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US3811484A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and apparatus for delivering a predetermined volume of a liquid

Assignee: Individual
•
Filing: 1971-11-08
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Granted: 1974-05-21
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Expires: 1991-11-08
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Abstract

Abstract The present invention resides in a method and apparatus suitable for laboratory or like use for transferring from one container a measured quantity of a liquid into a second container, this being accomplished by establishing a pressure difference preferably by suction applied temporarily to the second container, the first container having in it a dip pipe extending down to a selected level and leading into the second container through a stopper.

Inventors

  • 👤 E Engelbrecht

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 12:24
CPC Classifications
B; B01; B01L; B01L3/00; B01L3/02; B01L3/0289; B01L3/0293

Claims Analysis

Total Claims: 17
Claim 1
Independent Claim 224 words
A method of dividing a predetermined quantity of a liquid present in a first container into two predetermined parts one of which remains in said first container and the other of which is delivered to a second container which comprises charging a first container with a predetermined volume of a liquid to be distributed, inserting into the first container a first leg of a generally U-shaped tubular pipe so that the open end of the first leg faces upward and is located at a predetermined distance from the bottom of the first container thus establishing a known quantity of liquid above the open end, inserting the second leg of the U-shaped pipe into a second container, creating a pressure differential between the containers such that the first container is at a higher pressure than the second so that said known quantity of liquid above the open end of said first leg is moved through the U-shaped pipe to said second container, said known quantity of liquid above the open end of said first leg being caused first to move downwardly through the leg of said U-shaped pipe and then to move upwardly through said leg the upwardly facing open end of said first leg limiting inaccuracy of measurement due to meniscus deformation when the known quantity of liquid is moved through said first leg.
Claim 2
Independent Claim 224 words
A method of dividing a predetermined quantity of a liquid present in a first container into two predetermined parts one of which remains in said first container and the other of which is delivered to a second container which comprises charging a first container with a predetermined volume of a liquid to be distributed, inserting into the first container a first leg of a generally U-shaped tubular pipe so that the open end of the first leg faces upward and is located at a predetermined distance from the bottom of the first container thus establishing a known quantity of liquid above the open end, inserting the second leg of the U-shaped pipe into a second container, creating a pressure differential between the containers such that the first container is at a higher pressure than the second so that said known quantity of liquid above the open end of said first leg is moved through the U-shaped pipe to said second container, said known quantity of liquid above the open end of said first leg being caused first to move downwardly through the leg of said U-shaped pipe and then to move upwardly through said leg the upwardly facing open end of said first leg limiting inaccuracy of measurement due to meniscus deformation when the known quantity of liquid is moved through said first leg.
Claim 3
Dependent Claim 65 words
The method as claimed in claim 1 wherein said second container is cylindrical which comprises directing the end of the second leg of said U-shaped pipe at an angle to the axis of said container to cause liquid issuing therefrom into the second container to impinge on the wall of said container and to produce a rotary movement of any liquid in said second container.
Claim 4
Dependent Claim 37 words
The methoD as claimed in claim 1 wherein the end of the first leg of said U-shaped pipe is hooked and the leg is inserted into the first container so that its open end is turned upwardly.
Claim 5
Dependent Claim 205 words
Apparatus for delivering a predetermined volume of liquid from a first container to a second container comprising at least a first and second container, means operable to divide the predetermined quantity of the liquid contained in said first container into two predetermined quantities and for transferring one of said predetermined quantities of said liquid into said second container, said means being actuated by a reduction of the pressure in said second container relative to that in said first container and consisting of a first pipe extending into said first container, the end of said pipe being turned upwardly with the open upwardly facing end of said first pipe within said first container determining the lowest level to which liquid can be withdrawn from said first container and limiting inaccuracy of measurement due to meniscus deformation when the liquid reaches said lowest level, a second pipe extending into said second container through a stopper adapted to seal the opening of said second container when applied thereto, third pipe means connecting said first pipe to said second pipe, and means provided in said stopper through which suction can be applied to said second container when said second container has beeen sealed by application of said stopper thereto.
