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US3673085A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and apparatus for treating solutions by solid-ion exchangers

Assignee: GRENOBLOISE ETUDE APPL
•
Filing: 1969-11-19
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Granted: 1972-06-27
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Expires: 1989-11-19
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Abstract

Abstract An installation for the treatment of solutions by solid ion exchangers in a mobile bed, comprising an initial chamber formed by a central cylindrical column, followed by an even number of successive concentric annular chambers surrounding at least part of the central column, the exchange media rising up through the said column, spilling over the whole periphery of its top edge down into the first annular chamber, and passing from the bottom of the latter to the bottom of the second annular chamber. The flow of liquid in the column and the two chambers occurs in directions opposite to the directions of movement of the bed therethrough and whenever two liquids of different densities are present in the same chamber, the denser liquid is below the lighter liquid and is separated therefrom by an interface. The inlet and outlet flow rates of each liquid are controlled to keep the movements of an interface between certain limits during the operation of the installation.

Inventors

  • 👤 Paul Minart

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 00:18
CPC Classifications
B; B01; B01J; B01J47/00; B01J47/10; B01D; B01D15/00; B01D15/02; B01D15/08; B01D15/10; B01D15/18; B01D15/1892

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 116 words
An installation as defined in claim 1, in which said one chamber is the central chamber of said concentric chamber arrangement, and has a vertical dimension substantially greater than the vertical dimensions of the other chambers, in which said bed moving means is constructed to displace the bed upwardly in such central chamber, and in which said supplying means includes means for supplying a washing liquid to the liquid inlet associated with the upper end of such central chamber, and means for supplying a regenerant liquid to said first inlet for a denser liquid, the regenerant and washing liquids passing downwardly through said central chamber being discharged through said first liquid outlet at the bottom thereof.
Claim 2
Dependent Claim 68 words
An installation as defined in claim 2, in which said other bed containing chambers enclose one end portion of said central chamber, and in which said vessel is constructed to provide an exchanger collection chamber concentrically arranged with and in communication with the upper end of said central chamber, means for fluidizing the exchangers collected in said collection chamber, and an evacuation conduit for removing the fluidized exchangers.
Claim 3
Dependent Claim 44 words
An installation as defined in claim 3, in which said other bed containing chambers enclose the upper end portion of said central chamber and are located between said central chamber and said collection chamber and provide communication between the latter and said central chamber.
Claim 4
Dependent Claim 138 words
An installation as defined in claim 4, in which said vessel includes a cover for said central chamber spaced upwardly from the upper end of the latter and having a depending circular wall enclosing the upper part of the side wall of said central chamber in spaced relation, and an open cylindrical receptacle enclosing the upper part of said central chamber and said depending wall in spaced relation, the side wall of said central chamber, the top of said cover and the depending wall thereof forming one of said other bed containing chambers, and said depending wall and the side wall of said cylindrical receptacle forming a second other bed containing chamber, said cover having a side wall enclosing the upper open end of said cylindrical vessel and forming with the latter said collection chamber for the exchangers.
Claim 5
Dependent Claim 75 words
An installation as defined in claim 2, in which said bed moving means comprises a tangential inlet for supplying exchangers to a chamber enclosing and in communication with the lower end of said central chamber, said tangential inlet being spaced above the bottom of said enclosing chamber, and a liquid outlet provided in said enclosing chamber below said tangential inlet to draw off effluent in the peripheral zone at the bottom of said central column.
Claim 6
Dependent Claim 49 words
An installation as defined in claim 1, in which said other of said two chambers containing a treatment zone has said second inlet thereof located at the bottom of said other chamber, and has said second outlet thereof located intermediate the upper and bottom ends of said other chamber.
Claim 7
Dependent Claim 49 words
An installation as defined in claim 1, in which said other of said two chambers containing a treatment zone has said second inlet thereof located intermediate the upper and bottom ends of said other chamber, and has said second outlet thereof located at the bottom of said other chamber.
Claim 8
Dependent Claim 110 words
An installation as defined in claim 2, in which said other bed containing chambers include said other of said two chambers and a third chamber in annulAr communication with the latter, in which said liquid inlet means and said second outlet are constructed and arranged to provide two liquids of different densities in each of such two communicating chambers with the denser liquid in each located below the lighter liquid and separated therefrom by an interface, and in which said control means maintains the interface in one of such two communicating chambers at a different vertical position that that of the interface in the other of such two communicating chambers.
Claim 9
Independent Claim 352 words
A method of treatment of solutions by solid ion exchangers in a mobile bed, comprising providing a single bed of solid ion exchangers in a plurality of successive bed containing chambers concentrically arranged to be in annular communication at the ends thereof so that the bed has a plurality of connected vertically disposed parts, intermittently moving the bed forwardly under the impulsion of liquid through such chambers so that in each such forward movement, parts thereof are simultaneously moved downwardly and upwardly through the communicating bed containing chambers, then during each of the stationary periods of the ion exchangers in such chambers, supplying liquids to said bed so that they flow counter to the movements of bed parts in such chambers and provide separate treatment zones along the length of the compact mobile bed extending continuously in all of such successive chambers, such liquids being supplied to a plural of said chambers so that there are provided in each thereof two liquids of different densities, the lighter liquid being supplied to the upper portions of such plural chambers and the denser liquid being supplied to and extracted from portions of such plural chambers spaced below the places of supply of the lighter liquid thereto and so that there is formed in at least one of such plural chambers an interface between the lighter and denser liquids therein, the places of the supply and extraction of the denser liquid in said one of such plural chambers containing the interface being so located that one of them is intermediate the upper and bottom ends of such one chamber and the other is associated with the bottom end of such one chamber, and the supply of the denser liquid in another of such plural chambers being between the upper and bottom ends thereof and both the lighter and denser liquids supplied to each other chamber being extracted at the bottom thereof, and including the step of controlling the interface in said one of such plural chambers to compensate for changes in position thereof due to the displacement of the ion exchangers in such one chamber.

References Cited (Backward Citations)

US2699379A Cited
US2730239A Cited
US2963431A Cited
US2908596A Cited
US2973319A Cited
US3445382A Cited
US3503510A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-06-27 1975-12-27 1976-06-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-06-27 1979-12-27 1980-06-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-06-27 1983-12-27 1984-06-27 $7700.00 Window Closed / Lapsed

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