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US3689544A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparing chelating agents

Assignee: WR Grace and Co
•
Filing: 1971-06-14
•
Granted: 1972-09-05
•
Expires: 1991-06-14
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Abstract

Abstract A chelating agent having the formula WHEREIN; R is an alkyl group having about one to 20 carbon atoms, hydrogen, -CH2CH2OH, or -CH2COOM; and M is an alkali metal cation, is prepared by; (a) adjusting the pH of a first aqueous system consisting essentially of water and an amino acid having the formula OR AN ALKALI METAL SALT OF THE ACID TO ABOUT 6-10.5 TO FORM A SECOND AQUEOUS SYSTEM CONSISTING ESSENTIALLY OF THE ALKALI METAL SALT OF THE AMINO ACID DISSOLVED IN WATER, AND ADJUSTING THE TEMPERATURE OF THE SECOND AQUEOUS SYSTEM AT ABOUT 65*-105* C.; and (b) admixing epichlorohydrin with the second aqueous system while; (i) maintaining the pH of the resulting mixture at about 6-10.5; and (ii) maintaining the temperature of the resulting mixture at about 65*-105* C. for about 30-180 minutes to form a third aqueous system consisting essentially of an aqueous solution of the chelating agent.

Inventors

  • 👤 Patricia M Scanlon
  • 👤 Jon C Thunberg

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 21:01
CPC Classifications
C; C07; C07F; C07F1/00; C07F1/005

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 10 words
The compound of claim 1 in which R1 is -CH3.
Claim 2
Dependent Claim 10 words
The compound of claim 1 in which R1 is -CH2CH2OH.
Claim 3
Dependent Claim 10 words
The compound of claim 1 in which R1 is hydrogen.
Claim 4
Dependent Claim 13 words
The compound of claim 1 in which R2 is an alkali metal ion.
Claim 5
Dependent Claim 11 words
The compound of claim 1 in which R2 which is hydrogen.

References Cited (Backward Citations)

US2407645A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-09-05 1976-03-06 1976-09-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-09-05 1980-03-06 1980-09-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-09-05 1984-03-06 1984-09-05 $7700.00 Window Closed / Lapsed

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