Claim 6
Dependent Claim 205 words
Apparatus for delivering a predetermined volume of liquid from a first container to a second container comprising at least a first and second container, means operable to divide the predetermined quantity of the liquid contained in said first container into two predetermined quantities and for transferring one of said predetermined quantities of said liquid into said second container, said means being actuated by a reduction of the pressure in said second container relative to that in said first container and consisting of a first pipe extending into said first container, the end of said pipe being turned upwardly with the open upwardly facing end of said first pipe within said first container determining the lowest level to which liquid can be withdrawn from said first container and limiting inaccuracy of measurement due to meniscus deformation when the liquid reaches said lowest level, a second pipe extending into said second container through a stopper adapted to seal the opening of said second container when applied thereto, third pipe means connecting said first pipe to said second pipe, and means provided in said stopper through which suction can be applied to said second container when said second container has beeen sealed by application of said stopper thereto.
Claim 7
Independent Claim 328 words
A method of geometrically diluting a liquid which comprises charging a first container of a series of at least three containers with a predetermined volume of liquid to be diluted geometrically, charging the remaining containers of the series with a predetermined volume of diluent, inserting a generally U-shaped tubular pipe between the first and second containers so that the open end of the tubular pipe in the first container faces upwardly and is at a predetermined distance from the bottom of the container thereby establishing a known quantity of of liquid to be diluted above the open end, creating a pressure differential between the first and second containers such that the first container is at a higher pressure than the second, moving the known quantity of liquid to be diluted above the open end of the tubular pipe in the first container through the U-shaped tubular pipe into the second container by means of the pressure differential, mixing the liquid to be diluted which has been moved into the second container with the diluent in the second container, withdrawing the legs of the U-shaped tubular pipe from the first and second containers, then inserting the U-shaped pipe between the second and third containers so that the open end of the tubular pipe in the second container is at a predetermined distance from the bottom of the container and faces upwardly thereby establishing a known quantity of liquid to be further diluted above the open end thereof, creating a pressure differential between the second and third containers such that the second container is at a higher pressure than the third, moving the known quantity of liquid to be further diluted above the end of the tubular pipe in the second container through the U-shaped tubular pipe into the third container by means of the pressure differential, and mixing the liquid to be further diluted which has been moved into the third container with the diluent in the third container.
Claim 8
Independent Claim 328 words
A method of geometrically diluting a liquid which comprises charging a first container of a series of at least three containers with a predetermined volume of liquid to be diluted geometrically, charging the remaining containers of the series with a predetermined volume of diluent, inserting a generally U-shaped tubular pipe between the first and second containers so that the open end of the tubular pipe in the first container faces upwardly and is at a predetermined distance from the bottom of the container thereby establishing a known quantity of of liquid to be diluted above the open end, creating a pressure differential between the first and second containers such that the first container is at a higher pressure than the second, moving the known quantity of liquid to be diluted above the open end of the tubular pipe in the first container through the U-shaped tubular pipe into the second container by means of the pressure differential, mixing the liquid to be diluted which has been moved into the second container with the diluent in the second container, withdrawing the legs of the U-shaped tubular pipe from the first and second containers, then inserting the U-shaped pipe between the second and third containers so that the open end of the tubular pipe in the second container is at a predetermined distance from the bottom of the container and faces upwardly thereby establishing a known quantity of liquid to be further diluted above the open end thereof, creating a pressure differential between the second and third containers such that the second container is at a higher pressure than the third, moving the known quantity of liquid to be further diluted above the end of the tubular pipe in the second container through the U-shaped tubular pipe into the third container by means of the pressure differential, and mixing the liquid to be further diluted which has been moved into the third container with the diluent in the third container.
Claim 9
Dependent Claim 30 words
The method as claimed in claim 5 wherein the steps of creating pressure differentials between containers comprises evacuating air from the container which is to be at the lower pressure.
Claim 10
Dependent Claim 47 words
