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US3658688A Expired / Lapsed US ⏱️ 0.0 years remaining

Two-stage c{11 {0 dewaxing/deoiling process

Assignee: ExxonMobil Technology and Engineering Co
•
Filing: 1969-09-19
•
Granted: 1972-04-25
•
Expires: 1989-09-19
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Abstract

Abstract An improved process for dewaxing and deoiling a petroleum oil stock with a liquid, normally gaseous solvent in which the oil feed is chilled prior to autorefrigeration by dilution with cold recycled filtrate from the final filtration of the wax-oilsolvent mixture.

Inventors

  • 👤 Frank A Biribauer
  • 👤 James D Bushnell

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 19:54
CPC Classifications
C; C10; C10G; C10G73/00; C10G73/02; C10G73/06

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 12 words
The process of claim 1 wherein said stagewise filtration comprises 2 stages.
Claim 2
Dependent Claim 10 words
The process of claim 1 wherein said solvent comprises propane.
Claim 3
Dependent Claim 26 words
The process of claim 1 wherein the solvent-oil wax slurry is withdrawn from said cooling zone at a temperature of from about 0* to +40* F.
Claim 4
Dependent Claim 20 words
The process of claim 1 wherein said liquid, normally gaseous, solvent is a C2 to C4 hydrocarbon or mixtures thereof.
Claim 5
Dependent Claim 10 words
The process of claim 5 wherein said solvent comprises propylene.
Claim 6
Dependent Claim 217 words
A process for dewaxing a wax-containing petroleum oil fraction and deoiling the wax thus obtained, comprising introducing said fraction into a cooling zone divided into a plurality of stages, introducing a solvent selected from the group consisting of C2-C4 hydrocarbons and mixtures thereof, into said cooling zone at a plurality of points along said cooling zone, maintaining a high degree of agitation in each of said stages so as to provide substantially instantaneous mixing of said oil and said solvent, cooling said oil as it progresses through said cooling zone at a cooling rate of from about 2* to 10* F./minute, thereby precipitating at least a portion of the wax contained in said oil and forming a solvent-oil-wax slurry, vaporizing at least a portion of said solvent from said slurry thereby precipitating a further portion of said wax, separating a dewaxed oil and an oil-containing wax from said slurry, removing at least a portion of said oil from said oil-containing wax by mixing therewith solvent thereby forming an oil-solvent mixture containing said wax, separating a deoiled wax from said mixture by stagewise filtration thereof, recovering a final stage filtrate comprising an oil-solvent mixture and recycling at least a portion of said oil-solvent mixture of said final stage filtrate to said cooling zone for use as solvent therein.
Claim 7
Dependent Claim 11 words
The process of claim 7 wherein said C2-C4 hydrocarbon comprises propylene.
Claim 8
Dependent Claim 11 words
The process of claim 7 wherein said C2-C4 hydrocarbon comprises propane.
Claim 9
Dependent Claim 25 words
The process of claim 7 wherein said solvent-oil-wax slurry is withdrawn from said cooling zone at a temperature of from about 0* to 40* F.

References Cited (Backward Citations)

US2734849A Cited
US2281667A Cited
US2287966A Cited
US3350297A Cited
US3393144A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-04-25 1975-10-25 1976-04-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-04-25 1979-10-25 1980-04-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-04-25 1983-10-25 1984-04-25 $7700.00 Window Closed / Lapsed

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