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US3830652A Expired / Lapsed US ⏱️ 0.0 years remaining

Hot pressed, high strength silicon nitride

Assignee: United States Department of the Army
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Filing: 1973-06-28
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Granted: 1974-08-20
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Expires: 1993-06-28
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Abstract

Abstract The fabrication of high strength, high density, silicon nitride by the addition of between 1.0 to 3.5 percent by weight of yttrium in the form of a compound to silicon nitride powder and pressing the material at temperatures of between 1,750* C. and 1,800* C. and at uniaxial pressures of between 6,000 and 7,000 psi.

Inventors

  • 👤 G Gazza

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 11:44
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/515; C04B35/58; C04B35/584; C04B35/593

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 26 words
A composition according to claim 1 in which the yttrium compound is a member of the group consisting of yttrium chloride, yttrium nitrate and yttrium oxide.
Claim 2
Dependent Claim 14 words
A composition according to claim 1 in which the yttrium compound is yttrium oxide.
Claim 3
Dependent Claim 27 words
A composition according to claim 3 in which the amount of yttrium oxide is about 1.25 to 4.45 weight percent of the weight of the silicon nitride.
Claim 4
Independent Claim 49 words
A method of enhancing the strength of a silicon nitride monolith which comprises adding a powdered yttrium compound to powdered silicon nitride, the weight of yttrium in the yttrium compound being abOut 1.0 to 3.5 percent of the weight of the silicon nitride, and sintering the composition by hot-pressing.
Claim 5
Dependent Claim 14 words
A method according to claim 5 in which the yttrium compound is yttrium oxide.
Claim 6
Dependent Claim 24 words
A method according to claim 6 in which the amount of yttrium oxide is about 1.25 to 4.45 weight percent of the silicon nitride.
Claim 7
Dependent Claim 31 words
A method in accordance with claim 7 in which the sintering is carried out at temperatures between 1,750* C. and 1,800* C. and at pressures between 6,000 psi and 7,000 psi.
Claim 8
Dependent Claim 35 words
A method in accordance with claim 5 in which the sintering is carried out at a temperature of about 1,750* C. to 1,800* C. and at a pressure of about 6,000 psi to 7,000 psi.
Claim 9
Dependent Claim 35 words
A method in accordance with claim 9 in which the sintering is carried out at a temperature of about 1,750* C. to 1,800* C. and at a pressure of about 6,000 psi to 7,000 psi.
Claim 10
Dependent Claim 27 words
A method in accordance with claim 5 in which the yttrium compound is a member of the group consisting of yttrium chloride, yttrium nitrate and yttrium oxide.

References Cited (Backward Citations)

US3108887A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-08-19 1978-02-18 1978-08-20 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-08-19 1982-02-18 1982-08-20 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-08-19 1986-02-18 1986-08-20 $7700.00 Window Closed / Lapsed

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