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US3862829A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of processing ferroelectric devitrifiable glass ceramics

Assignee: United States Department of the Army
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Filing: 1973-08-14
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Granted: 1975-01-28
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Expires: 1993-08-14
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Abstract

Abstract The electrical properties of ferroelectric devitrifiable glass ceramics are improved by subjecting the ceramics to inert gas pressures of about 5,000 pounds per square inch to about 50,000 pounds per square inch at temperatures from about 700* C. to about 1,100* C. for about 15 minutes to about 2 hours.

Inventors

  • 👤 Ronald J Brandmayr
  • 👤 Sam Divita

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 20:40
CPC Classifications
C; C03; C03C; C03C10/00; C03C10/0072

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 104 words
Method according to claim 1 wherein the ferroelectric devitrifiable glass ceramic is barium strontium niobate devitrifiable glass ceramic, the temperature is about 775*C., and the inert gas pressure is about 10,000 to about 30,000 pounds per square inch of helium; the devitrified body so obtained being characterized by a dielectric constant of 380, a dielectric strength of up to 3,000 volts per mil, a dissipation factor below 0.25 percent, and a more stable coefficient of dielectric constant under DC stress that is improved from a 20 percent change at 500 volts per mil to only a 14 percent cHange at 500 volts per mil.
Claim 2
Dependent Claim 41 words
Method according to claim 1 wherein the ferroelectric devitrifiable glass ceramic is barium strontium titanate devitrifiable glass ceramic, the temperature is about 900* C., and the inert gas pressure is about 10,000 to about 30,000 pounds per square inch of argon.
Claim 3
Dependent Claim 41 words
Method according to claim 1 wherein the ferroelectric devitrifiable glass ceramic is lead zirconate-lead titanate devitrifiable glass ceramic, the temperature is about 750* C., and the inert gas pressure is about 10,000 to about 30,000 pounds per square inch of argon.
Claim 4
Dependent Claim 33 words
Method according to claim 1 in which the ferroelectric devitrifiable glass ceramic is encapsulated in a stainless steel container back filled with oxygen prior to subjecting the ceramic to the inert gas pressures.

References Cited (Backward Citations)

US3116137A Cited
US3459503A Cited
US3490887A Cited
US3503717A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-01-27 1978-07-29 1979-01-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-01-27 1982-07-29 1983-01-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-01-27 1986-07-29 1987-01-28 $7700.00 Window Closed / Lapsed

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