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US3821841A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for fabricating a beryllium fiber reinforced composite having a titanium matrix

Assignee: Materion Brush Inc
•
Filing: 1972-08-18
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Granted: 1974-07-02
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Expires: 1992-08-18
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Abstract

Abstract A process for forming fibrous beryllium/titanium composites from separate beryllium and titanium materials wherein the resultant composite consists of continuous Be fibers of selective size, array, placement, and geometry in a matrix of continuous Ti or Ti alloy phase. The process is characterized by surrounding discrete preformed Be shapes or fiber precursor bodies with either powdered or preformed Ti material and extruding a cannister containing this assembled body at a temperature of from 1,350* to 1,525*F. to a reduction ratio of from 6/1 to 100/1 or greater to form a consolidated Be/Ti composite having a very limited but discernible intermetallic reaction zone of titanium beryllide formed in situ. After extrusion and cooling, the yield strength of the composite can, if desired, be substantially improved by cold working at 70% to 80% of the ultimate tensile strength. Composite beryllium titanium bodies so fabricated have tensile properties superior to those of Be/Ti composites fabricated up to 1,300*F. and superior ductility, toughness and strength to those of Be/Ti composites made from blended Be and Ti powders hot extruded at 1,350*F. to 1,525*F. Furthermore, because of the capability of controlling the geometry of the array of fibers in composite sections, it is possible to ''''design'''' properties to specific applications. These materials may be fabricated by known techniques into aircraft engine parts, e.g., gas turbine compressor blades, vanes and shafts. They would also be useful in other shaft applications requiring high modulus and low weight such as high speed machinery.

Inventors

  • 👤 V Goodwin

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 19:48
CPC Classifications
C; C22; C22C; C22C47/00; C22C47/02; C22C47/025; C22C47/14; C22C49/00; C22C49/02; C22C49/10; C22C49/11; B; B22; B22F; B22F2998/00; B22F2998/10; B22F2999/00; Y; Y10; Y10S; Y10S29/00; Y10S29/045; Y10S29/047; Y10T; Y10T29/00; Y10T29/49; Y10T29/49801; Y10T428/00; Y10T428/12; Y10T428/12465

Claims Analysis

Total Claims: 20
Claim 1
Independent Claim 17 words
A process in accordance with claim 1 which also includes the step of prestressing the extruded composite.
Claim 2
Dependent Claim 55 words
filling the balance of the assembly with titanium to form a continuous titanium matrix surrounding said bodies; b. encasing said assembly in an extrusion canister; and c. extruding said canister at a temperature of from 1,400* to 1, 525*F. at a reduction ratio of from 6:1 to 100:1 to form a solid fibrous beryllium/titanium composite.
Claim 3
Dependent Claim 30 words
A process in accordance with claim 1 in which the beryllium fiber precursor is formed from beryllium powder having a particle size no greater than 3 X 10 2 inch.
Claim 4
Dependent Claim 23 words
A process in accordance with claim 1 in which the beryllium has a beryllium oxide content of from 0.2% to 6% by weight.
Claim 5
Dependent Claim 20 words
A process in accordance with claim 1 in which the beryllium fiber precursors are composed of vacuum hot pressed beryllium.
Claim 6
Dependent Claim 20 words
A process in accordance with claim 1 in which the beryllium fiber precursors are composed of cold pressed beryllium powder.
Claim 7
Dependent Claim 22 words
A process in accordance with claim 1 in which the beryllium fiber precursors are composed of cold pressed and sintered beryllium powder.
Claim 8
Dependent Claim 23 words
A process in accordance with claim 1 in which the beryllium fiber precursors are composed of cold pressed, sintered and coined beryllium powder.
Claim 9
Dependent Claim 22 words
A process iN accordance with claim 1 in which the beryllium fiber precursors are composed of beryllium powder rigidized with a binder.
Claim 10
Dependent Claim 21 words
A process in accordance with claim 1 in which the titanium is in the form of a -20 +325 mesh powder.
Claim 11
Dependent Claim 25 words
A process in accordance with claim 10 in which the titanium powder has a particle size of no more than 3 X 10 2 inch.
Claim 12
Dependent Claim 18 words
A process in accordance with claim 1 in which the titanium is at least partially consolidated titanium powder.
Claim 13
Dependent Claim 22 words
A process in accordance with claim 1 in which the titanium is in the form of solid cast or wrought titanium metal.
Claim 14
Dependent Claim 15 words
A process in accordance with claim 1 in which the titanium material is titanium alloy.
Claim 15
Dependent Claim 15 words
A process in accordance with claim 14 in which the titanium alloy is Ti-6Al-4V alloy.
Claim 16
Dependent Claim 16 words
A process in accordance with claim 14 in which the titanium alloy is a Ti-5Al-2.5Sn alloy.
Claim 17
Dependent Claim 24 words
A process in accordance with claim 1 which also includes the step of degassing the extrusion canister to less than 10 microns of mercury.
Claim 18
Dependent Claim 25 words
A process in accordance with claim 1 which includes the step of isopressing the extrudable assembly at a pressure of 30 ksi prior to extrusion.
Claim 19
Dependent Claim 18 words
A process in accordance with claim 1 in which the extrusion canister is formed of low carbon steel.
Claim 20
Dependent Claim 27 words
A process in accordance with claim 1 in which the volume percent of beryllium is from 40% to 60%, and the balance is titanium or titanium alloy.

References Cited (Backward Citations)

US2940163A Cited
US3475142A Cited
US3390985A Cited
US3510275A Cited
US3681037A Cited
US3609855A Cited
US3667108A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-07-01 1977-12-31 1978-07-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-07-01 1981-12-31 1982-07-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-07-01 1985-12-31 1986-07-02 $7700.00 Window Closed / Lapsed

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