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US3764540A Expired / Lapsed US ⏱️ 0.0 years remaining

Magnetofluids and their manufacture

Assignee: United States Department of the Interior
•
Filing: 1971-05-28
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Granted: 1973-10-09
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Expires: 1991-05-28
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Abstract

Abstract Magnetofluids, comprising a stable, colloidal suspension of magnetite and elemental iron, are produced by comminuting a nonmagnetic or antimagnetic precursor compound to colloidal size, dispersing the precursor in a carrier fluid and thereafter converting the precursor to ferromagnetic forms while in stable suspension.

Inventors

  • 👤 S Khalafalla
  • 👤 G Reimers

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 02:01
CPC Classifications
H; H01; H01F; H01F1/00; H01F1/44; H01F1/445

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 35 words
The process of claim 1 wherein said dispersing step comprises agitation of the particulate suboxide and liquid mixture together with an aliphatic monocarboxylic acid dispersing agent having from about eight to about 24 carbon atoms.
Claim 2
Dependent Claim 22 words
The process of claim 1 wherein the suboxide of iron is wustite having a composition in the range of Fe0.95O to Fe0.85O.
Claim 3
Dependent Claim 23 words
The process of claim 3 wherein the wustite is converted to ferromagnetic forms by heating for a time greater than about one-half hour.
Claim 4
Dependent Claim 26 words
The process of claim 4 where the wustite is produced from finely divided ferric oxide by reduction at temperatures within the range of 570* to 800*C.
Claim 5
Dependent Claim 41 words
The process of claim 5 wherein the wustite is recovered from the reduction step in pyrophoric form and is protected from reoxidation by coating it with an aliphatic monocarboxylic acid dispersing agent having from about eight to about 24 carbon atoms.
Claim 6
Dependent Claim 18 words
The process of claim 6 wherein the dispersing agent-coated wustite is comminuted by wet grinding in the liquid.
Claim 7
Dependent Claim 19 words
The process of claim 7 wherein the liquid is a hydrocarbon and wherein the dispersing agent is oleic acid.
Claim 8
Dependent Claim 10 words
The process of claim 8 wherein the hydrocarbon is kerosene.

References Cited (Backward Citations)

US3531413A Cited
US3526598A Cited
US3635819A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-10-08 1977-04-09 1977-10-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-10-08 1981-04-09 1981-10-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-10-08 1985-04-09 1985-10-09 $7700.00 Window Closed / Lapsed

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