← Back to Patent Explorer
US3771958A Expired / Lapsed US ⏱️ 0.0 years remaining

Gaseous diffusion paper deacidification

Assignee: Research Corp
•
Filing: 1971-12-30
•
Granted: 1973-11-13
•
Expires: 1991-12-30
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract Paper, for example having a pH of about 5.0 or lower, is rendered resistant to the deterioration that is promoted by acidic conditions in paper by impregnating the paper, for example in the form of a book, with gaseous morpholine.

Inventors

  • 👤 J Kusterer
  • 👤 R Sproull

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 10:26
CPC Classifications
D; D21; D21H; D21H17/00; D21H17/03; D21H17/05; D21H17/07; A; A61; A61L; A61L2/00; A61L2/16; A61L2/20; D21H25/00; D21H25/18

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 15 words
The process of claim 1 wherein the paper is in the form of a book.
Claim 2
Dependent Claim 25 words
The process of claim 1 wherein the morpholine accounts for about 90 to 100 volume percent of the atmosphere surrounding the paper during the impregnation.
Claim 3
Dependent Claim 15 words
The process of claim 3 wherein the paper is in the form of a book.
Claim 4
Dependent Claim 82 words
The process of claim 1 wherein the amount of morpholine impregnated into the paper is sufficient to provide the paper with a pH (measured after the paper has been allowed to stand at room temperature and atmospheric pressure for 24 hours) of at least about 7.6, as determined by soaking one gram of one-eighth inch squares of the paper for one hour in 70 ml. of distilled, deionized water at room temperature and then measuring the pH of the resultant aqueous solution.
Claim 5
Dependent Claim 15 words
The process of claim 5 wherein the paper is in the form of a book.
Claim 6
Dependent Claim 19 words
The process of claim 5 wherein the paper prior to treatment has a pH of about 5.0 or lower.
Claim 7
Dependent Claim 15 words
The process of claim 7 wherein the paper is in the form of a book.
Claim 8
Dependent Claim 124 words
A process of treating a book made of paper having a pH of about 5.0 or lower so as to render the paper resistant to the deterioration that is promoted by acidic conditions, which process comprises impregnating the book with a gaseous atmosphere consisting essentially of morpholine, the said morpholine being present in at least about one-third the volume of said gaseous atmosphere, at about 25* to 75*C. in an amount sufficient to raise the pH of the paper to at least about 8.5, said pH values being as determined by soaking one gram of one-eighth inch squares of the paper for one hour in 70 ml. of distilled, deionized water at room temperature and then measuring the pH of the resultant aqueous solution.
Claim 9
Dependent Claim 25 words
The process of claim 9 wherein the morpholine accounts for about 90 to 100 volume percent of the atmosphere surrounding the book during the impregnation.

References Cited (Backward Citations)

US2185954A Cited
US3135627A Cited
US3472611A Cited
US3419498A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-11-12 1977-05-14 1977-11-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-11-12 1981-05-14 1981-11-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-11-12 1985-05-14 1985-11-13 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag