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US3868376A Expired / Lapsed US ⏱️ 0.0 years remaining

Bis N,N piperazine phosphoramides and their preparation

Assignee: Chevron USA Inc
•
Filing: 1972-08-25
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Granted: 1975-02-25
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Expires: 1992-08-25
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Abstract

Abstract WHEREIN: X is the same or different element selected from nitrogen or oxygen; Y is the same or different element selected from oxygen, sulfur or nitrogen and nitrogen when both X''s are oxygen; R is a hydrocarbylene or dihydrocarbylene having from 2 to 18 carbon atoms; R1 is the same of different hydrogen or a hydrocarbyl having from 1 to 24 carbons; R2 is the same or different R1 or a hydrocarbylene having from 2 to 18 carbon atoms with one end of each R2 bonding to the other R2 or to said R dihydrocarbylene; N IS 1 WHEN Y is oxygen or sulfur and 2 when Y is nitrogen; and M IS N-1. Novel bisphosphoramides are prepared by reacting phosphorus oxychloride with a difunctional compound and a monofunctional compound within a liquid phase reaction medium to produce compounds having the structure:

Inventors

  • 👤 Bruce W Hotten

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 18:14
CPC Classifications
C; C10; C10M; C10M1/00; C10M1/08; C07; C07F; C07F9/00; C07F9/02; C07F9/06; C07F9/08; C07F9/09; C07F9/093; C07F9/16; C07F9/165; C07F9/1652; C07F9/22; C07F9/224; C07F9/24; C07F9/547; C07F9/645; C07F9/6509; C07F9/650952; C10M2201/00; C10M2201/08; C10M2201/082; C10M2201/083; C10M2203/00; C10M2203/06; C10M2205/00; C10M2205/02; C10M2205/024; C10M2205/026; C10M2207/00; C10M2207/02; C10M2207/023; C10M2207/024; C10M2207/027; C10M2207/04; C10M2207/10; C10M2207/12; C10M2207/121; C10M2207/123; C10M2207/125; C10M2207/129; C10M2207/22; C10M2207/28; C10M2207/281; C10M2207/282; C10M2207/283; C10M2207/286; C10M2207/34; C10M2209/00; C10M2209/10; C10M2209/103; C10M2209/105; C10M2209/108; C10M2215/00; C10M2215/02; C10M2215/04; C10M2215/06; C10M2215/062; C10M2215/064; C10M2215/065; C10M2215/066; C10M2215/08; C10M2215/082; C10M2215/10; C10M2215/102; C10M2215/22; C10M2215/223; C10M2215/224; C10M2215/24; C10M2215/26; C10M2215/28; C10M2217/00; C10M2217/02; C10M2217/028; C10M2217/04; C10M2217/042; C10M2217/043; C10M2217/06; C10M2219/00; C10M2219/02; C10M2219/022; C10M2219/04; C10M2219/044; C10M2219/08; C10M2219/082; C10M2219/085; C10M2219/10; C10M2219/104; C10M2219/108; C10M2223/00; C10M2223/02; C10M2223/04; C10M2223/041; C10M2223/042; C10M2223/043; C10M2223/045; C10M2223/047; C10M2223/049; C10M2227/00; C10M2227/02; C10M2229/00; C10M2229/04; C10M2229/041; C10M2229/043; C10M2229/044; C10N; C10N2010/00; C10N2010/02; C10N2010/04; C10N2010/06; C10N2040/00; C10N2040/02; C10N2040/08; C10N2040/10; C10N2040/12; C10N2040/13; C10N2040/135; C10N2040/20; C10N2040/22; C10N2040/25; C10N2040/252; C10N2040/253; C10N2040/255; C10N2040/26; C10N2050/00; C10N2050/04; C10N2050/10; F; F02; F02B; F02B1/00; F02B1/02; F02B1/04

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 5 words
A COMPOUND HAVING THE FORMULA:
Claim 2
Dependent Claim 5 words
A COMPOUND HAVING THE FORMULA:
Claim 3
Dependent Claim 18 words
A compound defined in claim 1 wherein said R3 is an analkyl having from 16 to 20 carbons.
Claim 4
Dependent Claim 18 words
A compound defined in claim 1 wherein said R4 is an alkyl having from 12 to 18 carbons.
Claim 5
Dependent Claim 21 words
A compound as defined in claim 1 wherein said R3 and R4 are derived from a C10-C30 secondary vegetable oil amine.
Claim 6
Dependent Claim 20 words
The compound defined in claim 1 wherein said R3 and R4 is a fatty acid group obtained from coconut oil.
Claim 7
Independent Claim 45 words
A method for preparing a bisphosphoramide which comprises contacting (1) phosphorous oxychloride, (2) a secondary diamine, and (3) a C1 to C24 primary or secondary monoamine at a temperature from 20* to 150*C and at a pressure sufficient to maintain a liquid phase reaction medium.
Claim 8
Independent Claim 45 words
A method for preparing a bisphosphoramide which comprises contacting (1) phosphorous oxychloride, (2) a secondary diamine, and (3) a C1 to C24 primary or secondary monoamine at a temperature from 20* to 150*C and at a pressure sufficient to maintain a liquid phase reaction medium.

References Cited (Backward Citations)

US2574516A Cited
US2574518A Cited
US3524908A Cited
US3476685A Cited
US3674804A Cited
US3668237A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-02-24 1978-08-26 1979-02-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-02-24 1982-08-26 1983-02-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-02-24 1986-08-26 1987-02-25 $7700.00 Window Closed / Lapsed

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