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US3718612A Expired / Lapsed US ⏱️ 0.0 years remaining

A process for producing a cigarette filter material

Assignee: STRICKMAN FOUNDATION Inc R
•
Filing: 1970-06-16
•
Granted: 1973-02-27
•
Expires: 1990-06-16
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Abstract

Abstract Filter materials for filtering aerosols, such as cigarette filters for filtering tobacco smoke, are provided comprising rigid polyurethane particles devoid of any cellular structure. Preferably the particles are granular and of jagged, spiny, cragged nature. The rigid polyurethane is produced from a polyol and a polyisocyanate. The particles are produced by first preparing a rigid polyurethane foam, preferably with the aid of a blowing agent, granulating the foam, treating the granules with hot water or steam to hydrolyze unreacted isocyanate and other free materials to render them inert, and then dried. Preferably, inorganic additives may be present during the preparation of the rigid polyurethane foam, such as the lower alkyl silicates, e.g., ethyl silicate, and water soluble salts of the acids of metals of groups VA and VIA of the Periodic Table, e.g., sodium tungstate. Inorganic additives may be added to the filter particles, such as an alkaline earth metal carbonate, silicate or hydroxide.

Inventors

  • 👤 R Strickman

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 23:04
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/0066; A; A24; A24D; A24D3/00; A24D3/06; A24D3/08; A24D3/16; C08K; C08K3/00; C08K3/18; C08K3/20; C08K3/22; C08K3/24; C08K3/26; C08K3/34; C08K5/00; C08K5/54; C08J2207/00; C08J2207/04; C08J2375/00; C08J2375/04; Y; Y10; Y10S; Y10S521/00; Y10S521/918

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 13 words
A process in accordance with claim 1 wherein the polyisocyanate is tolylene diisocyanate.
Claim 2
Dependent Claim 26 words
A process in accordance with claim 1 wherein between about 40 and 150 parts by weight of polyisocyanate are employed for each 100 parts of polyol.
Claim 3
Dependent Claim 35 words
A process according to claim 1 wherein the polyurethane is prepared in the presence of a water-soluble salt of an acid of a metal of Groups VA and VIA of the Periodic Table of Elements.
Claim 4
Dependent Claim 36 words
A process according to claim 1 wherein the polyurethane is prepared in the presence of a water-soluble alkali salt of an acid of a metal selected from the class consisting of tungsten, vanadium, chromium and molybdenum.
Claim 5
Dependent Claim 19 words
A process according to claim 1 wherein the polyurethane is prepared in the presence of a water-soluble alkali tungstate.
Claim 6
Dependent Claim 29 words
A process according to claim 4 wherein the amount of said water-soluble alkali salt employed is between about 0.2 and 4 parts by weight per 100 parts of polyol.
Claim 7
Dependent Claim 19 words
A process according to claim 1 wherein the polyurethane is prepared in the presence of a lower alkyl silicate.
Claim 8
Dependent Claim 30 words
A process according to claim 1 wherein the polyurethane is prepared in the presence of up to about 5 parts by weight of ethyl silicate per 100 parts of polyol.
Claim 9
Dependent Claim 29 words
A process according to claim 1 wherein there is added to the dried product a member selected from the class consisting of alkaline earth metal carbonates, silicates and hydroxides.
Claim 10
Dependent Claim 24 words
A process according to claim 10, wherein said member is added in an amount not exceeding 25 percent by weight of the dried product.
Claim 11
Dependent Claim 34 words
A process according to claim 1 wherein there is added to the dried product between about 3 and 15 percent by weight of an approximately equal parts mixture of aluminum hydroxide and magnesium trisilicate.

References Cited (Backward Citations)

GB922306A Cited
CA620248A Cited
US3127373A Cited
US2181614A Cited
US2770241A Cited
US2916464A Cited
US3006346A Cited
US3120849A Cited
US3171820A Cited
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GB1173449A Cited
US3574150A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-02-27 1976-08-28 1977-02-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-02-27 1980-08-28 1981-02-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-02-27 1984-08-28 1985-02-27 $7700.00 Window Closed / Lapsed

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