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US3753651A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and apparatus for surface sterilization

Assignee: Wave Energy Systems Inc
•
Filing: 1970-08-27
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Granted: 1973-08-21
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Expires: 1990-08-27
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Abstract

Abstract A method and apparatus for the rapid sterilization of a contaminated surface which involves the use of microwave energy fields combined with a humid atmosphere having a relative humidity of at least 50 percent. The material to be sterilized is placed into a self-sealed container at least partially transparent to microwaves. Said container is then introduced into an oven cavity. The moist atmosphere is confined inside the container walls. Through both thermal and non-thermal effects, surface decontamination by electromagnetic radiation takes place in a matter of minutes. The apparatus of the invention eliminates potential oven walls contamination and is entirely safe from the radiation view point. It can be operated by unskilled personnel.

Inventors

  • 👤 R Boucher

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 23:06
CPC Classifications
A; A61; A61L; A61L2/00; A61L2/02; A61L2/08; A61L2/12

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 32 words
The invention of claim 1, wherein the microwave energy field has a frequency of from about 100 MHz to about 300,000 MHz, and an average electromagnetic density greater than about .01 watt/cm3.
Claim 2
Dependent Claim 14 words
The invention of claim 1 wherein the processing time is greater than 2 seconds.
Claim 3
Dependent Claim 14 words
The invention of claim 3 wherein the electromagnetic field is a continuous wave emission.
Claim 4
Dependent Claim 30 words
The invention of claim 3 wherein the electromagnetic field is a pulsed wave emission having a repetition rate of the order of between one per nanosecond and one per minute.
Claim 5
Dependent Claim 21 words
The invention of claim 1, including the step of introducing a chemical having bactericidal or sporicidal effects into said sealed container.
Claim 6
Dependent Claim 17 words
The invention of claim 6, including the step of introducing a gas sterilant into said sealed container.
Claim 7
Dependent Claim 19 words
The invention of claim 6, including the step of introducing a sterilant vapor or aerosol into said sealed container.
Claim 8
Dependent Claim 37 words
The invention of claim 6, wherein said chemical is a liquid and including the step of utilizing said microwave energy to evaporate said cehmical and thus produce said at least 50% relative humidity inside said sealed container.
Claim 9
Dependent Claim 34 words
The invention of claim 6, wherein the chemical sterilant is an organic compound selected from the group consisting of ethylene oxide, propylene oxide, methylbromide, chloropicrin, epichlorohydrin, ethylene immine, glutaraldehyde, formaldehyde, glycidaldehyde, and peracetic acid.
Claim 10
Dependent Claim 178 words
Apparatus for surface decontamination of contaminated articles comprising: a microwave oven having top, bottom and opposite side walls defining a processing cavity therein; means connected with said microwave oven for generating a microwave electromagnetic energy field inside said processing cavity; a reusable gas-tight container for said articles and made of a material impermeable to moisture and at least partially transparent to microwave energy, said container having a readily removable top and a bottom and means for sealing said top to said bottom with said articles sealed inside said container, a receptacle for said separate source of moisture located within said container; access means in said microwave oven for introducing into and removing said container from said processing cavity, and means in said container other than said articles for producing at least 50 percent relative humidity inside said container during irradiation of said articles with said microwave energy; said at least 50% relative humidity and said microwave energy decontaminating said articles in a shorter time and at a lower temperature than heretofore obtained and without contaminating said oven walls.
Claim 11
Dependent Claim 106 words
The invention of claim 11, wherein the means for generating microwave energy includes a source of microwave energy, a wave guide connected between said source and said cavity, a means in said cavity in the path of the microwave energy entering said cavity from said wave guide to spread said microwave energy throughout said cavity, said oven walls made of metallic material to reflect microwave energy, and said access means comprising a door in one oven wall constructed to seal the processing cavity and keep radiation through said door to less than one milliwatt per square centimeter at a distance of two inches from said door.
Claim 12
Dependent Claim 15 words
The invention of claim 12, wherein said generating means comprises a source of continuous waves.
Claim 13
Dependent Claim 15 words
The invention of claim 12, wherein said generating means comprises a source of pulse waves.
Claim 14
Dependent Claim 217 words
Apparatus for surface decontamination of instruments or other materials comprising a housing, a cavity within said housing, a container in said cavity for said articles or other materials and made of a material at least partially transparent to microwave energy, means for sealing said container with said articles or other material therein, means connected with said cavity for generating a microwave electromagnetic energy field inside said cavity and said container, means in said container for producing at least 50 percent relative humidity inside said container during irradiation, said container having means associated therewith for selectively establishing communication between the interior of the container and the exterior of the container for introducing a chemical having bactericidal, or sporicidal characteristics into said container, means in said cavity for spreading the microwave energy field in all directions throughout the entire cavity and container, access door means in said housing for introducing and removing said container into and from said cavity, means to automatically expose the contaminated instruments or other materials to microwave energy for a period at least longer than two seconds and means to maintain the level of radiation through said housing to outside thereof during the radiation of said articles and other materials below 1 milliwatt per square centimeter at a distance of 2 inches from said housing.
Claim 15
Dependent Claim 34 words
The invention of claim 15, wherein the chemical sterilant is an organic compound selected from the group consisting of ethylene oxide, propylene oxide, methylbromide, chloropicrin, epichlorohydrin, ethylene immine, glutaraldehyde, formaldehyde, glycidaldehyde, and peracetic acid.

References Cited (Backward Citations)

US2714070A Cited
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US3215539A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-08-20 1977-02-19 1977-08-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-08-20 1981-02-19 1981-08-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-08-20 1985-02-19 1985-08-21 $7700.00 Window Closed / Lapsed

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