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US3755170A
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Preparation of highly basic alkylphenates and sulfurized alkyphenates
Assignee: ConocoPhillips Co
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Filing: 1971-05-17
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Granted: 1973-08-28
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Expires: 1991-05-17
Abstract
Abstract Process for preparing highly basic alkaline earth metal alkylphenates or sulfurized alkylphenates wherein the process comprises: A. FORMING AN ADMIXTURE OF ALKYLPHENOL OR SULFURIZED ALKYLPHENOL, NONVOLATILE DILUENT OIL, VOLATILE PROCESS SOLVENT AND WATER, B. ADDING AN OVERBASING AMOUNT OF ALKALINE EARTH METAL IN A GLYCOL ETHER AT A TEMPERATURE FROM ABOUT 20* TO ABOUT 55* C., c. adding a neutralizing amount of alkaline earth metal in a glycol ether at a temperature of about 55* to about 100* C., and D. REMOVING THE VOLATILE MATERIALS BY HEATING. The products are useful as additive agents for lubricating oils.
Inventors
- 👤 L Rogers
- 👤 M Hunt
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-06 11:26
CPC Classifications
C; C10; C10M; C10M159/00; C10M159/12; C10M159/20; C10M159/22; C09; C09K; C09K8/00; C09K8/50; C09K8/502; C10M2203/00; C10M2203/06; C10M2205/00; C10M2205/02; C10M2205/024; C10M2205/028; C10M2207/00; C10M2207/02; C10M2207/023; C10M2207/028; C10M2207/28; C10M2207/282; C10M2207/34; C10M2207/40; C10M2207/404; C10M2209/00; C10M2209/10; C10M2209/103; C10M2209/105; C10M2219/00; C10M2219/02; C10M2219/04; C10M2219/046; C10M2219/08; C10M2219/082; C10M2219/084; C10M2223/00; C10M2223/02; C10M2223/04; C10M2223/042; C10N; C10N2070/00; C10N2070/02
Claims Analysis
Total Claims: 31
Claim 1
Independent Claim
24 words
The process of claim 1 wherein the non-volatile diluent oil is selected from the group consisting of mineral lubricating oils and synthetic lubricating oils.
Claim 2
Dependent Claim
30 words
The process of claim 2 wherein the process solvent is selected from the group consisting of aromatic hydrocarbons, aliphatic hydrocarbons, primary aliphatic C1-C6 alcohols and C3 to C8 glycol ethers.
Claim 3
Dependent Claim
33 words
The process of claim 3 wherein the glycol ether used to prepare the glycol ether solution of magnesium, calcium or barium is monomethyl ether of ethylene glycol or monoethyl ether of ethylene glycol.
Claim 4
Dependent Claim
51 words
The process of claim 4 wherein the amounts of materials in step (a) are: parts by weight (i) alkylphenol or sulfurized alkylphenol about 6 to about 70 (ii) nonvolatile diluent about 5 to about 90 (iii) volatile process solvent about 1 to about 100 (iv) water about 0.3 to about 10
Claim 5
Dependent Claim
12 words
The process of claim 5 wherein the metal is magnesium or calcium.
Claim 6
Dependent Claim
23 words
The process of claim 6 wherein the process solvent is a mixture of an aliphatic hydrocarbon and a C3 to C8 glycol ether.
Claim 7
Dependent Claim
17 words
The process of claim 7 wherein the process solvent is a mixture of hexane and methoxy ethanol.
Claim 8
Dependent Claim
15 words
The process of claim 8 wherein the nonvolatile diluent oil is a mineral lubricating oil.
Claim 9
Dependent Claim
23 words
The process of claim 6 wherein the process solvent is a mixture of an aromatic hydrocarbon and a C3 to C8 glycol ether.
Claim 10
Dependent Claim
17 words
The process of claim 10 wherein the process solvent is a mixture of benzene and methoxy ethanol.
Claim 11
Dependent Claim
15 words
The process of claim 11 wherein the nonvolatile diluent oil is a mineral lubricating oil.
Claim 12
Dependent Claim
32 words
The process of claim 1 wherein the admixture of step (a) contains additionally from about 0.1 to about 50 parts of oil-soluble sulfonic acid per 100 parts of alkylphenol or sulfurized alkylphenol.
