US3765655A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Mixing process
Assignee: Monsanto Co
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Filing: 1971-08-16
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Granted: 1973-10-16
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Expires: 1991-08-16
Abstract
Abstract A mixing process in which a liquid is simultaneously subjected to a combination of vertical displacement, horizontal recirculation, and horizontal roll. The process is especially well adapted for use with highly viscous fluids and can be practiced with surprisingly low power requirements. A substantially homogeneous liquid system can be produced and maintained in a relatively short mixing time.
Inventors
- 👤 G Latinen
- 👤 M Latinen
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 22:41
CPC Classifications
C; C08; C08F; C08F212/00; C08F212/02; C08F212/04; C08F212/06; C08F212/08; C08F212/10; C08F20/00; C08F20/02; C08F20/42; B; B01; B01J; B01J2219/00; B01J2219/18; B01J2219/182
Claims Analysis
Total Claims: 21
Claim 1
Independent Claim
466 words
In an improved process for agitating a liquid and adapted to achieve and maintain substantial homogeneity and uniformity therein, the step which comprises subjecting a liquid which, from about 10 to 90 per cent by volume, fills a generally enclosed, horizontally elongated treating zone simultaneously to a combination of: A. cyclical vertical displacement in said zone such that at a cycle rate in the range from about one-half to 60 times per minute, 1. first, said liquid is subjected to a vertical lifting force greater than that exerted downwardly thereon by gravity, and at least sufficient to move vertically at least about 10 per cent of the total volume of said liquid from a gravitationally lower region to a gravitationally higher region in said zone, and 2. secondly, such so displaced liquid is subjected to a gravitational falling force by effective removal of said lifting force therefrom, the total gravitational falling force applied thereon being at least sufficient to return substantially all of such so displaced liquid to said gravitationally lower region before said cycle is repeated on such so displaced liquid, B. rolling action in a generally peripherally located and generally horizontally extending region in said zone, said region extending circumferentially about the entire internal periphery of said zone, said region being continuously moving in a direction which is generally normal to the horizontal, said rolling action being produced by a similarly so moving band of pressure located adjacent to but following behind said region, said band of pressure exerting a force on said liquid in said region at least sufficient to cause movement of a portion of said liquid in said region along a roughly crosssectionally circular path normally away from the adjacent internal periphery of said zone adjacent to said band of pressure towards the interior of said zone a distance which is generally less than the maximum distance across said zone at a given peripheral position and then back towards said internal periphery forwardly of said band of pressure before moving towards said band of pressure, there being a shear rate between said internal periphery and said zone of pressure of at least about 5sec. 1, C. horizontal displacement in said zone in a longitudinal circulatory manner at a cycle rate such that the actual volume of said liquid moved from one end region of said treating zone to the opposite end region thereof and back within one minute is equivalent to from about one-tenth to 30 times the total volume of said liquid in said zone, such equivalent volume and the horizontal circulation rate for such liquid so moved, respectively, being approximately proportional to said cyclical vertical displacement cycle rate in any given instance, while continuously maintaining substantially the total volume of said liquid in said zone under laminar flow conditions.
