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US3753757A Expired / Lapsed US ⏱️ 0.0 years remaining

Two step porous boiling surface formation

Assignee: Union Carbide Corp
•
Filing: 1970-05-15
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Granted: 1973-08-21
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Expires: 1990-05-15
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Abstract

Abstract A method of coating metal substrates with a porous metal layer, comprising the steps of: A. PROVIDING A METAL SUBSTRATE TO BE POROUS METAL COATED; B. APPLYING A LIQUID BINDER SOLUTION CONSISTING ESSENTIALLY OF AT LEAST ONE HIGH VOLATILITY SOLVENT COMPONENT AND AT LEAST ONE LOW VOLATILITY COMPONENT IN A LAYER FROM 0.002 TO 0.040 INCH THICK ONTO SAID METAL SUBSTRATE; C. APPLYING A 0.005 TO 0.050 INCH THICK LAYER OF METAL POWDER 30-500 MESH ONTO THE BINDER LAYER SO THAT THE BINDER LAYER WETS THE METAL POWDER COATING AND IS SATURATED THEREBY AND RETAINS SUBSTANTIALLY ALL OF SAID POWDER AGAINST SAID METAL SUBSTRATE; D. EVAPORATING SUBSTANTIALLY ALL OF THE HIGH VOLATILITY COMPONENT OF SAID LIQUID BINDER SOLUTION AT ABOUT AMBIENT TEMPERATURE; E. HEATING THE METAL POWDER COATED METAL SUBSTRATE OF (D) TO TEMPERATURE SUFFICIENT TO EVAPORATE SUBSTANTIALLY ALL OF THE BINDER LOW VOLATILITY COMPONENT; F. FURTHER HEATING THE METAL POWDER COATED METAL SUBSTRATE TO TEMPERATURE SUFFICIENT TO BOND THE METAL POWDER TO ITSELF AND TO THE METAL SUBSTRATE SO AS TO FORM A POROUS METAL LAYER HAVING INTERCONNECTED SURFACE AND SUBSURFACE CAVITIES; AND G. COOLING THE POROUS METAL LAYER BONDED METAL SUBSTRATE.

Inventors

  • 👤 A Rodgers
  • 👤 R Weiner

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 14:49
CPC Classifications
B; B22; B22F; B22F7/00; B22F7/002; F; F28; F28F; F28F13/00; F28F13/18; F28F13/185; F28F13/187

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 23 words
A method as described in claim 1 wherein the liquid binder solution consists of by weight 15-50 percent isobutylene polymer, 50-85 percent kerosene.
Claim 2
Dependent Claim 27 words
A method as described in claim 1 wherein the liquid binder solution consists of by weight 15-25 percent isobutylene polymer, 40-60 percent toluene, and 25-40 percent kerosene.
Claim 3
Dependent Claim 21 words
A method as described in claim 1 wherein one low volatility and two high volatility components comprise the liquid binder solution.
Claim 4
Dependent Claim 20 words
A method as described in claim 1 wherein the metal powder layer is accomplished in two separate metal powder applications.
Claim 5
Dependent Claim 22 words
A method as described in claim 1 for coating corrugated metal tubes wherein the metal powder application is accomplished by electrostatic spraying.
Claim 6
Dependent Claim 67 words
A method according to claim 1 wherein said metal substrate to be porous metal coated is horizontal, the liquid binder solution consists of 16 percent by weight isobutylene polymer and 84 percent by weight kerosene and is applied in a thickness of 0.015 inch, and 100-200 mesh metal powder is applied onto the binder layer in quantity such that the final thickness of powder is 0.020 inch.
Claim 7
Dependent Claim 67 words
A method according to claim 1 wherein said metal substrate to be porous metal coated is horizontal, the liquid binder solution consists of 15 percent by weight isobutylene polymer and 85 percent by weight kerosene and is applied in a thickness of 0.010 inch, and 200-400 mesh metal powder is applied onto the binder layer in quantity such that the final thickness of powder is 0.015 inch.
Claim 8
Dependent Claim 70 words
A method according to claim 1 wherein said metal substrate to be porous metal coated is an internal tube surface, the liquid binder solution consists of 36 percent by weight isobutylene polymer and 64 percent by weight toluene and is applied in a thickness of 0.017 inch, and 100-270 mesh metal powder is applied onto the binder layer in quantity such that the final thickness of powder is 0.023 inch.
Claim 9
Dependent Claim 70 words
A method according to claim 1 wherein said metal substrate to be porous metal coated is an internal tube surface, the liquid binder solution consists of 34 percent by weight isobutylene polymer and 66 percent by weight toluene and is applied in a thickness of 0.012 inch, and 270-400 mesh metal powder is applied onto the binder layer in quanTity such that the final thickness of powder is 0.019 inch.
Claim 10
Dependent Claim 62 words
A method according to claim 1 wherein said metal substrate is vertical, the liquid binder solution consists of 18 percent by weight isobutylene polymer and 82 percent by weight kerosene and is applied in a thickness of 0.013 inch, and 100-270 mesh metal powder is applied onto the binder layer in quantity such that the final thickness of powder is 0.020 inch.
Claim 11
Dependent Claim 62 words
A method according to claim 1 wherein said metal substrate is vertical, the liquid binder solution consists of 17 percent by weight isobutylene polymer and 83 percent by weight kerosene and is applied in a thickness of 0.008 inch, and 270-400 mesh metal powder is applied onto the binder layer in quantity such that the final thickness of powder is 0.015 inch.

References Cited (Backward Citations)

US2289614A Cited
US2461878A Cited
US3024128A Cited
US3384154A Cited
US3096567A Cited
US3513012A Cited
US3378365A Cited
US3389006A Cited
US3410714A Cited
US3475161A Cited
US3565662A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-08-20 1977-02-19 1977-08-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-08-20 1981-02-19 1981-08-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-08-20 1985-02-19 1985-08-21 $7700.00 Window Closed / Lapsed

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