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US3655464A Expired / Lapsed US ⏱️ 0.0 years remaining

Process of preparing a liquid sintered cobalt-rare earth intermetallic product

Assignee: General Electric Co
•
Filing: 1970-04-30
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Granted: 1972-04-11
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Expires: 1990-04-30
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Abstract

Abstract A process for preparing novel sintered cobalt-rare earth intermetallic products which can be magnetized to form permanent magnets having stable improved magnetic properties. A particulate mixture is formed of a base CoR alloy and an additive CoR alloy, where R is a rare earth metal. The base CoR alloy is one which, at sintering temperature, exists as a solid Co5R intermetallic single phase. The additive CoR alloy is richer in rare earth metal than the base CoR alloy, and at sintering temperature is at least partly liquid. The base and additive alloys, in particulate form, are each used in an amount to form a mixture which has a cobalt and rare earth metal content substantially corresponding to that of the final desired sintered product. The mixture is pressed into compacts and sintered to the desired sintered product phase composition and density. At sintering temperature, the final sintered product has a phase composition lying outside the Co5R single phase on the rare earth richer side. Specifically, the final sintered product contains a major amount of the Co5R single phase on the solid intermetallic phase and up to about 35 percent by weight of the product of a second solid CoR intermetallic phase which is richer in rare earth content than the Co5R phase.

Inventors

  • 👤 Mark G Benz

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 11:42
CPC Classifications
H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/032; H01F1/04; H01F1/047; H01F1/053; H01F1/055; H01F1/0555; H01F1/0557; C; C22; C22C; C22C19/00; C22C19/07

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 22 words
A process for producing a sintered cobalt-rare earth intermetallic product according to claim 1 wherein said cobalt-rare earth alloys are cobalt-samarium alloys.
Claim 2
Dependent Claim 22 words
A process according to claim 2 wherein said base alloy ranges in samarium content from about 32 to 36 percent by weight.
Claim 3
Dependent Claim 13 words
A process according to claim 3 wherein said base alloy is substantially Co5Sm.
Claim 4
Dependent Claim 27 words
A process according to claim 2 wherein said additive alloy ranges in samarium content from about 46 percent to about 65 percent by weight of said additive.
Claim 5
Dependent Claim 24 words
A process according to claim 2 wherein said mixture is composed of about 62 percent by weight cobalt and 38 percent by weight samarium.
Claim 6
Dependent Claim 19 words
A process according to claim 2 wherein said sintering temperature ranges from about 950* C. to about 1,200* C.
Claim 7
Dependent Claim 17 words
A process according to claim 1 wherein said base cobalt-rare earth alloy is a cobalt-samarium-cerium mischmetal alloy.
Claim 8
Dependent Claim 24 words
A process according to claim 1 wherein said pressing of said mixture into a green body is carried out in an aligning magnetizing field.
Claim 9
Dependent Claim 21 words
A process according to claim 1 wherein said sintered product has a density of at least about 87 percent of theoretical.
Claim 10
Dependent Claim 21 words
A process according to claim 1 wherein the particle size of said particulate mixture ranges from about 1 to 10 microns.
Claim 11
Dependent Claim 28 words
A process according to claim 1 wherein said sintered product contains said Co5R intermetallic phase in an amount of about 95 percent by weight of said sintered product.
Claim 12
Dependent Claim 10 words
A process according to claim 12 wherein R is samarium.
Claim 13
Dependent Claim 29 words
A process according to claim 1 which includes the steps of crushing said sintered product into particles, and bonding the resulting particles of sintered product to a matrix material.
Claim 14
Dependent Claim 25 words
A process according to claim 1 which includes the step of subjecting said sintered product to a magnetizing field to produce a magnetized sintered product.
Claim 15
Dependent Claim 27 words
A process according to claim 14 which includes the step of subjecting said bonded particles in said matrix material to a magnetizing field to magnetize said particles.

References Cited (Backward Citations)

US3425828A Cited
US3546030A Cited
US3424578A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-04-11 1975-10-11 1976-04-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-04-11 1979-10-11 1980-04-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-04-11 1983-10-11 1984-04-11 $7700.00 Window Closed / Lapsed

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