE IN SAID PYRROLIDONE, THE RATIO OF SAID DYE TO SAID PYRROLIDONE IN SAID COMPOSITION RANGING FROM ABOUT 1 PART OF DYE TO ABOUT 25 PARTS OF PYRROLIDONE, TO ABOUT 2 PARTS OF SAID DYE TO ABOUT 1 PARTS OF PYRROLIDONE, BY VOLUME, AND ABOUT 50 TO ABOUT 97% BY VOLUME OF SAID DYE PENETRANT COMPOSITION, OF A VOLATILE SOLVENT SELECTED FROM THE GROUP CONSISTING OF 1,1,1-TRICHLOROETHANE, TRICHLOROETHYLENE, 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE, TRICHLOROFLUOROMETHANE AND BROMOTRIFLUOROMETHANE.
Claim 3
Dependent Claim 15 words
A liquid dye penetrant composition as defined in claim 1, wherein said pyrrolidone is N-methyl-2-pyrrolidone.
Claim 4
Dependent Claim 17 words
A liquid dye penEtrant composition as defined in claim 1, wherein said dye is a fluorescent dye.
Claim 5
Dependent Claim 17 words
A liquid dye penetrant composition as defined in claim 2, wherein said dye is a fluorescent dye.
Claim 6
Dependent Claim 14 words
A dye penetrant composition as defined in claim 1, said volatile solvent being 1,1,1-trichloroethane.
Claim 7
Dependent Claim 14 words
A dye penetrant composition as defined in claim 4, said volatile solvent being 1,1,1-trichloroethane.
Claim 8
Dependent Claim 33 words
A dye penetrant composition as defined in claim 1, said dye penetrant composition additionally including a surfactant employed in an amount ranging from about 2 to about 25% by volume of said composition.
Claim 9
Dependent Claim 33 words
A dye penetrant composition as defined in claim 4, said dye penetrant composition additionally including a surfactant employed in an amount ranging from about 2 to about 25% by volume of said composition.
Claim 10
Dependent Claim 22 words
A dye penetrant composition as defined in claim 7, said surfactant being a water soluble or water insoluble surfactant containing ether-oxygen groups.
Claim 11
Dependent Claim 31 words
A dye penetrant composition as defined in claim 9, said surfactant selected from the group consisting of a nonyl phenyl polyethylene glycol ether and a trimethyl nonyl ether of polyethylene glycol.
Claim 12
Dependent Claim 129 words
A liquid dye penetrant composition for use in nondestructive testing for detecting cracks and flaws in a specimen surface, which consists essentially of an N-alkyl-2-pyrrolidone, said alkyl group containing from 1 to 4 carbon atoms, a dye which is soluble in said pyrrolidone, about 50 to about 97% by volume of said dye penetrant composition, of a volatile solvent selected from the group consisting of 1,1,1-trichloroethane, trichloroethylene, 1,1,2-trichloro-1,2,2-trifluoroethane, trichlorofluoromethane and bromotrifluoromethane, and including a surfactant employed in an amount ranging from about 2 to about 25% by volume of said composition, said surfactant being a water soluble or water insoluble surfactant containing ether-oxygen groups, selected from the group consisting of a nonyl phenyl polyethylene glycol ether and a trimethyl nonyl ether of polyethylene glycol, and including isobutyl heptyl ketone.
Claim 13
Dependent Claim 129 words
A liquid dye penetrant composition for use in nondestructive testing for detecting cracks and flaws in a specimen surface, which consists essentially of an N-alkyl-2-pyrrolidone, said alkyl group containing from 1 to 4 carbon atoms, a dye which is soluble in said pyrrolidone, about 50 to about 97% by volume of said dye penetrant composition, of a volatile solvent selected from the group consisting of 1,1,1-trichloroethane, trichloroethylene, 1,1,2-trichloro-1,2,2-trifluoroethane, trichlorofluoromethane and bromotrifluoromethane, and including a surfactant employed in an amount ranging from about 2 to about 25% by volume of said composition, said surfactant being a water soluble or water insoluble surfactant containing ether-oxygen groups, selected from the group consisting of a nonyl phenyl polyethylene glycol ether and a trimethyl nonyl ether of polyethylene glycol, and including isobutyl heptyl ketone.
Claim 14
Dependent Claim 109 words
A liquid dye penetrant composition for use in nondestructive testing for detecting cracks and flaws in a specimen surface, which consists essentially of N-methyl-2-pyrrolidone, a fluorescent dye which is soluble in said pyrrolidone, about 50 to about 97% by volume of said dye penetrant composition, of a volatile solvent selected from the group consisting of 1,1,1-trichloroethane, trichloroethylene, 1,1,2-trichloro-1,2,2-trifluoroethane, trichlorofluoromethane and bromotrifluoromethane, and including a surfactant employed in an amount ranging from about 2 to about 25% by volume of said composition, said surfactant selected from the group consisting of a nonyl phenyl polyethylene glycol ether and a trimethyl nonyl ether of polyethylene glycol, and also including isobutyl heptyl ketone.
Claim 15
Dependent Claim 109 words
A liquid dye penetrant composition for use in nondestructive testing for detecting cracks and flaws in a specimen surface, which consists essentially of N-methyl-2-pyrrolidone, a fluorescent dye which is soluble in said pyrrolidone, about 50 to about 97% by volume of said dye penetrant composition, of a volatile solvent selected from the group consisting of 1,1,1-trichloroethane, trichloroethylene, 1,1,2-trichloro-1,2,2-trifluoroethane, trichlorofluoromethane and bromotrifluoromethane, and including a surfactant employed in an amount ranging from about 2 to about 25% by volume of said composition, said surfactant selected from the group consisting of a nonyl phenyl polyethylene glycol ether and a trimethyl nonyl ether of polyethylene glycol, and also including isobutyl heptyl ketone.

References Cited (Backward Citations)

US3311479A Cited
US3751970A Cited
US3686920A Cited
US3764265A Cited
US3636759A Cited
US3777157A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-08-11 1979-02-10 1979-08-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-08-11 1983-02-10 1983-08-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-08-11 1987-02-10 1987-08-12 $7700.00 Window Closed / Lapsed

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