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US3753647A Expired / Lapsed US ⏱️ 0.0 years remaining

Liquid oxygen compatible dye penetrant method for metal defect inspection

Assignee: Boeing North American Inc
•
Filing: 1970-03-05
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Granted: 1973-08-21
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Expires: 1990-03-05
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Abstract

Abstract A liquid fluorescent dye penetrant containing a high volume concentration of a liquid halocarbon is taught as a very sensitive microdefect detector on metal surfaces. The dye penetrant is insensitive to chemical reaction or detonation with liquid oxygen in a standard impact safety test. The liquid dye penetrant safety factor is important in inspection of metal components later fabricated into rocket motor systems, which use liquid oxygen (LOX) in propellant systems, or the like powerful liquid oxidizers.

Inventors

  • 👤 O Molina

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 15:08
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/84; G01N21/88; G01N21/91; Y; Y10; Y10S; Y10S8/00; Y10S8/907

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 28 words
The sensitive liquid dye penetrant of claim 1 and further including a nonionic wetting and spreading agent constituting not more than five volume percent of said dye penetrant.
Claim 2
Dependent Claim 15 words
The sensitive liquid dye penetrant of claim 1, wherein said ketone is isobutyl heptyl ketone.
Claim 3
Dependent Claim 31 words
The sensitive liquid dye penetrant of claim 1, wherein said halocarbon solvent is selected from the group consisting of: 1-bromo-1-difluoro-2-bromo-2-difluoro ethane, 1-dichloro-1-fluoro-2 ethane, 1-dichloro-1-fluoro-2-dichloro-2-fluoro ethane, 1,1,1 trichloro ethane, trichloroethylene, and tetrachloroethylene.
Claim 4
Dependent Claim 21 words
The sensitive liquid dye penetrant of claim 1, wherein said nonionic wetting and spreading agent is a nonyl phenyl polyethylene glycol.
Claim 5
Dependent Claim 26 words
The sensitive liquid dye penetrant of claim 1, wherein the volume ratio of halocarbon solvents to the sum of the other components is at least 10:1.

References Cited (Backward Citations)

US3096142A Cited
US3265461A Cited
US3386920A Cited
US3518205A Cited
US3555071A Cited
US3561262A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-08-20 1977-02-19 1977-08-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-08-20 1981-02-19 1981-08-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-08-20 1985-02-19 1985-08-21 $7700.00 Window Closed / Lapsed

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