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US3872032A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the preparation of graphite fluoride

Assignee: Nippon Carbon Co Ltd
•
Filing: 1973-02-08
•
Granted: 1975-03-18
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Expires: 1993-02-08
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Abstract

Abstract A process for the preparation of a white-colored graphite fluoride by reacting carbon with a fluorine material containing not more than 5% by volume of hydrogen fluoride.

Inventors

  • 👤 Toyonosuke Kanemaru
  • 👤 Toshio Shimada
  • 👤 Isao Inudow

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 20:01
CPC Classifications
C; C01; C01B; C01B32/00; C01B32/10

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 76 words
A PROCESS FOR THE PRREPARATION OF A WHITE-COLORED, INORGANIC, HIGH MOLECULAR WEIGHT GRAPHITE FLUORIDE HAVING A CARBON-TO-FLUORINE ATOMIC RATIO OF 1:1, COMPRISING REACTING A NON-CRYSTALLINE CARBON SELECTED FROM THE GROUP CONSISTING OF COKE, CARBON BLACK, CHARCOAL AND CARBONIZED SUGAR WITH A FLUORINE MATERIAL CONSISTING ESSENTIALLY OF FLUORINE AND HYDROGEN FLUORIDE, SAID HYDROGEN FLUORIDE BEING PRESENT IN AN AMOUNT NOT MORE THAN 5% BY VOLUME, OF SAID FLUORINE, FOR A SUFFICIENT TIME TO OBTAIN THE GRAPHITE FLUORIDE.
Claim 2
Dependent Claim 76 words
A PROCESS FOR THE PRREPARATION OF A WHITE-COLORED, INORGANIC, HIGH MOLECULAR WEIGHT GRAPHITE FLUORIDE HAVING A CARBON-TO-FLUORINE ATOMIC RATIO OF 1:1, COMPRISING REACTING A NON-CRYSTALLINE CARBON SELECTED FROM THE GROUP CONSISTING OF COKE, CARBON BLACK, CHARCOAL AND CARBONIZED SUGAR WITH A FLUORINE MATERIAL CONSISTING ESSENTIALLY OF FLUORINE AND HYDROGEN FLUORIDE, SAID HYDROGEN FLUORIDE BEING PRESENT IN AN AMOUNT NOT MORE THAN 5% BY VOLUME, OF SAID FLUORINE, FOR A SUFFICIENT TIME TO OBTAIN THE GRAPHITE FLUORIDE.
Claim 3
Dependent Claim 13 words
A process according to claim 1, wherein the hydrogen fluoride content is 1-3%.
Claim 4
Dependent Claim 16 words
A process according to claim 1, wherein the reaction is effected at a temperature between 300*-450*C.
Claim 5
Dependent Claim 14 words
A process according to claim 1, wherein the reaction time is 1/2 -10 hours.
Claim 6
Dependent Claim 16 words
A process according to claim 1, wherein the reaction is effected at a temperature between 350*-400*C.
Claim 7
Dependent Claim 13 words
A process according to claim 6, wherein the reaction time is 5-7 hours.

References Cited (Backward Citations)

US3397087A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-03-17 1978-09-16 1979-03-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-03-17 1982-09-16 1983-03-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-03-17 1986-09-16 1987-03-18 $7700.00 Window Closed / Lapsed

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