US3855020A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Processing for high permeability silicon steel comprising copper
Assignee: Allegheny Ludlum Corp
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Filing: 1973-05-07
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Granted: 1974-12-17
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Expires: 1993-05-07
Abstract
Abstract A process for producing silicon steel having a cube-on-edge orientation and a permeability of at least 1850 (G/Oe) at 10 oersteds, which includes the steps of: annealing silicon steel prior to a final cold roll at a temperature of from 1400* to 2150*F; cooling the steel from a temperature below 1700*F and above 750*F to a temperature at least as low as 500*F at a rate which is faster than a still air cool and from its maximum annealing temperature to the temperature below 1700*F and above 750*F at a rate which is no faster than a still air cool; and cold rolling the steel at a reduction of at least 80 percent.
Inventors
- 👤 J Salsgiver
- 👤 F Malagari
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 04:18
CPC Classifications
C; C22; C22C; C22C38/00; C22C38/02; C21; C21D; C21D8/00; C21D8/12; C21D8/1244; C21D8/1266; C21D8/1261
Claims Analysis
Total Claims: 19
Claim 1
Independent Claim
250 words
IN A PROCESS FOR PRODUCING ELECTROMAGNETIC SILICON STEEL HAVING A CUBE-ON-EDGE ORIENTATION AND A PERMEABILITY OF AT LEAST 1850 (G/OE) AT 10 OERSTEDS, WHICH PROCESS INCLUDES THE STEPS OF: ROLLING SAID STEEL INTO A HOT ROLLED BAND; SUBJECTING SAID STEEL TO AT LEAST ONE COLD ROLLING; SUBJECTING SAID STEEL TO A FINAL ANNEALING PRIOR TO THE FINAL COLD ROLLING; DECARBURIZING SAID STEEL; AND FINAL TEXTURE ANNEALING SAID STEEL; THE IMPROVEMENT COMPRISING THE STEPS OF CARRYING OUT SAID FINAL ANNEAL PRIOR TO THE FINAL COLD ROLLING AT A TEMPERATURE OF FROM 1400* TO 2150*F FOR A PERIOD OF FROM 15 SECONDS TO 2 HOURS; COOLING SAID STEEL FROM A TEMPERATURE BELOW 1700*F AND ABOVE 750*F TO A TEMPERATURE AT LEAST AS LOW AS 500*F WITH A LIQUID QUENCHING MEDIUM OR GASEOUS STREAM AND FROM ITS MAXIMUM ANNEALING TEMPERATURE TO SAID TEMPERATURE BELOW 1700*F AND ABOVE 750*F AT A RATE WHICH IS NO FASTER THAN ONE WHEREIN THE STEEL IS COOLED IN A STATIC ATMOSPHERE OR IN A CONTINUOUS PROCESSING LINE WHERE THERE IS SOME RELATIVE MOTION BETWEEN THE ATMOS SPHERE AND THE STEEL, ALTHOUGH THE ONLY DELIBERATE MOTION IS THAT IMPARTED TO THE STEEL; AND COLD ROLLING THE COOLED STEEL AT A REDUCTION OF AT LEAST 80 PERCENT; SAID MELT CONSISTING ESSENTIALLY OF, BY WEIGHT, UP TO 0.70% CARBON FROM 2.60 TO 4.0% SILICON, FROM 0.03 TO 0.24% MANGANESE, FROM 0.01 TO 0.07% SULFUR, FROM 0.015 TO 0.04% ALUMINUM, UP TO 0.02% NITROGEN, FROM 0.1 TO 0.5% AND THE BALANCE IRON.
Claim 2
Dependent Claim
250 words
IN A PROCESS FOR PRODUCING ELECTROMAGNETIC SILICON STEEL HAVING A CUBE-ON-EDGE ORIENTATION AND A PERMEABILITY OF AT LEAST 1850 (G/OE) AT 10 OERSTEDS, WHICH PROCESS INCLUDES THE STEPS OF: ROLLING SAID STEEL INTO A HOT ROLLED BAND; SUBJECTING SAID STEEL TO AT LEAST ONE COLD ROLLING; SUBJECTING SAID STEEL TO A FINAL ANNEALING PRIOR TO THE FINAL COLD ROLLING; DECARBURIZING SAID STEEL; AND FINAL TEXTURE ANNEALING SAID STEEL; THE IMPROVEMENT COMPRISING THE STEPS OF CARRYING OUT SAID FINAL ANNEAL PRIOR TO THE FINAL COLD ROLLING AT A TEMPERATURE OF FROM 1400* TO 2150*F FOR A PERIOD OF FROM 15 SECONDS TO 2 HOURS; COOLING SAID STEEL FROM A TEMPERATURE BELOW 1700*F AND ABOVE 750*F TO A TEMPERATURE AT LEAST AS LOW AS 500*F WITH A LIQUID QUENCHING MEDIUM OR GASEOUS STREAM AND FROM ITS MAXIMUM ANNEALING TEMPERATURE TO SAID TEMPERATURE BELOW 1700*F AND ABOVE 750*F AT A RATE WHICH IS NO FASTER THAN ONE WHEREIN THE STEEL IS COOLED IN A STATIC ATMOSPHERE OR IN A CONTINUOUS PROCESSING LINE WHERE THERE IS SOME RELATIVE MOTION BETWEEN THE ATMOS SPHERE AND THE STEEL, ALTHOUGH THE ONLY DELIBERATE MOTION IS THAT IMPARTED TO THE STEEL; AND COLD ROLLING THE COOLED STEEL AT A REDUCTION OF AT LEAST 80 PERCENT; SAID MELT CONSISTING ESSENTIALLY OF, BY WEIGHT, UP TO 0.70% CARBON FROM 2.60 TO 4.0% SILICON, FROM 0.03 TO 0.24% MANGANESE, FROM 0.01 TO 0.07% SULFUR, FROM 0.015 TO 0.04% ALUMINUM, UP TO 0.02% NITROGEN, FROM 0.1 TO 0.5% AND THE BALANCE IRON.