The method as claimed in claim 5 wherein the mixing steps comprise directing the fluid issuing from the U-shaped pipe against the side of the container to induce a rotary motion in said fluid and diluent whereby the fluid is mixed with the diluent in the container.
Claim 11
Dependent Claim 56 words
The method as claimed in claim 5 wherein the steps of moving the liquid through the U-shaped pipe compRise first moving the liquid downwardly through the open end of the pipe and then upwardly through the pipe by providing the pipe with a hook at its open end so that its open end is turned upwardly.
Claim 12
Dependent Claim 259 words
Apparatus for geometrically diluting a liquid which comprises: a. a series of at least three containers, the first of said containers containing a predetermined volume of liquid to be diluted, b. a generally U-shaped tubular pipe to interconnect two adjacent containers in said series, the first leg of said pipe extending into a first container with the open end of said leg facing upwardly and determining the lowest level to which liquid can be withdrawn from the container and limiting inaccuracy of measurement due to meniscus deformation when the liquid reaches said lowest level, the second leg of said pipe extending into a second container adjacent to the first container, c. means for adding a predetermined volume of diluent to a third container adjacent to the container in said series into which the second leg of said U-shaped pipe extends, and d. means for creating a pressure differential between the containers into which the legs of said U-shaped pipe extend, the container into which the first leg extends being at a higher pressure than the container into which the second leg extends thereby causing the fluid above the open end of the first leg of said U-shaped pipe to be transferred through said pipe into the interconnected container to be mixed therein with the diluent present, whereby a predetermined volume of diluent may be added to each container in the series and the liquid to be diluted may be geometrically diluted by sequentially transferring a predetermined amount of the fluid contained in one container to another in the series.
Claim 13
Dependent Claim 259 words
Apparatus for geometrically diluting a liquid which comprises: a. a series of at least three containers, the first of said containers containing a predetermined volume of liquid to be diluted, b. a generally U-shaped tubular pipe to interconnect two adjacent containers in said series, the first leg of said pipe extending into a first container with the open end of said leg facing upwardly and determining the lowest level to which liquid can be withdrawn from the container and limiting inaccuracy of measurement due to meniscus deformation when the liquid reaches said lowest level, the second leg of said pipe extending into a second container adjacent to the first container, c. means for adding a predetermined volume of diluent to a third container adjacent to the container in said series into which the second leg of said U-shaped pipe extends, and d. means for creating a pressure differential between the containers into which the legs of said U-shaped pipe extend, the container into which the first leg extends being at a higher pressure than the container into which the second leg extends thereby causing the fluid above the open end of the first leg of said U-shaped pipe to be transferred through said pipe into the interconnected container to be mixed therein with the diluent present, whereby a predetermined volume of diluent may be added to each container in the series and the liquid to be diluted may be geometrically diluted by sequentially transferring a predetermined amount of the fluid contained in one container to another in the series.
Claim 14
Dependent Claim 56 words
The apparatus as defined in claim 9 wherein the means for creating a pressure differential comprises means for hermetically sealing the container into which the second leg of said U-shaped pipe extends, and means for evacuating air from the container into which the second leg of said U-shaped pipe extends while said container is hermetically sealed.
Claim 15
Dependent Claim 41 words
The apparatus as defined in claim 10 wherein the hermetically sealing means comprises a stopper through which the second leg of said U-shaped pipe extends and which is adapted to seal the mouth of the container to which it is applied.
Claim 16
Dependent Claim 54 words
The apparatus as defined in claim 9 wherein the diluent adding means includes a tubular pipe adjacent to the second leg of said U-shaped pipe and adapted to extend into the container adjacent to the container into which said second leg is adapted to extend and through which the diluent passes into the container.
Claim 17
Dependent Claim 71 words
The apparatus as defined in claim 9 wherein the first leg of said U-shaped tubular pipe is hooked near its open end so that its open end faces upwardly and the liquid to be transferred first passes downwardly and then upwardly in said leg, and the second leg of said U-shaped tubular pipe is slightly bent at its end to direct the liquid issuing therefrom against the side of the container.

References Cited (Backward Citations)

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US1325991A Cited
US978667A Cited
FR917763A Cited
US2724535A Cited
US2884021A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-05-20 1977-11-19 1978-05-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-05-20 1981-11-19 1982-05-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-05-20 1985-11-19 1986-05-21 $7700.00 Window Closed / Lapsed

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