Claim 13
Dependent Claim
32 words
The process of claim 5 wherein the admixture of step (a) contains additionally from about 0.1 to about 50 parts of oil-soluble sulfonic acid per 100 parts of alkylphenol or sulfurized alkylphenol.
Claim 14
Dependent Claim
32 words
The process of claim 9 wherein the admixture of step (a) contains additionally from about 0.1 to about 50 parts of oil-soluble sulfonic acid per 100 parts of alkylphenol or sulfurized alkylphenol.
Claim 15
Dependent Claim
32 words
The process of claim 12 wherein the admixture of step (a) contains additionally from about 0.1 to about 50 parts of oil-soluble sulfonic acid per 100 parts of alkylphenol or sulfurized alkylphenol.
Claim 16
Dependent Claim
47 words
A process for preparing a highly basic magnesium salt or alkylphenols and sulfurized alkylphenols wherein the process comprises: a. forming an admixture of i. about 4 to about 80 parts by weight of an alkylphenol or a sulfurized alkylphenol wherein the alkylphenol is represented by the formula
Claim 17
Dependent Claim
24 words
The process of claim 17 wherein the nonvolatile diluent oil is selected from the group consisting of mineral lubricating oils and synthetic lubricating oils.
Claim 18
Dependent Claim
30 words
The process of claim 18 wherein the process solvent is selected from the group consisting of aromatic hydrocarbons, aliphatic hydrocarbons, primary aliphatic C1-C6 alcohols, and C3 to C8 glycol ethers.
Claim 19
Dependent Claim
15 words
The process of claim 19 wherein the glycol ether is monomethyl ether of ethylene glycol.
Claim 20
Dependent Claim
52 words
The process of claim 17 wherein the amounts of materials in step (a) are parts by weight (i) alkylphenol or sulfurized alkylphenol about 9 to about 70 (ii) nonvolatile diluent oil about 20 to about 90 (iii) volatile process solvent about 2 to about 80 (iv) water about 0.3 to about 10
Claim 21
Dependent Claim
24 words
The process of claim 21 wherein the nonvolatile diluent oil is selected from the group consisting of mineral lubricating oils and synthetic lubricating oils.
Claim 22
Dependent Claim
30 words
The process of claim 22 wherein the process solvent is selected from the group consisting of aromatic hydrocarbons, aliphatic hydrocarbons, primary aliphatic C1-C6 alcohols and C3 to C8 glycol ethers.
Claim 23
Dependent Claim
23 words
The process of claim 23 wherein the process solvent is a mixture of an aliphatic hydrocarbon and a C3 to C8 glycol ether.
Claim 24
Dependent Claim
17 words
The process of claim 24 wherein the process solvent is a mixture of hexane and methoxy ethanol.
Claim 25
Dependent Claim
15 words
The process of claim 25 wherein the nonvolatile diluent oil is a mineral lubricating oil.
Claim 26
Dependent Claim
23 words
The process of claim 23 wherein the process solvent is a mixture of an aromatic hydrocarbon and a C3 to C8 glycol ether.
Claim 27
Dependent Claim
17 words
The process of claim 27 wherein the process solvent is a mixture of benzene and methoxy ethanol.
Claim 28
Dependent Claim
15 words
The process of claim 28 wherein the nonvolatile diluent oil is a mineral lubricating oil.
Claim 29
Dependent Claim
32 words
The process of claim 17 wherein the admixture of step (a) contains additionally from about 0.1 to about 50 parts of oil-soluble sulfonic acid per 100 parts of alkylphenol or sulfurized alkylphenol.
Claim 30
Dependent Claim
32 words
The process of claim 26 wherein the admixture of step (a) contains additionally from about 0.1 to about 50 parts of oil-soluble sulfonic acid per 100 parts of alkylphenol or sulfurized alkylphenol.
Claim 31
Dependent Claim
32 words
The process of claim 29 wherein the admixture of step (a) contains additionally from about 0.1 to about 50 parts of oil-soluble sulfonic acid per 100 parts of alkylphenol or sulfurized alkylphenol.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1976-08-27 | 1977-02-26 | 1977-08-28 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1980-08-27 | 1981-02-26 | 1981-08-28 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1984-08-27 | 1985-02-26 | 1985-08-28 | $7700.00 | Window Closed / Lapsed |