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US3882014A Expired / Lapsed US ⏱️ 0.0 years remaining

Reaction zone effluents separation and hydrogen enrichment process

Assignee: Universal Oil Products Co
•
Filing: 1974-06-24
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Granted: 1975-05-06
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Expires: 1994-06-24
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Abstract

Abstract A method for the separation of a hydrogen-containing hydrocarbonaceous reaction zone effluent accompanied by hydrogen enrichment of a recycled gaseous phase. The method involves the technique of cooling and partially condensing the effluent material emanating from a hydrocarbon reaction zone with introduction thereof into a vapor-liquid separation zone. A first vaporous phase is compressed and introduced upwardly into a contacting-condensation zone wherein the vapors countercurrently contact a descending stream of cooled fractionation zone liquid bottoms material. Partial condensation and selective absorption of the upwardly flowing vapors is effected with hydrogen enrichment of the vaporous phase withdrawn from the upper portion of the contacting-condensation zone. The liquid phases from the vapor-liquid separation zone and the contacting-condensation zone are admixed and introduced, at elevated pressure into a fractionation zone. A portion of the liquid bottoms material recovered from the fractionation zone is cooled and introduced into the contacting-condensation zone to contact countercurrently the upwardly flowing vapor phase therein.

Inventors

  • 👤 Richard D Monday
  • 👤 Norman H Scott

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 18:07
CPC Classifications
C; C10; C10G; C10G45/00; C10G35/00; C10G35/04; C10G45/02; C10G45/72; C10G49/00; C10G49/22; C10G49/24; C10G49/26

