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US3835658A Expired / Lapsed US ⏱️ 0.0 years remaining

Freeze crystallization of saline water with a direct contact refrigerant

Assignee: United Kingdom Atomic Energy Authority
•
Filing: 1973-01-31
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Granted: 1974-09-17
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Expires: 1993-01-31
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Abstract

Abstract A method and apparatus for the desalination of saline water by freezing in which a mixture of ice and concentrated saline water is formed by cooling the saline water by heat exchange with an evaporating liquid refrigerant, the ice is separated from the concentrated saline water and melted, and at least a portion of the evaporated refrigerant is reliquified by heat exchange with an aqueous solution which is itself cooled by heat exchange with liquid methane or liquid natural gas.

Inventors

  • 👤 J Wilson

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 23:34
CPC Classifications
F; F25; F25C; F25C1/00; B; B01; B01D; B01D9/00; B01D9/0004; B01D9/0009; B01D9/0059; C; C02; C02F; C02F1/00; C02F1/22; C02F2103/00; C02F2103/08; Y; Y02; Y02A; Y02A20/00; Y02A20/124

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 14 words
A method as claimed in claim 1 wherein the aqueous solution comprises sodium chloride.
Claim 2
Dependent Claim 15 words
A method as claimed in claim 1 wherein the aqueous solution comprises calcium chloride hexahydrate.
Claim 3
Dependent Claim 16 words
A method as claimed in claim 1 wherein the aqueous solution comprises an aqueous organic solution.
Claim 4
Dependent Claim 95 words
Apparatus for the desalination of saline water by freezing, the apparatus comprising a crystalliser in which a mixture of ice and concentrated saline water is formed by cooling the saline water by heat exchange with an evaporating liquid refrigerant, a wash column in which the ice is separated from the concentrated saline water, a melter in which the separated ice is melted, a condenser for reliquefying a portion of the evaporated refrigerant by heat exchange with an aqueous solution, and a heat exchanger for cooling the aqueous solution with liquid methane or liquid natural gas.
Claim 5
Dependent Claim 59 words
A method according to claim 1 wherein the separated ice is melted by contact with vapors of said liquid refrigerant evaporated while cooling said saline water, a portion of said vapors being condensed to a liquid during melting of said ice, and wherein the remaining, uncondensed, portion of said vapors is reliquefied by heat exchange with said aqueous solution.
Claim 6
Dependent Claim 65 words
Apparatus according to claim 5 including means for conveying evaporated vapors of said liquid refrigerant to said melter for melting said separated ice by contact between said ice and said vapors whereby a portion of said vapors condenses, and means for conveying the remaining, uncondensed, portion of said vapors from said melter to said condenser for reliquefying same by heat exchange with said aqueous solution.

References Cited (Backward Citations)

US3477241A Cited
US2997856A Cited
AU217766A Cited
US3478531A Cited
US3486848A Cited
US3528256A Cited
US3605426A Cited
US3675436A Cited
US3677405A Cited
US3714791A Cited
US3724229A Cited
US3803860A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-09-16 1978-03-18 1978-09-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-09-16 1982-03-18 1982-09-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-09-16 1986-03-18 1986-09-17 $7700.00 Window Closed / Lapsed

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