Patent US4510343A successfully refreshed from Google Patents.
US3798014A
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US
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Method of manufacturing crystalline glass articles
Assignee: Individual
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Filing: 1970-11-05
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Granted: 1974-03-19
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Expires: 1990-11-05
Abstract
Abstract A method of making crystalline glass products, comprising: melting the batch mix to obtain a glass crystallizable about the microparticles of metal sulfides present therein, cooling the glass mass to a temperature of 670*-750*C with simultaneous shaping of the material, holding the material at said temperature, raising its temperature to 930*-970*C at a rate of 75*-320*C per hour, holding the material at that temperature, and its subsequently cooling at a controlled rate.
Inventors
- 👤 V Minakov
- 👤 A Strekalov
- 👤 T Golius
- 👤 A Minakov
- 👤 K Bondarev
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 17:05
CPC Classifications
C; C03; C03C; C03C10/00; C03C10/0036
Claims Analysis
Total Claims: 1
Claim 1
Independent Claim
206 words
A method of making a crystalline glass product comprising the steps of melting a batch mix until a glass is obtained in which the main components are taken in the following quantities, in weight per cent: SiO2, 45 to 69; CaO, 18 to 45; and Al2O3, 2 to 22; and sulfur sulfide in an amount from 0.3 to 0.5 per cent, at least a stoichiometric quantity of iron ions, and further additives of Na2O, up to 5 per cent, and fluorine, up to 2 per cent; shaping a blank while the glass mass being shaped is cooled down to a temperature of 670*-750*C at which crystallization centers in the form of FeS are formed; holding the product at said temperature; raising the temperature to 930*-970*C at a rate of 75-320'''' an hour; holding the blank at said temperature in order to attain from 60 to 80 per cent of the maximum possible crystalline phase; gradually cooling the blank to room temperature; cutting out a product from said blank; heating said product to a temperature of 930*-970*C; holding said product at said temperature for 1.5 to 3 minutes per each millimeter of thickness of said product, and cooling the product at a rate of 85*-250* per minute.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1977-03-18 | 1977-09-17 | 1978-03-19 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1981-03-18 | 1981-09-17 | 1982-03-19 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1985-03-18 | 1985-09-17 | 1986-03-19 | $7700.00 | Window Closed / Lapsed |