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US3856918A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the beneficiation of titaniferous ores utilizing hot wall continuous plasma reactor

Assignee: KEMIRA Inc A GA CORP
•
Filing: 1973-03-28
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Granted: 1974-12-24
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Expires: 1993-03-28
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Abstract

Abstract There is provided a process for the beneficiation of titaniferous ores utilizing a plasma jet to carry out the high temperature reduction of the oxides of iron with a hydrocarbon gas in a hot wall continuous plasma reactor which enables particulate solids to be recovered. Iron can readily be removed by leaching or magnetic separation of the particulate solids so as to obtain a feed product containing 90-97 percent titania which is eminently suitable as a feed material for manufacturing titanium dioxide pigment by the chloride process.

Inventors

  • 👤 J Skrivan
  • 👤 J Chase

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 18:15
CPC Classifications
C; C22; C22B; C22B5/00; C22B5/02; C22B5/12; B; B01; B01J; B01J15/00; C22B34/00; C22B34/10; C22B34/12; C22B34/1204; C22B4/00; C22B4/005; H; H01; H01J; H01J37/00; H01J37/32; B01J2219/00; B01J2219/08; B01J2219/0894; Y; Y10; Y10S; Y10S423/00; Y10S423/09; Y10S423/10

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 314 words
A PROCESS FOR BENEFICIATING TITANIFEROUS ORES UTILIZING A HOT WALL CONTINUOUS PLASMA JET REACTOR ADAPTED FOR THE PRODUCTION OF AT LEAST A 90 PERCENT TIO2 MATERIAL HAVING IN COMBINATION A VERTICALLY POSITIONED, ELONGATED, WATER-COOLED CASING HAVING AN UPPER HOT WALL REACTOR ZONE, A MIDDLE REACTOR BASE ZONE, AND A LOWER COOL WALL ZONE, SAID UPPER HOT WALL REACTOR ZONE HAVING MEANS FOR INTRODUCING A PLASMA REDUCING GAS, MEANS FOR INTRODUCING TITANIFEROUS FEED MATERIAL INTO THE LATTER CHAMBER ON WHICH MOLTEN SLAG FLOWS, SAID REACTOR ZONE HAVING A LENGTH OF DIAMETER RATIO GREATER THAN 3; SAID MIDDLE REACTOR BASE ZONE HAVING A VERTICAL CHAMBER OF DIAMETER EQUAL TO AT LEAST THREE TIMES THAT OF THE DIAMETER IN SAID UPPER HOT WALL REACTOR ZONE, AND MEANS FOR QUENCHING SAID MOLTEN SLAG IMMEDIATELY EMANATING FROM THE SAID UPPER REACTION ZONE SO AS TO FORM DISCRETE DROPS OR PARTICLES; AND SAID LOWER COOL-WATER ZONE HAVING A WATER-COOLED CHAMBER, WHICH COMPRISES THE STEPS OF: INTRODUCING A GROUND LOW-GRADE TITANIFEROUS ORE COMPRISING TITANIUM AND IRON VALUES INTO A REACTION ZONE OF SAID PLASMA JET REACTOR WHERE OXIDES OF IRON IN THE ORE ARE PARTIALLY OR COMPLETELY REDUCED BY HOT HYDROCARBON GAS IN WHICH THE LENGTH TO DIAMETER RATIO OF THE REACTION ZONE IS AT LEAST 3, CONTACTING AN MELTING SAID ORE WITH A REDUCING GAS EFFLUENT OF A PLASMA TORCH OR ARC FOR A PERIOD FROM 0.01 TO 5.0 MINUTES, FLOWING MOLTEN ORE PREDOMINATELY ON THE WALLS OF SAID REACTION ZONE, QUENCHING THE MOLTEN ORE AT THE BASE OF THE SAID UPPER REACTION ZONE SO AS TO BREAK-UP MOLTEN ORE INTO DROPLETS THEREBY SOLIDIFYING THE MOLTEN ORE AFTER SAID QUENCH IN A RECTION BASE ZONE, EFFECTING FREE FALL OF THE SO BROKEN-UP AND SOLIDIFIED MATERIAL THROUGH SAID REACTOR BASE ZONE WITHOUT TOUCHING THE WALL OF SAID LATTER REACTOR, SAID RECOVERING SAID SOLIDIFIED DROPLET CONTAINING AT LEAST ABOUT 90 PERCENT TIO2.
Claim 2
Dependent Claim 314 words
