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US3715416A Expired / Lapsed US ⏱️ 0.0 years remaining

Filter start-up in dry spinning acrylonitrile copolymer

Assignee: Celanese Corp
•
Filing: 1971-06-14
•
Granted: 1973-02-06
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Expires: 1991-06-14
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Abstract

Abstract In dry spinning a heated solution of an acrylonitrile polymer in acetonitrile:water after passage through an apparatus comprising at least one filter, the improvement in the process of resuming flow of solution through said filter after interruption which comprises: positioning said filter in the path of flow of said solution from said supply to the spinnerette without establishing communication therebetween, filling said filter with solvent for said polymer, establishing a predetermined superatmospheric pressure-responsive normally closed outlet for solvent in said filter, either prior to or after filling said filter with solvent, heating it approximately to the temperature of said solution during filtration, establishing communication between said supply and said filter whereby the superatmospheric pressure builds up in said filter and bleeding solvent and solution out through said outlet, continuing to bleed solution through said outlet for a period of time sufficient to reestablish equilibrium conditions with said supply, and establishing communication between said filter and said spinnerette, whereby dry spinning is resumed.

Inventors

  • 👤 K Campbell
  • 👤 R Rhinehart

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 17:52
CPC Classifications
D; D01; D01D; D01D1/00; D01D1/10; D01D1/106; B; B01; B01D; B01D35/00; B01D35/12; B01D35/18; B01D37/00

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 221 words
In a process wherein a heated solution of an acrylonitrile polymer containing at least about 85 percent by weight of acrylonitrile and up to about 15 percent of another ethylenically unsaturated compound in a volatile organic liquid is extruded from a supply where it is maintained under pressure into an evaporative atmosphere after passage through an apparatus comprising at least one filter wherein solution flow through at least one filter is periodically terminated, and is thereafter resumed, the improvement in the process of resuming flow of solution through said filter which comprises positioning said filter in the path of flow of said solution from said supply to the point of extrusion without establishing communication therebetween, filling said filter with solvent for said polymer, establishing a predetermined superatmospheric pressure-responsive normally closed outlet for solvent in said filter, heating said filter to approximately the temperature of said solution during filtration, establishing communication between said supply and said filter whereby the superatmospheric pressure builds up in said filter and bleeding solvent and solution from said filter through said outlet, continuing to bleed solution through said outlet for a period of time sufficient to reestablish equilibrium conditions with said supply, and establishing communication between said filter and said point of extrusion, whereby solution passes through said filter to said extrusion point into the evaporative atmosphere.
Claim 2
Dependent Claim 221 words
In a process wherein a heated solution of an acrylonitrile polymer containing at least about 85 percent by weight of acrylonitrile and up to about 15 percent of another ethylenically unsaturated compound in a volatile organic liquid is extruded from a supply where it is maintained under pressure into an evaporative atmosphere after passage through an apparatus comprising at least one filter wherein solution flow through at least one filter is periodically terminated, and is thereafter resumed, the improvement in the process of resuming flow of solution through said filter which comprises positioning said filter in the path of flow of said solution from said supply to the point of extrusion without establishing communication therebetween, filling said filter with solvent for said polymer, establishing a predetermined superatmospheric pressure-responsive normally closed outlet for solvent in said filter, heating said filter to approximately the temperature of said solution during filtration, establishing communication between said supply and said filter whereby the superatmospheric pressure builds up in said filter and bleeding solvent and solution from said filter through said outlet, continuing to bleed solution through said outlet for a period of time sufficient to reestablish equilibrium conditions with said supply, and establishing communication between said filter and said point of extrusion, whereby solution passes through said filter to said extrusion point into the evaporative atmosphere.
Claim 3
Dependent Claim 15 words
The process of claim 1 wherein said solvent comprises acetonitrile, dimethylformamide, dimethylacetamide or ethylene carbonate.
Claim 4
Dependent Claim 11 words
The process of claim 1 wherein said solvent comprises aqueous acetonitrile.
Claim 5
Dependent Claim 19 words
The process of claim 1 wherein said heating is effected after said piece of apparatus is filled with solvent.
Claim 6
Dependent Claim 32 words
The process of claim 1 wherein said heating is effected prior to filling said piece of apparatus with solvent, said solvent also being heated prior to addition to said piece of apparatus.
Claim 7
Dependent Claim 23 words
The process of claim 1 wherein said solution of an acrylonitrile copolymer comprises a copolymer of acrylonitrile and methyl acrylate in aqueous acetonitrile.
Claim 8
Dependent Claim 16 words
The process of claim 1 wherein said piece of apparatus comprises a plurality of filter units.
Claim 9
Dependent Claim 65 words
The process of claim 7 wherein a first filter unit is maintained in use until a predetermined time interval or pressure threshold has been reached, after which a second filter unit is placed in operation while the first unit is still active, the first unit is inactivated, after a predetermined time interval or pressure threshold the second unit is replaced, and the cycle is repeated.

References Cited (Backward Citations)

US2166051A Cited
US2330932A Cited
US3503096A Cited
US2644195A Cited
US3436789A Cited
US3461193A Cited
US3480706A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-02-06 1976-08-07 1977-02-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-02-06 1980-08-07 1981-02-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-02-06 1984-08-07 1985-02-06 $7700.00 Window Closed / Lapsed

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