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US3765837A Expired / Lapsed US ⏱️ 0.0 years remaining

Flame retardant finish for polyester/cotton blends

Assignee: Burlington Industries Inc
•
Filing: 1971-09-03
•
Granted: 1973-10-16
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Expires: 1991-09-03
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Abstract

Abstract A process for decreasing the flammability of textiles comprising a cellulosic fiber component and preferably a nitrogen-free thermoplastic fiber component which comprises treating the cellulosic fiber component with a condensate or a physical admixture of an allylurea and a phosphine/formaldehyde condensate such as a tetrakis (hydroxymethyl)-phosphonium salt to introduce allyl groups into the cellulosic component, and subsequently halogenating, preferably brominating, the allyl groups thus introduced.

Inventors

  • 👤 B Aycock
  • 👤 G Tesoro

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 04:52
CPC Classifications
D; D06; D06M; D06M15/00; D06M15/19; D06M15/37; D06M15/39; D06M15/423; D06M15/43; D06M15/431; D06M13/00; D06M13/322; D06M13/402; D06M13/432; Y; Y10; Y10S; Y10S8/00; Y10S8/04

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 17 words
The process of claim 1 wherein the allylurea and phosphine/formaldehyde condensate are used together in physical admixture.
Claim 2
Dependent Claim 17 words
The process of claim 1 wherein the allylurea and phosphine/formaldehyde condensate are used together in precondensate form.
Claim 3
Dependent Claim 11 words
The process of claim 1 wherein the allylurea is allylurea itself.
Claim 4
Dependent Claim 17 words
The process of claim 1 wherein the allylurea is N,N-diallylurea, N,N''-diallylurea, triallylurea, N-allyl-N-methylurea, N-allyl-N''-methylurea, N-allyl-N''-etHylurea or N-allylethyleneurea.
Claim 5
Dependent Claim 12 words
The process of claim 1 wherein the phosphine/formaldehyde condensate is tetrakis(hydroxymethyl)phosphonium chloride.
Claim 6
Dependent Claim 19 words
The process of claim 1 wherein the textile is treated with a 1:1 precondensate of allylurea and tetrakis(hydroxymethyl)phosphonium chloride.
Claim 7
Dependent Claim 12 words
The process of claim 1 wherein the textile comprises a cellulosic/polyester blend.
Claim 8
Dependent Claim 20 words
The process of claim 1 wherein the textile comprises a blend of cellulosic fiber and a different nitrogen-free thermoplastic fiber.
Claim 9
Dependent Claim 10 words
The process of claim 1 wherein the halogenating is brominating.
Claim 10
Dependent Claim 33 words
The process of claim 1 wherein the textile is treated with the allylurea and phosphine/formaldehyde condensate by padding with an aqueous solution containing the allylurea and the condensate, followed by drying and curing.
Claim 11
Dependent Claim 15 words
The process of claim 11 wherein curing is carried out in the presence of ammonia.
Claim 12
Dependent Claim 12 words
The process of claim 11 wherein the textile is washed after curing.
Claim 13
Dependent Claim 17 words
The process of claim 11 wherein the aqueous solution has a pH of at least about 5.
Claim 14
Dependent Claim 9 words
The textile obtained by the process of claim 1.

References Cited (Backward Citations)

US2983623A Cited
US3374292A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-10-15 1977-04-16 1977-10-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-10-15 1981-04-16 1981-10-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-10-15 1985-04-16 1985-10-16 $7700.00 Window Closed / Lapsed

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