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US3796543A Expired / Lapsed US ⏱️ 0.0 years remaining

Automatic analysis for phosphorous content

Assignee: ADMINISTRATOR ENVIRONMENTAL PR
•
Filing: 1972-02-07
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Granted: 1974-03-12
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Expires: 1992-02-07
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Abstract

Abstract A continuous automatic analytical system for measuring the phosphate content in aqueous fluids. First the phosphate containing sample is acidified, then reacted in an acid medium with molybdate to form molybdiphosphoric acid. Thereafter the molybdenum in the heterpoly acid is selectively reduced by hydrazine to a blue heterpoly complex. The quantity of blue color is directly proportional to the ortho-phosphate concentration in the sampling and a colorimeter reading thereof a measure of the phosphate content in the sample.

Inventors

  • 👤 L Kamphake

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 19:57
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/75; G01N21/77; G01N21/78; G01N21/783; G01N31/00; G01N31/02; G01N31/22; Y; Y10; Y10T; Y10T436/00; Y10T436/16

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 43 words
The method of claim 1 wherein successive sample portions are spaced apart by flow of air introduced at pulsed intervals into the combined stream of acidified sample and molybdate, said hydrazine bEing introduced into the liquid pulses in timed pulses in synchronization therewith.
Claim 2
Dependent Claim 18 words
The method of claim 1 wherein the mineral acid is sulfuric acid, and the hydrazine is hydrazine sulfate.
Claim 3
Dependent Claim 19 words
The method of claim 1 wherein the sample fluid being tested comprises the effluent from a waste sewage plant.

References Cited (Backward Citations)

US3479142A Cited
US3547586A Cited
US3572994A Cited
US3690833A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-03-11 1977-09-10 1978-03-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-03-11 1981-09-10 1982-03-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-03-11 1985-09-10 1986-03-12 $7700.00 Window Closed / Lapsed

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