Claim 2
Dependent Claim
466 words
In an improved process for agitating a liquid and adapted to achieve and maintain substantial homogeneity and uniformity therein, the step which comprises subjecting a liquid which, from about 10 to 90 per cent by volume, fills a generally enclosed, horizontally elongated treating zone simultaneously to a combination of: A. cyclical vertical displacement in said zone such that at a cycle rate in the range from about one-half to 60 times per minute, 1. first, said liquid is subjected to a vertical lifting force greater than that exerted downwardly thereon by gravity, and at least sufficient to move vertically at least about 10 per cent of the total volume of said liquid from a gravitationally lower region to a gravitationally higher region in said zone, and 2. secondly, such so displaced liquid is subjected to a gravitational falling force by effective removal of said lifting force therefrom, the total gravitational falling force applied thereon being at least sufficient to return substantially all of such so displaced liquid to said gravitationally lower region before said cycle is repeated on such so displaced liquid, B. rolling action in a generally peripherally located and generally horizontally extending region in said zone, said region extending circumferentially about the entire internal periphery of said zone, said region being continuously moving in a direction which is generally normal to the horizontal, said rolling action being produced by a similarly so moving band of pressure located adjacent to but following behind said region, said band of pressure exerting a force on said liquid in said region at least sufficient to cause movement of a portion of said liquid in said region along a roughly crosssectionally circular path normally away from the adjacent internal periphery of said zone adjacent to said band of pressure towards the interior of said zone a distance which is generally less than the maximum distance across said zone at a given peripheral position and then back towards said internal periphery forwardly of said band of pressure before moving towards said band of pressure, there being a shear rate between said internal periphery and said zone of pressure of at least about 5sec. 1, C. horizontal displacement in said zone in a longitudinal circulatory manner at a cycle rate such that the actual volume of said liquid moved from one end region of said treating zone to the opposite end region thereof and back within one minute is equivalent to from about one-tenth to 30 times the total volume of said liquid in said zone, such equivalent volume and the horizontal circulation rate for such liquid so moved, respectively, being approximately proportional to said cyclical vertical displacement cycle rate in any given instance, while continuously maintaining substantially the total volume of said liquid in said zone under laminar flow conditions.
Claim 3
Dependent Claim
339 words
secondly, such so displaced liquid is subjected to a gravitational falling force by effective removal of said lifting force therefrom, the total gravitational falling force applied thereon being at least sufficient to return substantially all of such so displaced liquid to said gravitationally lower region before said cycle is repeated on such so displaced liquid, B. rolling action in a generally peripherally located and generally horizontally extending region in said zone, said region extending circumferentially about the entire internal periphery of said zone, said region being continuously moving in a direction which is generally normal to the horizontal, said rolling action being produced by a similarly so moving band of pressure located adjacent to but following behind said region, said band of pressure exerting a force on said liquid in said region at least sufficient to cause movement of a portion of said liquid in said region along a roughly cross-sectionally circular path normally away from the adjacent internal periphery of said zone adjacent to said band of pressure towards the interior of said zone a distance which is generally less than the maximum distance across said zone at a given peripheral position and then back towards said internal periphery forwardly of said band of pressure before moving towards said band of pressure, there being a shear rate between said internal periphery and said zone of pressure of at least about 5sec. 1, C. horizontal displacement in said zone in a longitudinal circulatory manner at a cycle rate such that the actual volume of said liquid moved from one end region of said treating zone to the opposite end region thereof and back within one minute is equivalent to from about one-tenth to 30 times the total volume of said liquid in said zone, such equivalent volume and the horizontal circulation rate for such liquid so moved, respectively, being approximately proportional to said cyclical vertical displacement cycle rate in any given instance, while continuously maintaining substantially the total volume of said liquid in said zone under laminar flow conditions.
Claim 4
Dependent Claim
339 words
secondly, such so displaced liquid is subjected to a gravitational falling force by effective removal of said lifting force therefrom, the total gravitational falling force applied thereon being at least sufficient to return substantially all of such so displaced liquid to said gravitationally lower region before said cycle is repeated on such so displaced liquid, B. rolling action in a generally peripherally located and generally horizontally extending region in said zone, said region extending circumferentially about the entire internal periphery of said zone, said region being continuously moving in a direction which is generally normal to the horizontal, said rolling action being produced by a similarly so moving band of pressure located adjacent to but following behind said region, said band of pressure exerting a force on said liquid in said region at least sufficient to cause movement of a portion of said liquid in said region along a roughly cross-sectionally circular path normally away from the adjacent internal periphery of said zone adjacent to said band of pressure towards the interior of said zone a distance which is generally less than the maximum distance across said zone at a given peripheral position and then back towards said internal periphery forwardly of said band of pressure before moving towards said band of pressure, there being a shear rate between said internal periphery and said zone of pressure of at least about 5sec. 1, C. horizontal displacement in said zone in a longitudinal circulatory manner at a cycle rate such that the actual volume of said liquid moved from one end region of said treating zone to the opposite end region thereof and back within one minute is equivalent to from about one-tenth to 30 times the total volume of said liquid in said zone, such equivalent volume and the horizontal circulation rate for such liquid so moved, respectively, being approximately proportional to said cyclical vertical displacement cycle rate in any given instance, while continuously maintaining substantially the total volume of said liquid in said zone under laminar flow conditions.
