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US3767378A Expired / Lapsed US ⏱️ 0.0 years remaining

Production of rutile and iron from ilmenite

Assignee: United States Department of the Interior
•
Filing: 1972-01-05
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Granted: 1973-10-23
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Expires: 1992-01-05
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Abstract

Abstract Ilmenite is treated with a reducing agent to selectively reduce iron oxide to metallic iron. The product is then treated with carbon monoxide in the presence of ammonium polysulfide solution to form iron carbonyl, which is removed by volatilization leaving rutile. The iron carbonyl is then decomposed to produce metallic iron.

Inventors

  • 👤 A Cochran
  • 👤 A Starliper

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 23:17
CPC Classifications
C; C21; C21B; C21B13/00; C21B13/006; C01; C01G; C01G49/00; C01G49/16; C22; C22B; C22B34/00; C22B34/10; C22B34/12; C22B34/1204; Y; Y02; Y02P; Y02P10/00; Y02P10/10; Y02P10/134

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 23 words
The method of claim 1 in which the reduction is preceded by an oxidation step to convert any ferrous iron to ferric iron.
Claim 2
Dependent Claim 13 words
The method of claim 1 in which the reduction is accomplished with hydrogen.
Claim 3
Dependent Claim 13 words
The method of claim 1 in which the reduction is accomplished with coke.
Claim 4
Dependent Claim 19 words
The method of claim 1 in which the carbonyl is decomposed at a temperature of about 280* to 350*C.

References Cited (Backward Citations)

US1480212A Cited
US1789813A Cited
US1852541A Cited
US2757077A Cited
US2811434A Cited
US3079235A Cited
US3250697A Cited
US3376129A Cited
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US3460913A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-10-22 1977-04-23 1977-10-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-10-22 1981-04-23 1981-10-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-10-22 1985-04-23 1985-10-23 $7700.00 Window Closed / Lapsed

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