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US3879475A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for the preparation of biodegradable glycidol surfactants

Assignee: Olin Corp
•
Filing: 1973-01-10
•
Granted: 1975-04-22
•
Expires: 1993-01-10
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Abstract

Abstract This invention relates to a novel method of preparing biodegradable glycidol surfactants by reacting selected aliphatic alcohols with glycidol in the presence of a polar, non-reactive, miscible solvent and to the surfactants produced by such method.

Inventors

  • 👤 John A Wojtowicz
  • 👤 Milton Lapkin

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 08:27
CPC Classifications
C; C11; C11D; C11D1/00; C11D1/66; C11D1/72; Y; Y10; Y10S; Y10S516/00; Y10S516/01; Y10S516/02; Y10S516/905; Y10S516/917

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 14 words
THE METHOD FOR PREPARING SURFACTANTS COMPRISING REACTING: A. AN ALIPHATIC ALCOHOL HAVING THE FORMULA:
Claim 2
Independent Claim 14 words
THE METHOD FOR PREPARING SURFACTANTS COMPRISING REACTING: A. AN ALIPHATIC ALCOHOL HAVING THE FORMULA:
Claim 3
Dependent Claim 29 words
The method of claim 1 wherein said Lewis acid is selected from the group consisting of BF3, BFetherate, SnCl4, TiCl4, SbCl5, HF, AlCl3, Al(C2H5)3, AlBr3, FeCl3, ZnCl2 and ZnBr2.
Claim 4
Dependent Claim 12 words
The method of claim 2 wherein said Lewis acid is BF3 etherate.
Claim 5
Dependent Claim 21 words
The method of claim 3 wherein said reaction is carried out at a temperature of from about 40* to about 75*C.
Claim 6
Dependent Claim 25 words
The method of claim 4 wherein R contains 10 to 18 carbons and the molar ratio of glycidol to alcohol is from 6:1 to 12:1.
Claim 7
Dependent Claim 12 words
The method of claim 5 wherein said Lewis acid is BF3 etherate.

References Cited (Backward Citations)

US2723294A Cited
US2089569A Cited
US2131142A Cited
US2236919A Cited
US2380185A Cited
US2782240A Cited
US2807651A Cited
US3042666A Cited
US3445525A Cited
US3317508A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-04-21 1978-10-21 1979-04-22 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-04-21 1982-10-21 1983-04-22 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-04-21 1986-10-21 1987-04-22 $7700.00 Window Closed / Lapsed

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