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US3862047A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and composition for detecting flaws in metallic surfaces, holes and otherwise

Assignee: General Dynamics Corp
•
Filing: 1972-04-26
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Granted: 1975-01-21
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Expires: 1992-04-26
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Abstract

Abstract A procedure for examining and inspecting drilled holes or other metal surface conformations by applying a castable, two component, magnetically active material comprised of room temperature vulcanizing rubber or a polymerizing material containing magnetizable particles and specific sensitizing agents, magnetizing the area to be inspected, and curing the castable material to form a permanent replica impression of the inspection area which, when removed, reveals the presence of surface flaws, such as cracks, scratches, tool marks or dimensional inaccuracies and subsurface flaws which may tend to develop in structurally deficient members.

Inventors

  • 👤 Henry J Weltman
  • 👤 Mark T Carroll
  • 👤 John E Halkias
  • 👤 William T Kaarlela
  • 👤 Jack D Reynolds

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 03:31
CPC Classifications
G; G01; G01N; G01N27/00; G01N27/72; G01N27/82; G01N27/83; G01N27/84; G01N15/00; G01N15/06; G01N15/0656

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 234 words
A COMPOSITION FORMING A ROOM TEMPERATURE VULCANIZABLE CASTING MATERIAL FOR PRECISE VISUAL INSPECTION OF MAGNETICALLY INDUCTIVE SUBSTANCES BY APPLICATION OF THE MATERIAL DIRECTLY TO A WORKPIECE TO BE INSPECTED, SOLIDIFYING IN SITU TO ELASTIC FLEXIBLE FORM AND REMOVING THE CASTING, FOR DETERMINING AND PERMANENTLY RECORDING THE PRESENCE OF A FLAW OR FLAWS IN THE WORKPIECE BY MIGRATION OF MAGNETIZABLE PARTICLES IN THE COMPOSITION TO THE FLAWED AREA WHEN THE WORKPIECE AND CASTING MATERIAL ARE SUBJECTED TO MAGNETIC FLUX COMPRISING: A BASE FORMULATON HAVING A. ABOUT 100 PARTS BY WEIGHT SILICONE RUBBER COMPOUND, VULCANIZABLE AT ROOM TEMPERATURE BY ADDITION OF SUITABLE CATALYST MATERIAL THERETO, AND COMPRISING A SUBSTANTIALLY LINEAR POLYDIMETHYL SILOXANE B. ABOUT 0.1 TO 10.0 PARTS BY WEIGHT OF FERROMAGNETIC PARTICLES IN THE SIZE RANGE OF FROM ABOUT 5 TO 60 MICRONS; C. A LIQUID NAPHTHA HYDROCARBON DILUENT IN AN AMOUNT SUFFICIENT TO ADJUST VISCOSITY OF THE FORMULATION TO WITHIN A RANGE OF ABOUT 1 TO ABOUT 120 POISES; AND ABOUT ABOUT 0.2 TO ABOUT 6 PARTS BY WEIGHT PER 100 PARTS OF SAID BASE FORMULATION OF A CATALYST COMPRISING A METALLIC SOAP FOR VULCANIZING SAID SILICONE RUBBER COMPOUND TO SAID FLEXIBLE ELASTIC FORM; SAID RUBBER DIFFERING IN COLOR FROM SAID FERROMAGNETIC PARTICLES TO PROVIDE VISUAL CONTRAST BETWEEN SAID COMPOSITION AS A WHOLE AND AN ACCUMULATION THEREIN OF SAID PARTICLES AT THE AREA OF A DETECTED FLAW WHEN SAID COMPOSITION IS CURED OR VULCANIZED.
Claim 2
Dependent Claim 234 words