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 288 words
IN A LHYDROCARBON CONVERSION PROCESS WHEREIN (1) A HYCROCARBON CHANGE STOCK AND HYDROGEN ARE CONTACTED IN A CATALYTIC REACTION ZONE, (2) A HYDROGEN-CONTAINING HYDROCARBON EFFLUENT STREAM IS WITHDRAWN FROM SAID ZONE, (3) SAID EFFLUENT IS SEPARATED TO PROVIDE A PRINCIPALLY LIQUID PHASE AND A PRINCIPALLY VAPOROUS PHASE, AND (4) AT LEAST A PORTION OF SAID VAPOROUS PHASE IS RECYCLED TO SAID REACTION ZONE, THE IMPROVEMENT COMPRISING SEPARATEING SAID EFFLUENT AND INCREASING THE HYDROFEN CONCENTRATION OF SAID RECYCLED VAPOROUS PHASE BY THE STEPS OF: A. PARTICALLY CONDENSING SAID HYDROCARBON REACTION ZONE EFFLUENT AT A TEMPERATURE FROM ABOUT 150*F TO ABOUT 300*F AND INTRODUCING THE SAME INTO A VAPOR-LIQUID SEPARATION ZONE, THEREIN EFFECTING SEPARATION INTO A FIRST HYDROGEN-CONTAINING VAPOUOUS PHASE AND A FIRST LIQUID PHASE; B. INTRODUCING SAID FIRST VAPOROUS PHASE UPWARDLY INTO A CONTACTING-CONDENSING ZONE AND THEREIN COUNTERCURRENTLY CONTACTING THE SAME WITH A DOWNWARDLY FLOWING, COOLED FRACTIONATION BOTTOMS MATERIAL, AT CONTACTING CONDITIONS SELECTED TO EFFECT CONDENSATION AND SELECTIVE ABSORPTION OF A PORTION OF SAID FIRST VAPOROUS PHASE; C. RECOVERING, FROM SAID CONTACTING-CONDENSING ZONE, A SECOND VAPOROUS PHASE ENRICHED IN HYDROGEN AND A SECOND LIQUID PHASE OF SAID LIQUID BOTTOMS MATERIALS AND THE CONDENSED-ABSORBED PORTION OF SAID FIRST VAPOROUS PHASE; D. RECYCLING AT LEAST A PORTION OF SAID SECOND VARPOROUS PHASE TO COMBINE WITH SAID HYDROCARBON CHARGE STOCK; E. FRACTIONATING A MIXTURE OF SAID FIRST AND SECOND LIQUID PHASES, IN A FRACTIONATION ZONE, AT CONDITIONS SELECTED TO VAPORIZE LIGHT COMPONENTS THEREFROM, AND RECOVERING THE SAME AS A THIRD VAPOROUS PHASE; F. RECOVERING A LIQUID BOTTOMS MATERIAL FROM SAID FRACTIONATION ZONE; AND, G. COOLING SAID LIQUID BOTTOMS MATERIAL AND PASSING AT LEAST A PORTION OF THE COOLED MATERIAL DOWNWARDYL INTO SAID CONTACTING-CONDENSING ZONE TO COUNTERCURRENTLY CONTACT SAID FIRST VAPOROUS PHASE THEREIN.
Claim 2
Dependent Claim 288 words
IN A LHYDROCARBON CONVERSION PROCESS WHEREIN (1) A HYCROCARBON CHANGE STOCK AND HYDROGEN ARE CONTACTED IN A CATALYTIC REACTION ZONE, (2) A HYDROGEN-CONTAINING HYDROCARBON EFFLUENT STREAM IS WITHDRAWN FROM SAID ZONE, (3) SAID EFFLUENT IS SEPARATED TO PROVIDE A PRINCIPALLY LIQUID PHASE AND A PRINCIPALLY VAPOROUS PHASE, AND (4) AT LEAST A PORTION OF SAID VAPOROUS PHASE IS RECYCLED TO SAID REACTION ZONE, THE IMPROVEMENT COMPRISING SEPARATEING SAID EFFLUENT AND INCREASING THE HYDROFEN CONCENTRATION OF SAID RECYCLED VAPOROUS PHASE BY THE STEPS OF: A. PARTICALLY CONDENSING SAID HYDROCARBON REACTION ZONE EFFLUENT AT A TEMPERATURE FROM ABOUT 150*F TO ABOUT 300*F AND INTRODUCING THE SAME INTO A VAPOR-LIQUID SEPARATION ZONE, THEREIN EFFECTING SEPARATION INTO A FIRST HYDROGEN-CONTAINING VAPOUOUS PHASE AND A FIRST LIQUID PHASE; B. INTRODUCING SAID FIRST VAPOROUS PHASE UPWARDLY INTO A CONTACTING-CONDENSING ZONE AND THEREIN COUNTERCURRENTLY CONTACTING THE SAME WITH A DOWNWARDLY FLOWING, COOLED FRACTIONATION BOTTOMS MATERIAL, AT CONTACTING CONDITIONS SELECTED TO EFFECT CONDENSATION AND SELECTIVE ABSORPTION OF A PORTION OF SAID FIRST VAPOROUS PHASE; C. RECOVERING, FROM SAID CONTACTING-CONDENSING ZONE, A SECOND VAPOROUS PHASE ENRICHED IN HYDROGEN AND A SECOND LIQUID PHASE OF SAID LIQUID BOTTOMS MATERIALS AND THE CONDENSED-ABSORBED PORTION OF SAID FIRST VAPOROUS PHASE; D. RECYCLING AT LEAST A PORTION OF SAID SECOND VARPOROUS PHASE TO COMBINE WITH SAID HYDROCARBON CHARGE STOCK; E. FRACTIONATING A MIXTURE OF SAID FIRST AND SECOND LIQUID PHASES, IN A FRACTIONATION ZONE, AT CONDITIONS SELECTED TO VAPORIZE LIGHT COMPONENTS THEREFROM, AND RECOVERING THE SAME AS A THIRD VAPOROUS PHASE; F. RECOVERING A LIQUID BOTTOMS MATERIAL FROM SAID FRACTIONATION ZONE; AND, G. COOLING SAID LIQUID BOTTOMS MATERIAL AND PASSING AT LEAST A PORTION OF THE COOLED MATERIAL DOWNWARDYL INTO SAID CONTACTING-CONDENSING ZONE TO COUNTERCURRENTLY CONTACT SAID FIRST VAPOROUS PHASE THEREIN.
Claim 3
Dependent Claim 24 words
The method of claim 1 further characterized in that said first vaporous phase is compressed prior to the introduction thereof into said contacting-condensing zone.
Claim 4
Dependent Claim 26 words
The method of claim 1 further characterized in that said first liquid phase is increased in pressure prior to the introduction thereof into said fractionation zone.
Claim 5
Dependent Claim 26 words
THe method of claim 1 further characterized in that said second liquid phase is increased in pressure prior to the introduction thereof into said fractionation zone.
Claim 6
Dependent Claim 22 words
The method of claim 1 further characterized in that said liquid bottoms material is cooled via indirect heat-exchange with said charge stock.
Claim 7
Dependent Claim 24 words
The method of claim 1 further characterized in that said hydrocarbon effluent is cooled prior to the introduction thereof into said vapor-liquid separation zone.
Claim 8
Dependent Claim 27 words
The method of claim 1 further characterized in that said hydrocarbon effluent is a catalytically reformed naphtha fraction containing hydrogen, normally vaporous hydrocarbons and normally liquid hydrocarbons.

References Cited (Backward Citations)

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US3000812A Cited
US3296118A Cited
US3131235A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-05-05 1978-11-04 1979-05-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-05-05 1982-11-04 1983-05-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-05-05 1986-11-04 1987-05-06 $7700.00 Window Closed / Lapsed

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