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US3882034A Expired / Lapsed US ⏱️ 0.0 years remaining

Simultaneous formation of expanding borax particles and spray dried detergents

Assignee: Colgate Palmolive Co
•
Filing: 1974-02-11
•
Granted: 1975-05-06
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Expires: 1994-02-11
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Abstract

Abstract Hydrated borax, such as Na2E4O7.5H2O, is expanded to a product of low density by passing individual particles downwardly through a relatively slow-moving countercurrent hot air stream in which the particles are heated by convection and by radiation from internal walls of a confining structure. The expanded and dehydrated borax particles resulting are of a bulk density about half or less than that of the density of the original particles. In a preferred embodiment of the invention, a detergent composition less borax is sprayed into the top of a countercurrent spray tower and at a point below the spray inlet, where the produced detergent composition particles are virtually dry, borax pentahydrate is fed into the tower and is dehydrated, expanded and intimately mixed with the other spray dried particles to form a built detergent product containing desired low density borax. Since the densities of the products and particle sizes thereof may be controlled, non-stratifying built detergent can be made, in which the detergent and borax particles are of comparable size and density, or the bulk density of the overall product can be varied by controlling the degree of expansion of the borax.

Inventors

  • 👤 Edward James Gibbons

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 13:16
CPC Classifications
C; C11; C11D; C11D3/00; C11D3/02; C11D3/04; C11D3/046; B; B01; B01D; B01D1/00; B01D1/16; B01D1/18; C11D11/00; C11D11/02

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 184 words
A METHOD FOR PRODUCING A NON-STRATIFYING, BORAXCONTAINING DETERGENT COMPOSITION WHEREIN THE PROPORTION OF BORAX IN THE WHICH COMPRISES PASSING PARTICLES IS FROM 10-50% OF FEED HYDRATED BORAX HAVING A PARTICLE SIZE WITHIN THE RANGE OF 20 TO 200 MESH DOWNWARDLY THROUGH A HOT DRYING GAS MOVING COUNTERCURRENTLY AT A SPEED OF 0.05 TO 5 FT./SEC. IN A DRYING ZONE DEFINED BY AN ENCLOSING WALL, THE TEMPERATURE OF SAID DRYING GAS BEING FROM 120* TO 600*C., THE PRESSURE IN SAID DRYING ZONE RANGING FROM ATMOSPHERIC TO 1 M.M. OF MERCURY VACUUM, THE DWELL TIME OF SAID BORAX PARTICLES IN THE DRYING ZONE BEING FROM 0.1 TO 10 SECONDS SO THAT THE TEMPERATURE OF THE BORAX PARTICLES DOES NOT EXCEED 100*C., WHEREBY TO PRODUCE A PRODUCT BORAX PARTICLES HAVING A MOISTURE CONTENT OF 1 TO 10% AND A BULK DENSITY ABOUT 0.1 TO 0.8 TIMES THE BULK DENSITY OF THE FEED BORAX PARTICLES, CONCURRENTLY SPRAYING INTO SAID DRYING ZONE A DETERGENT SLURRY AT A POINT ABOVE THE POINT OF INTRODUCTION OF THE HYDRATED BORAX PARTICLES BLENDING THE SPRAY DRIED PARTICLES OF DETERGENT COMPOSISITON WITH THE PARTI-
Claim 2
Independent Claim 184 words
A METHOD FOR PRODUCING A NON-STRATIFYING, BORAXCONTAINING DETERGENT COMPOSITION WHEREIN THE PROPORTION OF BORAX IN THE WHICH COMPRISES PASSING PARTICLES IS FROM 10-50% OF FEED HYDRATED BORAX HAVING A PARTICLE SIZE WITHIN THE RANGE OF 20 TO 200 MESH DOWNWARDLY THROUGH A HOT DRYING GAS MOVING COUNTERCURRENTLY AT A SPEED OF 0.05 TO 5 FT./SEC. IN A DRYING ZONE DEFINED BY AN ENCLOSING WALL, THE TEMPERATURE OF SAID DRYING GAS BEING FROM 120* TO 600*C., THE PRESSURE IN SAID DRYING ZONE RANGING FROM ATMOSPHERIC TO 1 M.M. OF MERCURY VACUUM, THE DWELL TIME OF SAID BORAX PARTICLES IN THE DRYING ZONE BEING FROM 0.1 TO 10 SECONDS SO THAT THE TEMPERATURE OF THE BORAX PARTICLES DOES NOT EXCEED 100*C., WHEREBY TO PRODUCE A PRODUCT BORAX PARTICLES HAVING A MOISTURE CONTENT OF 1 TO 10% AND A BULK DENSITY ABOUT 0.1 TO 0.8 TIMES THE BULK DENSITY OF THE FEED BORAX PARTICLES, CONCURRENTLY SPRAYING INTO SAID DRYING ZONE A DETERGENT SLURRY AT A POINT ABOVE THE POINT OF INTRODUCTION OF THE HYDRATED BORAX PARTICLES BLENDING THE SPRAY DRIED PARTICLES OF DETERGENT COMPOSISITON WITH THE PARTI-
Claim 3
Dependent Claim 41 words
A method according to claim 1 wherein the removed detergent-borax composition is tested for density and the ratio of borax hydrate to detergent mixute charged to the drying zone is changed to control the density of the detergent-borax composition being made.
Claim 4
Dependent Claim 50 words
A method according to claim 1 wherein the removed detergent-borax composition is tested for density and the point or points of introduction of the borax hydrate into the drying zone are changed to control the density of the borax particles produced and thereby control the density of the detergent-borax composition.
Claim 5
Dependent Claim 56 words
A method according to claim 2 wherein the means for testing density is a weigh belt and the deflection of the belt actuates means for adding borax hydrate particles to the dehydrating zone when the density is higher than desired and diminishes the feed rate of the borax hydrate when the density is lower than desired.
Claim 6
Dependent Claim 59 words
A method according to claim 3 wherin the means for testing density is a weigh belt and the deflection of the belt actuates means for adding borax particles to the dehydrating zone at a relatively high level when the density is too high and of adding such particles at a relatively low level when the density is too low.
Claim 7
Dependent Claim 28 words
A method to claim 1 wherein a detergent composition constituent that is not stable to spray drying conditions is added to the decrepitation zone with the borax hydrate.
Claim 8
Dependent Claim 13 words
A method according to claim 6 wherein the unstable constituent is sodium perborate.

References Cited (Backward Citations)

US3454357A Cited
US3533942A Cited
US3600319A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-05-05 1978-11-04 1979-05-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-05-05 1982-11-04 1983-05-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-05-05 1986-11-04 1987-05-06 $7700.00 Window Closed / Lapsed

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