US3673290A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Foamed clay process
Assignee: Dow Chemical Co
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Filing: 1969-11-26
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Granted: 1972-06-27
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Expires: 1989-11-26
Abstract
Abstract Disclosed is a foamed ceramic material having a relatively small and uniform cell structure. The material is suitable for structural or insulating purposes. A continuous process for producing the foamed ceramic material comprises dropping a bloatable ceramic composition, in particulate form, through a heated zone thereby fusing and bloating the particles, and subsequently collecting the fused particles. To produce the desired cellular structure, the process does not fully bloat the particles during dropping, thereby delaying part of the bloating of the particles until after they have been collected as an agglomerated slab.
Inventors
- 👤 Burton D Brubaker
- 👤 Nathan Waldman
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 16:38
CPC Classifications
C; C04; C04B; C04B38/00; C04B38/06; C04B38/063; C04B38/0635; C04B38/064; Y; Y10; Y10T; Y10T428/00; Y10T428/249921; Y10T428/249953; Y10T428/249967; Y10T428/24997
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
47 words
A process as in claim 1 wherein the bloatable ceramic composition comprises at least about 3 weight percent of iron expressed as Fe2O3 and wherein the atmosphere in the heating zones through which the bloatable ceramic particles and agglomerated cellular material are passed is a reducing atmosphere.
Claim 2
Dependent Claim
61 words
A process as in claim 1 wherein the bloatable ceramic composition has a maximum bloating capacity of less than 25 p.c.f. and wherein the temperature in the dropping zone is regulated so that the ratio of the bulk density of bloated particles immediately before collection thereof, to the bulk density of particles before dropping is from aBout 0.20 to about 0.75.
Claim 3
Dependent Claim
17 words
The process of claim 3 wherein the bulk density ratio is from about 0.30 to about 0.50.
Claim 4
Dependent Claim
57 words
A process as in claim 3 wherein the temperature of the dropping zone is from about 175* C. to about 400* C. above the initial melting temperature of the composition, and wherein the temperature of the collection zone is from about 50* C. to about 250* C. above the initial melting temperature of the bloatable ceramic composition.
Claim 5
Dependent Claim
80 words
A process as in claim 5 wherein the temperature of the dropping zone is from about 200* C. to about 305* C. above the initial melting temperature of the composition, and wherein the temperature of the collection zone is from about 125* C. to about 225* C. above the initial melting temperature of the bloatable ceramic composition with the time of residence of the collected particles and foamed ceramic slab in the collection zone being about 0.5 to 5.0 minutes.
Claim 6
Dependent Claim
48 words
A process as in claim 6 wherein the initial melting temperature of the bloatable ceramic composition is about 1,020* C., the dropping zone temperature is about 1,260* C., with the falling time for particles being about 0.80 second, and wherein the collection zone temperature is about 1,165* C.
Claim 7
Dependent Claim
183 words
A process for preparing an agglomerated foamed ceramic material having a uniform density of about 12 pounds per cubic foot or less comprising: a. dropping particles of a bloatable ceramic composition containing from about 0.50 to about 2.0 percent by weight of organic carbon and having a maximum bloating capacity of less than about 25 p.c.f. downwardly through a heated dropping zone wherein the temperature is sufficiently in excess of the initial melting temperature of the composition to bloat the particles sufficiently to provide a ratio of the bulk density of the bloated particles immediately before collection thereof to the bulk density of the particles before dropping from about 0.20 to about 0.75, b. agglomerating the bloated particles below the dropping zone in a heated collection zone to form an initial agglomerate of a partially foamed ceramic material, c. heating said initial agglomerate at a temperature above the initial melting temperature and below the temperature of the dropping zone for a time sufficient to further bloat and coalesce the particles to form a foamed ceramic agglomerate, and d. cooling the foamed ceramic agglomerate.
Claim 8
Dependent Claim
187 words
A process for preparing an agglomerated foamed ceramic material having a uniform density of about 10 pounds per cubic foot or less comprising: a. dropping particles of a bloatable ceramic composition containing from about 0.50 to about 2.0 per cent by weight of organic carbon and having a maximum bloating capacity of less than about 20 p.c.f. downwardly through a heated dropping zone wherein the temperature is sufficiently in excess of the initial melting temperature of the composition to bloat the particles sufficiently to provide a ratio of the bulk density of the bloated particles immediately before collection thereof to the bulk density of the particles before dropping from about 0.30 to about 0.50, b. agglomerating the bloated particles below the dropping zone in a heated collection zone to form an initial agglomerate of a partially foamed ceramic material, c. heating said initial agglomerate at a temperature above the initial melting temperature of said composition and below the temperature of the dropping zone for a time sufficient to further bloat and coalesce the particles to form a foamed ceramic agglomerate, and d. cooling the foamed ceramic agglomerate.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1975-06-27 | 1975-12-27 | 1976-06-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1979-06-27 | 1979-12-27 | 1980-06-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1983-06-27 | 1983-12-27 | 1984-06-27 | $7700.00 | Window Closed / Lapsed |