Claim 5
Dependent Claim
22 words
The process of claim 1 wherein said cyclical vertical displacement in combination with said rolling action produces folding action in said liquid.
Claim 6
Dependent Claim
45 words
radially over said axial blade length uninterruptedly from said longitudinal axis to a location adjacent the perimeter of said zone, B. a second region which is axially adjacent said first region and adjacent an end of said zone, said second region having discontinuities formed therethrough.
Claim 7
Dependent Claim
45 words
radially over said axial blade length uninterruptedly from said longitudinal axis to a location adjacent the perimeter of said zone, B. a second region which is axially adjacent said first region and adjacent an end of said zone, said second region having discontinuities formed therethrough.
Claim 8
Dependent Claim
49 words
The process of claim 1 practiced continuously by both continuously introducing a material to be agitated into said zone with a liquid so filling said zone being in said zone and continuously withdrawing so agitated liquid product derived from mixing said material and said liquid together from said zone.
Claim 9
Dependent Claim
53 words
The process of claim 3 wherein the liquid so filling said zone has a volume average viscosity of from about 10,000 to 100, 000 centipoises and wherein said material so introduced is a liquid miscible with said liquid so filling said zone and having a viscosity of from about one-half to 100 centipoises.
Claim 10
Dependent Claim
25 words
The process of claim 1 practiced batch-wise by first so filling said zone with a liquid to be agitated and then so agitating such liquid.
Claim 11
Dependent Claim
20 words
The process of claim 1 wherein said zone is cross-sectionally circular and has a longitudinal axis which extends generally horizontally.
Claim 12
Dependent Claim
16 words
The process of claim 4 wherein paddle blades rotate in said zone about said longitudinal axis.
Claim 13
Dependent Claim
23 words
The process of claim 6 wherein each of said paddle blades is further characterized by having: A. a first region which both extends:
Claim 14
Dependent Claim
15 words
The process of claim 7 wherein the number of said blades is at least two.
Claim 15
Dependent Claim
19 words
The process of claim 1 wherein said liquid has volume average viscosity of from about one-half to 500,000 centipoises.
Claim 16
Dependent Claim
19 words
The process of claim 9 wherein said liquid has a volume average viscosity of at least about 1,000 centipoises.
Claim 17
Dependent Claim
20 words
The process of claim 1 wherein said liquid has a volume average viscosity of from about 10,000 to 100,000 centipoises.
Claim 18
Dependent Claim
23 words
The process of claim 1 wherein the cycle rate for said cyclical vertical displacement ranges from about 1 to 25 times per minute.
Claim 19
Dependent Claim
19 words
The process of claim 12 wherein said bulk average shear rate ranges from about 3 to 100 sec. 1.
Claim 20
Dependent Claim
25 words
The process of claim 12 wherein said horizontal displacement cycle rate is equivalent to from about one-third to 10 times the total volume per minute.
Claim 21
Dependent Claim
87 words
The process of claim 1 wherein: A. said liquid has a voluMe average viscosity of from about 10, 000 to 100,000 centipoises and fills said zone from about 30 to 75 per cent by volume, B. the cycle rate for said cyclical vertical displacement ranges from about 1 to 25 times per minute, C. the bulk average shear rate ranges from about 3 to 100 sec 1, and D. the horizontal displacement cycle rate is equivalent to about one-third to 10 times the total volume per minute.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1976-10-15 | 1977-04-16 | 1977-10-16 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1980-10-15 | 1981-04-16 | 1981-10-16 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1984-10-15 | 1985-04-16 | 1985-10-16 | $7700.00 | Window Closed / Lapsed |