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US3671560A Expired / Lapsed US ⏱️ 0.0 years remaining

Manufacture of palladium or platinum-containing compounds

Assignee: Phillips Petroleum Co
•
Filing: 1970-09-29
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Granted: 1972-06-20
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Expires: 1990-09-29
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Abstract

Abstract Compounds of the formula M(Z3P)4, where M is palladium or platinum and Z is a hydrocarbon or substituted hydrocarbon radical, are produced by reacting the metal in elemental form with a corresponding Z3P compound. One specific example is the production of tetrakis(triphenylphosphine)palladium(O) by reacting elemental palladium with triphenylphosphine.

Inventors

  • 👤 Darryl R Fahey

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 05:54
CPC Classifications
C; C07; C07F; C07F15/00; C07F15/0006; C07F15/006; C07F15/0066; C07F15/0086; C07F15/0093

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 27 words
The method of claim 1 wherein the contacting is carried out in the presence of a hydrocarbon in which said at least one Z3P compound is soluble.
Claim 2
Dependent Claim 16 words
The method of claim 2 wherein said material is recovered from the reaction medium by crystallization.
Claim 3
Dependent Claim 27 words
The method of claim 1 in which the contacting is for a period of 2 to 36 hours in the temperature range of 0* to 150* C.
Claim 4
Dependent Claim 21 words
The method oF claim 1 in which the M is supported on a material that is inert under the contacting conditions.
Claim 5
Dependent Claim 15 words
The method of claim 1 wherein tetrakis(triphenylphosphine)palladium(0) is produced by contacting elemental palladium with triphenylphosphine.
Claim 6
Dependent Claim 16 words
The method of claim 6 wherein the contacting is carried out in the presence of benzene.
Claim 7
Dependent Claim 13 words
The method of claim 7 wherein the palladium is supported on barium sulfate.
Claim 8
Dependent Claim 24 words
The method of claim 8 wherein the contacting is carried out at a temperature substantially the same as the boiling point of the benzene.

References Cited (Backward Citations)

US3102899A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-06-20 1975-12-20 1976-06-20 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-06-20 1979-12-20 1980-06-20 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-06-20 1983-12-20 1984-06-20 $7700.00 Window Closed / Lapsed

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