Claim 3
Dependent Claim
65 words
An improvement according to claim 1, wherein said steel is cooled from a temperature below 1600*F and above 1200*F to a temperature at least as low as 500*F at a rate which is faster than a still air cool and from its maximum annealing temperature to said temperature below 1600*F and above 1200*F at a rate which is no faster than a still air cool.
Claim 4
Dependent Claim
25 words
An improvement according to claim 1, wherein said final anneal prior to the final cold rolling is at a temperature of from 1800* to 2125*F.
Claim 5
Dependent Claim
65 words
An improvement according to claim 3, wherein said steel is cooled from a temperature below 1600*F and above 1200*F to a temperature at least as low as 500*F at a rate which is faster than a still air cool and from its maximum annealing temperature to said temperature below 1600*F and above 1200*F at a rate which is no faster than a still air cool.
Claim 6
Dependent Claim
32 words
An improvement according to claim 1 wherein said steel is cooled to a temperature at least as low as 500*F from a temperature below 1700F and above 750*F with a gaseous stream.
Claim 7
Dependent Claim
33 words
An improvement according to claim 1 wherein said steel is cooled to a temperature at least as low as 500*F from a temperature below 1700*F and above 750*F with a liquid quenching medium.
Claim 8
Dependent Claim
20 words
An improvement according to claim 1 wherein said steel is air cooled to said temperature below 1700*F and above 750*F.
Claim 9
Dependent Claim
32 words
An improvement according to claim 3 wherein said steel is cooled to a temperature at least as low as 500*F from a temperature below 1700*F and above 750*F with a gaseous stream.
Claim 10
Dependent Claim
33 words
An improvement according to claim 3 wherein said steel is cooled to a temperature at least as low as 500*F from a temperature below 1700F and above 750*F with a liquid quenching medium.
Claim 11
Dependent Claim
20 words
An improvement according to claim 3 wherein said steel is air cooled to said temperature below 1700*F and above 750*F.
Claim 12
Dependent Claim
25 words
An improvement according to claim 1, wherein said final anneal prior to the final cold rolling is carried out subsequent to an initial cold rolling.
Claim 13
Dependent Claim
90 words
An improvement according to claim 1, wherein said steel consists essentially of, by weight, from 0.02 to 0.07% carbon, from 2.60 to 3.5% silicon, a manganese equivalent of from 0.05 to 0.24% as expressed by an equivalency equation of % Mn + (0.1 to 0.25) X % Cu, from 0.01 to 0.05% sulfur, from 0.015 to 0.04% aluminum, from 0.0030 to 0.0090% nitrogen, from 0.1 to 0.3% copper, balance iron and residuals; and wherein the ratio of manganese equivalent to sulfur is in the range of from 2.0 to 4.75.
Claim 14
Dependent Claim
21 words
An improvement according to claim 1, wherein the cooled steel is cold rolled at a reduction of at least 85 percent.
Claim 15
Dependent Claim
21 words
An improvement according to claim 4, wherein the cooled steel is cold rolled at a reduction of at least 85 percent.
Claim 16
Dependent Claim
23 words
An improvement according to claim 1 wherein said final anneal prior to the final cold rolling is applied to a hot rolled band.
Claim 17
Dependent Claim
34 words
An improvement according to claim 1 wherein said steel has at least 0.15% Cu and wherein said final anneal prior to the final cold rolling is at a temperature of from 1400* to 1700*F.
Claim 18
Dependent Claim
29 words
An improvement according to claim 16 wherein said steel is cooled to a temperature at least as low as 500*F from a temperature above 750*F with a gaseous stream.
Claim 19
Dependent Claim
30 words
An improvement according to claim 16 wherein said steel is cooled to a temperature at least as low as 500*F from a temperature above 750*F with a liquid quenching medium.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1977-12-16 | 1978-06-17 | 1978-12-17 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1981-12-16 | 1982-06-17 | 1982-12-17 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1985-12-16 | 1986-06-17 | 1986-12-17 | $7700.00 | Window Closed / Lapsed |