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US3677477A Expired / Lapsed US ⏱️ 0.0 years remaining

Apparatus for preparing dispersions of finely-divided alkali metal

Assignee: Millennium Petrochemicals Inc
•
Filing: 1970-06-01
•
Granted: 1972-07-18
•
Expires: 1990-06-01
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Abstract

Abstract Apparatus for preparing dispersions of finely divided alkali metal substantially uniform in alkali metal concentration and having a narrow particle size below a predetermined median, said apparatus comprising a mixing tank divided by a vertically disposed baffle into a mixing zone and a substantially smaller quiescent, settling zone. Molten sodium feed and a dispersing aid mixture is agitated within said mixing zone in an inert gas blanket and alkali metal particles gravitate through the settling zone to the bottom of the mixing tank at which point the mixture containing said particles is drawn off in a continuous operation and passed to an homogenizer providing a high shear dispersion zone wherein the metallic particles are reduced in size and the mixture is returned to the mixing tank. Through repeated recirculation, such metallic particles as become reduced in size to the predetermined median size desired rise to the top of the quiescent, settling zone at which point the desired uniform dispersion containing only fine metallic particles within a closely controlled range is withdrawn.

Inventors

  • 👤 Lloyd M Watson
  • 👤 William R Birchall

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 11:10
CPC Classifications
B; B22; B22F; B22F9/00; B22F9/02; B22F9/06; B01; B01F; B01F33/00; B01F33/80; B01F33/82; B01F33/821

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 17 words
Apparatus as set forth in claim 1 wherein the high shear dispersion zone is a colloid mill.
Claim 2
Dependent Claim 18 words
Apparatus as set forth in claim 1 wherein the high shear dispersion zone is a displacement valve homogenizer.
Claim 3
Dependent Claim 17 words
Apparatus as set forth in claim 1 wherein the high shear dispersion zone is a reed-type homogenizer.
Claim 4
Dependent Claim 57 words
Apparatus as set forth in claim 1 wherein the vertical edge walls of the arcuate baffle are located in close and parallel relationship with respect to the adjacent interior wall of the mixing tank and the bottom of said mixing tank is conical and the conduit means for conveying mixture to the homogenizer is connected centrally thereof.

References Cited (Backward Citations)

US1977807A Cited
US2277477A Cited
US2520320A Cited
US2685826A Cited
US2903191A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-07-18 1976-01-17 1976-07-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-07-18 1980-01-17 1980-07-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-07-18 1984-01-17 1984-07-18 $7700.00 Window Closed / Lapsed

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