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US3655545A Expired / Lapsed US ⏱️ 0.0 years remaining

Post heating of sputtered metal oxide films

Assignee: PPG Industries Inc
•
Filing: 1970-07-02
•
Granted: 1972-04-11
•
Expires: 1990-07-02
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Abstract

Abstract This invention relates to a novel method of producing electroconductive metal oxide films by cathodic sputtering. It especially pertains to a method of increasing the electroconductivity of sputtered metal oxide films by mildly reducing said films. The reduction step follows sputtering and generally involves heating the metal oxide film in a nonoxidizing or reducing atmosphere for a sufficient period of time to reduce the oxygen content of said film by a minor amount but without substantially reducing the oxide film to metallic form.

Inventors

  • 👤 Frank H Gillery
  • 👤 Jean P Pressau

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 16:21
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/58; C23C14/5806; C03; C03C; C03C17/00; C03C17/22; C03C17/23; C03C17/245; C03C17/2453; C03C23/00; C03C23/007; C23C14/06; C23C14/08; C23C14/086; C23C14/5846; C03C2217/00; C03C2217/20; C03C2217/21; C03C2217/211; C03C2217/215; C03C2217/23; C03C2217/231; C03C2218/00; C03C2218/10; C03C2218/15; C03C2218/154

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 13 words
The method of claim 1 wherein the post heating is conducted in vacuo.
Claim 2
Dependent Claim 15 words
The method of claim 1 wherein the post heating is conducted in a reducing atmosphere.
Claim 3
Dependent Claim 15 words
The method of claim 1 wherein the post heating is conducted in a hydrogen-containing atmosphere.
Claim 4
Dependent Claim 10 words
The method of claim 1 wherein the substrate is glass.
Claim 5
Dependent Claim 21 words
The method of claim 1 wherein post heating is conducted at a temperature of about 240* C. to about 340* C.
Claim 6
Dependent Claim 11 words
The method of claim 1 wherein the metal cathode contains indium.
Claim 7
Dependent Claim 27 words
The method of claim 7 wherein the post heating is at a temperature of about 240* C. to about 340* C. for less than about two hours.
Claim 8
Dependent Claim 19 words
The method of claim 1 wherein the metal cathode contains a greater quantity of indium that that of tin.
Claim 9
Dependent Claim 23 words
The method of claim 9 wherein the metal cathode contains a maximum of 20 percent by weight of tin and the balance indium.

References Cited (Backward Citations)

CA566773A Cited
US2597562A Cited
US2825687A Cited
US3108019A Cited
US3370978A Cited
US3420706A Cited
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US3506556A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-04-11 1975-10-11 1976-04-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-04-11 1979-10-11 1980-04-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-04-11 1983-10-11 1984-04-11 $7700.00 Window Closed / Lapsed

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