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US3818111A Expired / Lapsed US ⏱️ 0.0 years remaining

Fining and increasing the chill haze stability of fermented alcoholic beverages

Assignee: Baroid Technology Inc
•
Filing: 1972-11-30
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Granted: 1974-06-18
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Expires: 1992-11-30
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Abstract

Abstract A novel process of fining and removing chill haze precursor substances from vegetable beverages, particularly beer, in order to improve the clarity and chill haze stability of such beverages which is characterized by the separate addition to the beverage of a nitrogeneous carbonyl containing organic material which is water soluble or colloidially dispersible in water selected from the group consisting of gelatin, N-vinylpyrrolidone and polymers of N-vinylpyrrolidone and a polysilicic acid coagulant from a source consisting of polysilicic acid hydrosols, stabilized polysilicic acid hydrosols, and polysilicic acid hydrogels in which the polysilicic acid has not polymerized to such an extent that syneresis has occurred, followed by aging of the beverage and removal of coagulated substances from the beverage.

Inventors

  • 👤 L Hoover

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 02:43
CPC Classifications
C; C12; C12H; C12H1/00; C12H1/02

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 10 words
The method of claim 1 wherein said beverage is beer.
Claim 2
Dependent Claim 36 words
The method of claim 2 wherein the amount of the nitrogeneous carbonyl containing organic material added is from 10 to 100 p.p.m. and the amount of the polysilicic acid added is from 50 to 500 p.p.m.
Claim 3
Dependent Claim 21 words
The method of claim 3 wherein the amount of the nitrogeneous carbonyl containing organic material is from 25 to 75 p.p.m.
Claim 4
Dependent Claim 18 words
The method of claim 4 wherein the amount of the polysilicic acid is from 100 to 300 p.p.m.
Claim 5
Dependent Claim 14 words
The method of claim 2 wherein the nitrogeneous carbonyl containing organic material is gelatin.
Claim 6
Dependent Claim 14 words
The method of claim 3 wherein the nitrogeneous carbonyl containing organic material is gelatin.
Claim 7
Dependent Claim 14 words
The method of claim 4 wherein the nitrogeneous carbonyl containing organic material is gelatin.
Claim 8
Independent Claim 224 words
A method of fining and increasing the chill haze stability of a fermented alcoholic beverage, which comprises, the following steps in the order indicated: a. adding to the beverage separately and in any order a nitrogeneous carbonyl containing organic material which is water soluble or colloidially dispersible in water selected from the group consisting of gelatin, N-vinylpyrrolidone, and polymers of N-vinylpyrrolidone and a polysilicic acid coagulant in the form of a stabilized polysilicic acid hydrosol obtained by (1) forming a silicic acid hydrosol by placing an aqueous solution of sodium silicate into intimate contact with a cation exchange resin in its hydrogen form whereby sodium ions in the silicate solution are removed by the resin and replaced with hydrogen ions from the resin, (2) aging the silicic acid hydrosol for a period of time which is sufficient to produce a polysilicic acid hydrosol and insufficient to produce a gelatinous semi-solid hydrogel, and (3) adjusting the silica to alkali oxide ratio of the polysilicic acid hydrosol to a value within the range from 10:1 to 500:1 with sodium hydroxide; b. aging the treated beverage for a period of time sufficient to allow the nitrogeneous carbonyl containing organic material and the polysilicic acid to coagulate and simultaneously fine and remove chill haze precursor substances from the beverage; and c. separating the coagulated substances from the beverage.
Claim 9
Dependent Claim 10 words
The method of claim 9 wherein the beverage is beer.
Claim 10
Dependent Claim 36 words
The method of claim 10 wherein the amount of the nitrogeneous carbonyl containing organic material added is from 10 to 100 p.p.m. and the amount of the polysilicic acid added is from 50 to 500 p.p.m.
Claim 11
Dependent Claim 21 words
The method of claim 11 wherein the amount of the nitrogeneous carbonyl containing organic material is from 25 to 75 p.p.m.
Claim 12
Dependent Claim 18 words
The method of claim 12 wherein the amount of the polysilicic acid is from 100 to 300 p.p.m.
Claim 13
Dependent Claim 14 words
The method of claim 10 wherein the nitrogeneous carbonyl containing organic material is gelatin.
Claim 14
Dependent Claim 23 words
The method of claim 14 wherein the gelatin is added to the beverage before the polysilicic acid coagulant is added to the beverage.
Claim 15
Dependent Claim 14 words
The method of claim 11 wherein the nitrogeneous carbonyl containing organic material is gelatin.
Claim 16
Dependent Claim 23 words
The method of claim 6 wherein the gelatin is added to the beverage before the polysilicic acid coagulant is added to the beverage.

References Cited (Backward Citations)

CA454856A Cited
US2316241A Cited
US3617301A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-06-17 1977-12-17 1978-06-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-06-17 1981-12-17 1982-06-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-06-17 1985-12-17 1986-06-18 $7700.00 Window Closed / Lapsed

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