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US3867128A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing high specific gravity material from low grade iron ore

Assignee: Individual
•
Filing: 1972-12-18
•
Granted: 1975-02-18
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Expires: 1992-12-18
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Abstract

Abstract A process is disclosed whereby low grade iron ores having a minimum specific gravity of about 3.45 are converted to iron oxide containing material having a specific gravity of 4.2 or greater. The process includes calcining under oxidizing conditions of washed and crushed iron ore of low specific gravity followed by a quench and separation step whereby the high specific gravity iron oxide-containing material is recovered from lower specific gravity contaminants. The material thus prepared can be ground to a size suitable for use as a weighting agent in drilling muds meeting the API specifications for such materials.

Inventors

  • 👤 Jr James Thomas Hancock

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 13:42
CPC Classifications
B; B03; B03B; B03B7/00; B03B1/00; B03B1/02

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 95 words
A PROCESS FOR PREPARING A NON-MAGNETIC IRON OXIDECONTAINING MATERIAL HAVING A SPECIFIC GRAVITY OF A LEAST 4.2 FROM AN IRON ORE HAVING A SPECIFIC GRAVITY OF ABOUT 3.6 TO ABOUT 3.9 WHICH COMPRISES THE STEPS OF: A. CALCINING SAID IRON ORE UNDER OXIDIZING CONDITIONS AT A RESIDENCE TIME SUFFICIENT TO MAINTAIN THE ORE AT BETWEEN ABOUT 1700*F. TO LESS THAN ABOUT 2050*F. FOR AT LEAST 20 MINUTES; B. QUENCHING THE CALCINED ORE; AND C. RECOVERING THE QUENCHED IRON OXIDE-CONTAINING MATERIALS; WHEREIN, THE RECOVERED MATERIAL IS NON-MAGNETIC AND HAS A SPECIFIC GRAVITY OF AT LEAST 4.2.
Claim 2
Dependent Claim 95 words
A PROCESS FOR PREPARING A NON-MAGNETIC IRON OXIDECONTAINING MATERIAL HAVING A SPECIFIC GRAVITY OF A LEAST 4.2 FROM AN IRON ORE HAVING A SPECIFIC GRAVITY OF ABOUT 3.6 TO ABOUT 3.9 WHICH COMPRISES THE STEPS OF: A. CALCINING SAID IRON ORE UNDER OXIDIZING CONDITIONS AT A RESIDENCE TIME SUFFICIENT TO MAINTAIN THE ORE AT BETWEEN ABOUT 1700*F. TO LESS THAN ABOUT 2050*F. FOR AT LEAST 20 MINUTES; B. QUENCHING THE CALCINED ORE; AND C. RECOVERING THE QUENCHED IRON OXIDE-CONTAINING MATERIALS; WHEREIN, THE RECOVERED MATERIAL IS NON-MAGNETIC AND HAS A SPECIFIC GRAVITY OF AT LEAST 4.2.
Claim 3
Dependent Claim 28 words
The process of claim 1 wherein the iron ore has a particle size which will pass through a 1/2 -inch screen and remain on a 1/8 -inch screen.
Claim 4
Dependent Claim 27 words
The process of claim 2 wherein the ore has a particle size which will pass through a 3/8 -inch screen and remain on a 1/8 -inch screen.
Claim 5
Dependent Claim 36 words
The process of claim 1 wherein the calcining step is carried out in a rotary kiln equipped with at least one gas burner with its flame directed so as not to impinge upon the raw ore.
Claim 6
Dependent Claim 21 words
The process of claim 4 wherein said kiln is equipped to provide a forced draft of air during the calcining step.
Claim 7
Dependent Claim 113 words
A process for preparing a non-magnetic iron oxide having a specific gravity of at least 4.2 from a raw iron ore having a specific gravity of less than 3.9 which comprises the steps of: a. crushing the raw ore to a particle size not greater than 1 1/2 inches; b. washing the crushed raw ore; c. calcining said washed ore under oxidizing conditions at residence time sufficient to maintain the ore at between about 1700*F. and less than about 2050*F. for at least 20 minutes; d. quenching the calcined ore; and e. recovering the quenched iron oxide-containing material whereby the recovered material is non-magnetic and has a specific gravity of at least 4.2.
Claim 8
Dependent Claim 113 words
A process for preparing a non-magnetic iron oxide having a specific gravity of at least 4.2 from a raw iron ore having a specific gravity of less than 3.9 which comprises the steps of: a. crushing the raw ore to a particle size not greater than 1 1/2 inches; b. washing the crushed raw ore; c. calcining said washed ore under oxidizing conditions at residence time sufficient to maintain the ore at between about 1700*F. and less than about 2050*F. for at least 20 minutes; d. quenching the calcined ore; and e. recovering the quenched iron oxide-containing material whereby the recovered material is non-magnetic and has a specific gravity of at least 4.2.
Claim 9
Dependent Claim 20 words
The process of claim 6 wherein the washed ore is calcined at from about 1800* F. to about 2000* F.
Claim 10
Dependent Claim 22 words
The process of claim 7 wherein the washed ore is calcined for a time period of from 30 to about 45 minutes.
Claim 11
Dependent Claim 180 words
A process for preparing a non-magnetic iron oxide material having a specific gravity of at least 4.2 from a raw iron ore having a specific gravity of at least 3.45 which comprises the steps of: a. crushing the raw ore to a particle size which will pass through a 3/8 -inch screen and be retained on a 1/8 -inch screen; b. washing the crushed raw ore; c. calcining the washed ore at a temperature of about 1800*F. to about 2000*F. for from about 30 to about 45 minutes in a rotary kiln equipped with a means producing an air draft and with at least one internal burner directed to avoid impingement of the flame on the iron ore during the calcining step; d. quenching the calcined material with water; e. recovering the quenched material from low specific gravity materials by a means whereby the iron oxide-containing material is separated from said low specific gravity material; and f. grinding the recovered iron oxides to a particle size such that 97 percent of the material will pass through a 200 mesh screen.
Claim 12
Dependent Claim 180 words
A process for preparing a non-magnetic iron oxide material having a specific gravity of at least 4.2 from a raw iron ore having a specific gravity of at least 3.45 which comprises the steps of: a. crushing the raw ore to a particle size which will pass through a 3/8 -inch screen and be retained on a 1/8 -inch screen; b. washing the crushed raw ore; c. calcining the washed ore at a temperature of about 1800*F. to about 2000*F. for from about 30 to about 45 minutes in a rotary kiln equipped with a means producing an air draft and with at least one internal burner directed to avoid impingement of the flame on the iron ore during the calcining step; d. quenching the calcined material with water; e. recovering the quenched material from low specific gravity materials by a means whereby the iron oxide-containing material is separated from said low specific gravity material; and f. grinding the recovered iron oxides to a particle size such that 97 percent of the material will pass through a 200 mesh screen.
Claim 13
Dependent Claim 20 words
The process of claim 9 wherein the calcining step is performed at from about 1850* F. to about 1950* F.
Claim 14
Dependent Claim 13 words
The process of claim 9 wherein the raw ore is a limonite ore.
Claim 15
Dependent Claim 13 words
The process of claim 9 wherein the raw ore is a goethite ore.

References Cited (Backward Citations)

US2119270A Cited
US2298984A Cited
US2551874A Cited
US2686593A Cited
US3238037A Cited
US3281235A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-02-17 1978-08-19 1979-02-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-02-17 1982-08-19 1983-02-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-02-17 1986-08-19 1987-02-18 $7700.00 Window Closed / Lapsed

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