A PROCESS FOR BENEFICIATING TITANIFEROUS ORES UTILIZING A HOT WALL CONTINUOUS PLASMA JET REACTOR ADAPTED FOR THE PRODUCTION OF AT LEAST A 90 PERCENT TIO2 MATERIAL HAVING IN COMBINATION A VERTICALLY POSITIONED, ELONGATED, WATER-COOLED CASING HAVING AN UPPER HOT WALL REACTOR ZONE, A MIDDLE REACTOR BASE ZONE, AND A LOWER COOL WALL ZONE, SAID UPPER HOT WALL REACTOR ZONE HAVING MEANS FOR INTRODUCING A PLASMA REDUCING GAS, MEANS FOR INTRODUCING TITANIFEROUS FEED MATERIAL INTO THE LATTER CHAMBER ON WHICH MOLTEN SLAG FLOWS, SAID REACTOR ZONE HAVING A LENGTH OF DIAMETER RATIO GREATER THAN 3; SAID MIDDLE REACTOR BASE ZONE HAVING A VERTICAL CHAMBER OF DIAMETER EQUAL TO AT LEAST THREE TIMES THAT OF THE DIAMETER IN SAID UPPER HOT WALL REACTOR ZONE, AND MEANS FOR QUENCHING SAID MOLTEN SLAG IMMEDIATELY EMANATING FROM THE SAID UPPER REACTION ZONE SO AS TO FORM DISCRETE DROPS OR PARTICLES; AND SAID LOWER COOL-WATER ZONE HAVING A WATER-COOLED CHAMBER, WHICH COMPRISES THE STEPS OF: INTRODUCING A GROUND LOW-GRADE TITANIFEROUS ORE COMPRISING TITANIUM AND IRON VALUES INTO A REACTION ZONE OF SAID PLASMA JET REACTOR WHERE OXIDES OF IRON IN THE ORE ARE PARTIALLY OR COMPLETELY REDUCED BY HOT HYDROCARBON GAS IN WHICH THE LENGTH TO DIAMETER RATIO OF THE REACTION ZONE IS AT LEAST 3, CONTACTING AN MELTING SAID ORE WITH A REDUCING GAS EFFLUENT OF A PLASMA TORCH OR ARC FOR A PERIOD FROM 0.01 TO 5.0 MINUTES, FLOWING MOLTEN ORE PREDOMINATELY ON THE WALLS OF SAID REACTION ZONE, QUENCHING THE MOLTEN ORE AT THE BASE OF THE SAID UPPER REACTION ZONE SO AS TO BREAK-UP MOLTEN ORE INTO DROPLETS THEREBY SOLIDIFYING THE MOLTEN ORE AFTER SAID QUENCH IN A RECTION BASE ZONE, EFFECTING FREE FALL OF THE SO BROKEN-UP AND SOLIDIFIED MATERIAL THROUGH SAID REACTOR BASE ZONE WITHOUT TOUCHING THE WALL OF SAID LATTER REACTOR, SAID RECOVERING SAID SOLIDIFIED DROPLET CONTAINING AT LEAST ABOUT 90 PERCENT TIO2.
Claim 3
Dependent Claim 22 words
The process according to claim 1 wherein the solidified droplets are leached with hydrochloric acid to remove iron values from said droplets.
Claim 4
Dependent Claim 18 words
The process according to claim 1 wherein the solidified droplets are magnetically treated to remove iron values therefrom.
Claim 5
Dependent Claim 30 words
The process according to claim 2 wherein the hydrochloric acid leached solidified droplets are hydrolyzed to recover a product ranging from 90 percent - 97 percent TiO2 as particulate solids.
Claim 6
Dependent Claim 18 words
The process according to claim 1 where the reducing gas effluent of the plasma torch is a hydrocarbon.
Claim 7
Dependent Claim 17 words
The process according to claim 1 where the reducing gas effluent of the plasma torch is methane.
Claim 8
Dependent Claim 17 words
The process according to claim 1 where the reducing gas effluent of the plasma torch is hydrogen.
Claim 9
Dependent Claim 19 words
The process according to claim 1 where the solidified droplets of slag are less than 1/16 inch in diameter.

References Cited (Backward Citations)

US3429665A Cited
US3446590A Cited
US3787139A Cited
US3649189A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-12-23 1978-06-24 1978-12-24 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-12-23 1982-06-24 1982-12-24 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-12-23 1986-06-24 1986-12-24 $7700.00 Window Closed / Lapsed

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