Patent US2703998A successfully refreshed from Google Patents.
US3681996A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Liquid sample valve
Assignee: Individual
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Filing: 1970-07-10
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Granted: 1972-08-08
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Expires: 1990-07-10
Abstract
Abstract A small hydraulic pressure injection valve having spaced apart plungers which are spring loaded with respect to each other for use in injecting a liquid sample into a chromatographic column without awaiting the action of a carrier flow gas. The sample, placed in the space between the plungers, is injected immediately into the chromatographic column as the plungers advance and are forced together. There is no problem of evaporation of the sample, as the flow path to the column is flushed as a new sample is loaded into the valve.
Inventors
- 👤 Michael C Crist
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 11:33
CPC Classifications
G; G01; G01N; G01N30/00; G01N30/02; G01N30/04; G01N30/16; G01N30/20; G01N2030/204
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
276 words
Sample valve apparatus comprising an elongated hollow cylinder having a side wall, a closed end, an open end and an array of four ports extending through said side wall, two of said ports lying essentially in a common plane perpendicular to the longitudinal axis of said cylinder, first and second normally spaced apart plungers having forward and rear ends, each of said plungers fitting closely but slidably in said cylinder in end to end relationship, each of said plungers having a portion of reduced cross section intermediate its ends, said first plunger being closest to the closed end of said cylinder and having a rod coupled thereto and extending from the rear end thereof, said second plunger having an axially extending bore therethrough through which said rod fits closely but slidably, means for spring loading said rod with respect to said second plunger, means for driving said plungers in reciprocating motion, said two ports lying essentially in a plane perpendicular to the longitudinal axis of said cylinder being aligned with the space between said plungers and the other two ports being aligned with the reduced cross section portion when said plungers are in their withdrawn reciprocating motion position, said space between said plungers being aligned with one of said other two ports when said plungers are in their forward position, the other of said other two ports being disposed closer to said closed end of said cylinder and being isolated from said space between said plungers at all times during operation of said apparatus, said means for spring loading applying pressure to closed the space between said plungers on maximum forward movement of said reciprocating motion.
Claim 2
Dependent Claim
276 words
Sample valve apparatus comprising an elongated hollow cylinder having a side wall, a closed end, an open end and an array of four ports extending through said side wall, two of said ports lying essentially in a common plane perpendicular to the longitudinal axis of said cylinder, first and second normally spaced apart plungers having forward and rear ends, each of said plungers fitting closely but slidably in said cylinder in end to end relationship, each of said plungers having a portion of reduced cross section intermediate its ends, said first plunger being closest to the closed end of said cylinder and having a rod coupled thereto and extending from the rear end thereof, said second plunger having an axially extending bore therethrough through which said rod fits closely but slidably, means for spring loading said rod with respect to said second plunger, means for driving said plungers in reciprocating motion, said two ports lying essentially in a plane perpendicular to the longitudinal axis of said cylinder being aligned with the space between said plungers and the other two ports being aligned with the reduced cross section portion when said plungers are in their withdrawn reciprocating motion position, said space between said plungers being aligned with one of said other two ports when said plungers are in their forward position, the other of said other two ports being disposed closer to said closed end of said cylinder and being isolated from said space between said plungers at all times during operation of said apparatus, said means for spring loading applying pressure to closed the space between said plungers on maximum forward movement of said reciprocating motion.
Claim 3
Dependent Claim
19 words
Apparatus in accordance with claim 1, wherein said closed end of said cylinder has adjustable stop means extending therethrough.
Claim 4
Dependent Claim
21 words
Apparatus in accordance with claim 1, wherein means coupled to said rod are provided for adjusting the space between said plungers.
Claim 5
Dependent Claim
21 words
Apparatus in accordance with claim 1, wherein said ports lying in a common plane are in opposed position to each other.
Claim 6
Dependent Claim
37 words
Apparatus in accordance with claim 1, wherein said ports lying in a common plane communicate with said reduced cross section portion of said second plunger when said reciprocatory motion is at other than the withdrawn part thereof.
Claim 7
Dependent Claim
24 words
Apparatus in accordance with claim 1, wherein seal means are provided on each plunger adjacent to each end of said reduced cross section portions.
References Cited (Backward Citations)
US3162050A
Cited
US3362228A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1975-08-08 | 1976-02-07 | 1976-08-08 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1979-08-08 | 1980-02-07 | 1980-08-08 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1983-08-08 | 1984-02-07 | 1984-08-08 | $7700.00 | Window Closed / Lapsed |