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US3691728A Expired / Lapsed US ⏱️ 0.0 years remaining

Regeneration process for solid desiccants

Assignee: Phillips Petroleum Co
•
Filing: 1969-10-29
•
Granted: 1972-09-19
•
Expires: 1989-10-29
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Abstract

Abstract A solid desiccant, used to dehydrate a gas, e.g., an ethylenecontaining gas resulting from the pyrolytic conversion of a saturated hydrocarbon such as ethane or propane, is washed of deposited or polymeric material by passing a solvent, for example, an aromatic solvent such as benzene, toluene, or xylene, into the same, draining the solvent from the desiccant and reducing the pressure on the desiccant to cause evaporation of solvent which is removed whereupon the desiccant is heated to regenerate the same. In a modification a gas, e.g., a fuel gas, is passed through the bed, wet with solvent, to agitate the solvent in the bed to aid in the removal of the deposit or polymer therefrom. The desiccant can be an alumina or molecular sieve or other known desiccant which can be used to dehydrate any known vapor or gas which tends to form deposits or polymers which can be removed with a solvent following a dehydrating cycle.

Inventors

  • 👤 Lucien H Vautrain
  • 👤 Russell W Lortz

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 07:40
CPC Classifications
B; B01; B01J; B01J20/00; B01J20/30; B01J20/34; B01J20/3408; B01D; B01D53/00; B01D53/02; B01D53/04; B01J20/02; B01J20/06; B01J20/08; B01J20/10; B01J20/16; B01J20/18; B01J20/3433; B01J20/345; B01J20/3475; B01J20/3483; C; C07; C07C; C07C7/00; C07C7/12; C07C7/13; B01D2253/00; B01D2253/10; B01D2253/104; B01D2256/00; B01D2256/24; B01D2257/00; B01D2257/80; B01D2259/00; B01D2259/40; B01D2259/40083; B01D2259/40086; B01D2259/40088; B01D2259/4009; B01D2259/402; B01J2220/00; B01J2220/50; B01J2220/56

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 45 words
A method according to claim 1 wherein there is passed through the bed in said zone, while it contains said solvent, a gas to agitate and, therefore, aid said solvent in diluting or loosening said deposit and, therefore, to better wash said bed of desiccant.
Claim 2
Dependent Claim 19 words
A method according to claim 1 wherein the solvent is drained from said bed prior to reducing the pressure.
Claim 3
Dependent Claim 21 words
A method according to claim 2 wherein the gas is passed through the bed prior to draining the solvent completely therefrom.
Claim 4
Dependent Claim 22 words
A method according to claim 1 wherein the gas is an unsaturated hydrocarbon and the deposit is a polymeric material formed therefrom.
Claim 5
Dependent Claim 27 words
A method according to claim 5 wherein the gas is an ethylene-containing gas derived from the pyrolytic conversion of a saturated hydrocarbon such as ethane or propane.
Claim 6
Dependent Claim 18 words
A method according to claim 1 wherein the desiccant is one of an alumina or a molecular sieve.
Claim 7
Dependent Claim 68 words
A method according to claim 1 wherein the solvent is passed downwardly through the bed of desiccant and wherein the solvent is drained from the bed, whereupon the pressure is reduced, the direction of flow remaining unchanged, so that the vapors of solvent forming due to reduction of pressure also pass downwardly from the bed, thus further aiding in the sweeping of the deposited material from the bed.
Claim 8
Dependent Claim 67 words
A method according to claim 1 wherein the introduced solvent which is in said bed is agitated by passing a gas through said bed, the bed is drained and the pressure then reduced, the gas being dehydrated is an ethylene-containing gas resulting from a pyrolytic conversion of a saturated hydrocaRbon such as ethane or propane and the deposit is a polymeric material formed from said ethylene-containing gas.
Claim 9
Dependent Claim 13 words
A method according to claim 9 wherein the solvent is an aromatic solvent.

References Cited (Backward Citations)

US3106593A Cited
US3242641A Cited
US3226913A Cited
US3304693A Cited
US3352840A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-09-19 1976-03-20 1976-09-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-09-19 1980-03-20 1980-09-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-09-19 1984-03-20 1984-09-19 $7700.00 Window Closed / Lapsed

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