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US3882210A Expired / Lapsed US ⏱️ 0.0 years remaining

Injection of a ceramic into a mould

Assignee: Rolls Royce PLC
•
Filing: 1972-11-17
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Granted: 1975-05-06
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Expires: 1992-11-17
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Abstract

Abstract A method of producing an injection moulded silicon carbide article comprises charging a chamber with a mix of alpha silicon carbide, graphite and a binder thereof, injecting the mix from the chamber into a mould, removing the mix from the mould, reheating the moulded mix so as to remove the binder and finally heating the finished moulded mix in a vacuum or inert atmosphere in the presence of molten silicon so as to absorb the silicon which reacts with the graphite to form beta silicon carbide and so obtain final densification of the finished moulded article.

Inventors

  • 👤 Ian Alexander Crossley
  • 👤 Geoffrey Eric Kirk
  • 👤 Norman Howell Anthony
  • 👤 Derek Robert Bamber

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 05:36
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/515; C04B35/56; C04B35/565; C04B35/573; B; B28; B28B; B28B1/00; B28B1/24

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 96 words
A METHOD OF PRODUCING AN ARTICLE FROM A MIXTURE OF ALPHA SILICON CARBIDE, GRAPHITE AND A BINDER THEREOF, INCLUDNG THE STEPS OF CHARGING A CHAMBER WITH THE MIX ATTACHING THE CHAMBER TO A MOULD MEMBER, HEATING THE ASSEMBLY, FORCING THE MIX THRUGH A NOZZLE IN THE CHAMBER SO AS TO FIRSTLY COMPACT THE MIX AND SECONDLY INJECT IT INTO SAID MOULD MEMBER, INCREASING SAID FORCE SO AS TO FURTHER COMPACT THE MIX WHILST IN THE MOULD MEMBER, THEN REMOVING SAID FORCE, SEPARATING THE CHAMBER FROM THE MOULD MEMBER AND THEN THE MIX FROM THE MOULD MEMBER.
Claim 2
Independent Claim 96 words
A METHOD OF PRODUCING AN ARTICLE FROM A MIXTURE OF ALPHA SILICON CARBIDE, GRAPHITE AND A BINDER THEREOF, INCLUDNG THE STEPS OF CHARGING A CHAMBER WITH THE MIX ATTACHING THE CHAMBER TO A MOULD MEMBER, HEATING THE ASSEMBLY, FORCING THE MIX THRUGH A NOZZLE IN THE CHAMBER SO AS TO FIRSTLY COMPACT THE MIX AND SECONDLY INJECT IT INTO SAID MOULD MEMBER, INCREASING SAID FORCE SO AS TO FURTHER COMPACT THE MIX WHILST IN THE MOULD MEMBER, THEN REMOVING SAID FORCE, SEPARATING THE CHAMBER FROM THE MOULD MEMBER AND THEN THE MIX FROM THE MOULD MEMBER.
Claim 3
Dependent Claim 26 words
A method of producing an article as claimed in claim 1 wherein said mix is removed from the mould member whilst induced heat is still present.
Claim 4
Dependent Claim 23 words
A method of producing an article as claimed in claim 1 wherein said moulded mix is re-heated so as to remove the binder.
Claim 5
Dependent Claim 59 words
A method of producing an article as claimed in claim 3 wherein said moulded mix is heated for a third time in a vacuum or inert atmosphere in the presence of molten silicon so as to absorb the silicon which reacts with the graphite to form beta silicon carbide and so obtain final densification of the finished moulded article.
Claim 6
Independent Claim 229 words
A method of producing an injection molded article composed of silicon carbide, comprising the steps of: a. mixing together alpha silicon carbide, graphite and a binder therefor to form a mix; b. charging the thus prepared mix under pressure into a chamber to densify the mix, the chamber fitted to a mold part which together constitute a molding assembly; c. heating the entire assembly thereby improving the flow characteristics of the mix contained within the chamber; d. increasing the pressure on the mix within the chamber and forcing the mix through a nozzle in the chamber to (i) further compact the mix, and (ii) inject the mix into the mold part; e. further increasing the pressure on the mix in the mold part to further compact the mix therein; f. discontinuing the applied pressure; g. separating the chamber from the mold piece; h. separating the mold piece while still heated and removing the injector molded mix; i. heating the injection molded mix to remove the binder; j. heating the injection molded mix of step (i) in a vacuum or an inert atmosphere in the presence of molten silicon which reacts exothermically with the graphite to form beta silicon grains; and k. reaction sintering together the alpha silicon carbide and beta silicon carbide to produce an injection molded ceramic article composed of beta silicon carbide, alpha silicon carbide and silicon.
Claim 7
Independent Claim 229 words
A method of producing an injection molded article composed of silicon carbide, comprising the steps of: a. mixing together alpha silicon carbide, graphite and a binder therefor to form a mix; b. charging the thus prepared mix under pressure into a chamber to densify the mix, the chamber fitted to a mold part which together constitute a molding assembly; c. heating the entire assembly thereby improving the flow characteristics of the mix contained within the chamber; d. increasing the pressure on the mix within the chamber and forcing the mix through a nozzle in the chamber to (i) further compact the mix, and (ii) inject the mix into the mold part; e. further increasing the pressure on the mix in the mold part to further compact the mix therein; f. discontinuing the applied pressure; g. separating the chamber from the mold piece; h. separating the mold piece while still heated and removing the injector molded mix; i. heating the injection molded mix to remove the binder; j. heating the injection molded mix of step (i) in a vacuum or an inert atmosphere in the presence of molten silicon which reacts exothermically with the graphite to form beta silicon grains; and k. reaction sintering together the alpha silicon carbide and beta silicon carbide to produce an injection molded ceramic article composed of beta silicon carbide, alpha silicon carbide and silicon.

References Cited (Backward Citations)

US2356081A Cited
US2593507A Cited
US2847712A Cited
US2938807A Cited
US3495939A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-05-05 1978-11-04 1979-05-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-05-05 1982-11-04 1983-05-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-05-05 1986-11-04 1987-05-06 $7700.00 Window Closed / Lapsed

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