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US3842266A Expired / Lapsed US ⏱️ 0.0 years remaining

Atmospheric sampling probe for a mass spectrometer

Assignee: United States Department of the Air Force
•
Filing: 1973-04-11
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Granted: 1974-10-15
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Expires: 1993-04-11
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Abstract

Abstract An atmospheric sampling probe capable of generating a molecular beam for mass spectrometer analyzation including a quartz gas inlet orifice adjustable in any plane with a first vacuum stage; a quartz skimmer orifice adjustable in one plane having a second vacuum stage and a collimating orifice and ionizing chamber adapted to be connected to a quadrupole mass spectrometer with a third vacuum stage.

Inventors

  • 👤 R Thomas

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 02:48
CPC Classifications
H; H01; H01J; H01J49/00; H01J49/02; H01J49/24; G; G01; G01N; G01N1/00; G01N1/02; G01N1/22; G01N1/2273; G01N33/00; G01N33/48; G01N33/483; G01N33/497

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 195 words
A system for continuously sampling gases at atmospheric pressure comprising: a sample probe means, including a first microorifice mounted on a frame and movable in any plane, a second microorifice positioned in line with said first microorifice, adjacent thereto and movable in one plane and a third orifice positioned in line with said first and second microorifices and spaced therefrom; a first stage vacuum system for creating a vacuum; a first vacuum chamber, connected between said first microorifice and said first stage vacuum system; a second stage vacuum system for creating a vacuum of greater magnitude than the first stage vacuum system; a second vacuum chamber positioned within said first vacuum chamber connecting the second stage vacuum system and said second microorifice; a third stage vacuum system for creating a vacuum of greater magnitude than said second stage vacuum system; a third vacuum chamber, connected between said third stage vacuum system and said third orifice, in juxtaposition to said second vacuum chamber and a mass spectrometer detector means connected to the said third vacuum chamber whereby gases entering the sampling probe means pass therethrough forming an uncontaminated molecular beam for detection in the mass spectrometer.
Claim 2
Independent Claim 195 words
A system for continuously sampling gases at atmospheric pressure comprising: a sample probe means, including a first microorifice mounted on a frame and movable in any plane, a second microorifice positioned in line with said first microorifice, adjacent thereto and movable in one plane and a third orifice positioned in line with said first and second microorifices and spaced therefrom; a first stage vacuum system for creating a vacuum; a first vacuum chamber, connected between said first microorifice and said first stage vacuum system; a second stage vacuum system for creating a vacuum of greater magnitude than the first stage vacuum system; a second vacuum chamber positioned within said first vacuum chamber connecting the second stage vacuum system and said second microorifice; a third stage vacuum system for creating a vacuum of greater magnitude than said second stage vacuum system; a third vacuum chamber, connected between said third stage vacuum system and said third orifice, in juxtaposition to said second vacuum chamber and a mass spectrometer detector means connected to the said third vacuum chamber whereby gases entering the sampling probe means pass therethrough forming an uncontaminated molecular beam for detection in the mass spectrometer.
Claim 3
Dependent Claim 19 words
A system for sampling gases according to claim 1 wherein said first and second orifices are formed of quartz.
Claim 4
Dependent Claim 50 words
A system for sampling gases according to claim 2 wherein said first stage vacuum system includes a pump, means for removing condensibles from said stage, and ballast means between the pump and condensibles removing means to prevent overload to the pump when the probe means is open to atmosphereic pressure.
Claim 5
Dependent Claim 19 words
A system for sampling gases according to claim 3 wherein said second stage vacuum system includes a turbomolecular pump.
Claim 6
Dependent Claim 17 words
A system for sampling gases according to claim 4 wherein said third stage include an ion pump.

References Cited (Backward Citations)

US2721270A Cited
US2769912A Cited
US2880323A Cited
US3227872A Cited
US3270773A Cited
US3385102A Cited
US3633027A Cited
US3639757A Cited
US3673405A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-10-14 1978-04-15 1978-10-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-10-14 1982-04-15 1982-10-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-10-14 1986-04-15 1986-10-15 $7700.00 Window Closed / Lapsed

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