A COMPOSITION FORMING A ROOM TEMPERATURE VULCANIZABLE CASTING MATERIAL FOR PRECISE VISUAL INSPECTION OF MAGNETICALLY INDUCTIVE SUBSTANCES BY APPLICATION OF THE MATERIAL DIRECTLY TO A WORKPIECE TO BE INSPECTED, SOLIDIFYING IN SITU TO ELASTIC FLEXIBLE FORM AND REMOVING THE CASTING, FOR DETERMINING AND PERMANENTLY RECORDING THE PRESENCE OF A FLAW OR FLAWS IN THE WORKPIECE BY MIGRATION OF MAGNETIZABLE PARTICLES IN THE COMPOSITION TO THE FLAWED AREA WHEN THE WORKPIECE AND CASTING MATERIAL ARE SUBJECTED TO MAGNETIC FLUX COMPRISING: A BASE FORMULATON HAVING A. ABOUT 100 PARTS BY WEIGHT SILICONE RUBBER COMPOUND, VULCANIZABLE AT ROOM TEMPERATURE BY ADDITION OF SUITABLE CATALYST MATERIAL THERETO, AND COMPRISING A SUBSTANTIALLY LINEAR POLYDIMETHYL SILOXANE B. ABOUT 0.1 TO 10.0 PARTS BY WEIGHT OF FERROMAGNETIC PARTICLES IN THE SIZE RANGE OF FROM ABOUT 5 TO 60 MICRONS; C. A LIQUID NAPHTHA HYDROCARBON DILUENT IN AN AMOUNT SUFFICIENT TO ADJUST VISCOSITY OF THE FORMULATION TO WITHIN A RANGE OF ABOUT 1 TO ABOUT 120 POISES; AND ABOUT ABOUT 0.2 TO ABOUT 6 PARTS BY WEIGHT PER 100 PARTS OF SAID BASE FORMULATION OF A CATALYST COMPRISING A METALLIC SOAP FOR VULCANIZING SAID SILICONE RUBBER COMPOUND TO SAID FLEXIBLE ELASTIC FORM; SAID RUBBER DIFFERING IN COLOR FROM SAID FERROMAGNETIC PARTICLES TO PROVIDE VISUAL CONTRAST BETWEEN SAID COMPOSITION AS A WHOLE AND AN ACCUMULATION THEREIN OF SAID PARTICLES AT THE AREA OF A DETECTED FLAW WHEN SAID COMPOSITION IS CURED OR VULCANIZED.
Claim 3
Dependent Claim 25 words
The composition defined by claim 1 wherein said metallic soap comprises a compound selected from the group consisting of stannous octoate and dibutyl tin dilaurate.
Claim 4
Dependent Claim 22 words
The composition defined by claim 1 wherein said formulation has a viscosity within the range of about 1 to about 10 poises.
Claim 5
Dependent Claim 26 words
The composition defined by claim 2 wherein said catalyst consists of about 0.3 parts by weight of stannous octoate per 100 parts of said base formulation.
Claim 6
Dependent Claim 27 words
The composition defined by claim 2 wherein said catalyst consists of about 5 parts by weight of dibutyl tin dilaurate per 100 parts of said base formulation.
Claim 7
Dependent Claim 25 words
The composition defined by claim 2 wherein said catalyst consists of about 1 part by weight dibutyl tin dilaurate per 100 parts of base formulation.
Claim 8
Dependent Claim 28 words
The composition of claim 2 wherein said catalyst is dibutyl tin dilaurate employed in parts, by weight, of about 3 parts per 100 parts of said base formulation.
Claim 9
Dependent Claim 27 words
The composition of claim 1 wherein said ferromagnetic particles are selected from the group consisting of black iron oxide (Fe3O4), metallic iron, metallic nickel and mixtures thereof.
Claim 10
Dependent Claim 18 words
The composition of claim 1 wherein said diluent is a naphtha hydrocarbon having a flash point exceeding 200*F.
Claim 11
Dependent Claim 18 words
The composition of claim 1 wherein water is added to reduce the time required for curing the composition.
Claim 12
Dependent Claim 52 words
The composition of claim 1 wherein said rubber is present as about 100 parts by weight, said naphtha diluent is present as about 50 parts by weight and said ferromagnetic particles are black iron oxide (Fe3O4) present as about 2 parts by weight, said formulation having a viscosity of about 5 poises.

References Cited (Backward Citations)

US2601212A Cited
US2791561A Cited
US2744040A Cited
US3087832A Cited
US3345564A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-01-20 1978-07-22 1979-01-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-01-20 1982-07-22 1983-01-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-01-20 1986-07-22 1987-01-21 $7700.00 Window Closed / Lapsed

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