Patent US1315536A successfully refreshed from Google Patents.
← Back to Patent Explorer
US3639718A Expired / Lapsed US ⏱️ 0.0 years remaining

Pressure- and temperature-controlled crystal growing apparatus

Assignee: Arthur D Little Inc
•
Filing: 1970-06-15
•
Granted: 1972-02-01
•
Expires: 1990-06-15
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract Furnace assembly providing a working volume the pressure in which may range from 10 5 torr to 100 atmospheres. Controlled temperatures up to 4,000* C. are attainable. Two load-bearing rods extending into the furnace are rotated and moved along their vertical axes over a wide speed range. Means are provided continuously to indicate the precise position of each rod, to monitor the operation within the furnace by TV, and to control the operations within the furnace from a remote location.

Inventors

  • 👤 Roger A Castonguay
  • 👤 Bernard C Hanley
  • 👤 Francis J Mallahan
  • 👤 Joseph F Wenckus

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 21:36
CPC Classifications
C; C30; C30B; C30B15/00; C30B15/20; C30B15/22; C30B15/26; C30B15/30; Y; Y10; Y10T; Y10T117/00; Y10T117/10; Y10T117/1004; Y10T117/1008; Y10T117/1012; Y10T117/1024; Y10T117/1032; Y10T117/1056; Y10T117/106; Y10T117/1064; Y10T117/1068; Y10T117/1072; Y10T117/1076; Y10T117/1092

Claims Analysis

Total Claims: 76
Claim 1
Independent Claim 142 words
A pressure- and temperature-controlled apparatus adapted for growing crystals and the like, comprising in combination. a. a pressuretight enclosure defining a working volume therein; b. upper and lower load-bearing rods extending through pressuretight bushing means into said volume and movable therein in both rotational and translational modes; c. upper and lower rotational and translational rod driving means located external of said pressuretight enclosure, said translational driving means including means to selectively drive said rods in a slow crystal-growing mode or in a rapidpositioning mode; d. rod-locating means associated with said translational driving means adapted continuously to indicate the precise position of said rods within said volume; e. heating means positioned with respect to said rods to heat a load supported by one or both of said rods within aid volume; and f. viewing port means providing for visual observation of said load.
Claim 2
Dependent Claim 142 words
A pressure- and temperature-controlled apparatus adapted for growing crystals and the like, comprising in combination. a. a pressuretight enclosure defining a working volume therein; b. upper and lower load-bearing rods extending through pressuretight bushing means into said volume and movable therein in both rotational and translational modes; c. upper and lower rotational and translational rod driving means located external of said pressuretight enclosure, said translational driving means including means to selectively drive said rods in a slow crystal-growing mode or in a rapidpositioning mode; d. rod-locating means associated with said translational driving means adapted continuously to indicate the precise position of said rods within said volume; e. heating means positioned with respect to said rods to heat a load supported by one or both of said rods within aid volume; and f. viewing port means providing for visual observation of said load.
Claim 3
Dependent Claim 20 words
An apparatus according to claim 1 wherein said pressuretight enclosure has a hinged access port equipped with pressure-relief valve means.
Claim 4
Dependent Claim 8 words
worm drive means for actuating said driving screw,
Claim 5
Dependent Claim 8 words
worm drive means for actuating said driving screw,
Claim 6
Dependent Claim 21 words
a radiamatic pyrometer connected to said light pipe means and adapted to generate DC voltage signals proportional to the light received,
Claim 7
Dependent Claim 21 words
a radiamatic pyrometer connected to said light pipe means and adapted to generate DC voltage signals proportional to the light received,
Claim 8
Dependent Claim 10 words
a magnet attached along the side of said shaft extension,
Claim 9
Dependent Claim 10 words
a magnet attached along the side of said shaft extension,
Claim 10
Dependent Claim 8 words
worm drive means for actuating said driving screw,
Claim 11
Dependent Claim 8 words
worm drive means for actuating said driving screw,
Claim 12
Dependent Claim 21 words
a radiamatic pyrometer connected to said light pipe means and adapted to generate DC voltage signals proportional to the light received,
Claim 13
Dependent Claim 21 words
a radiamatic pyrometer connected to said light pipe means and adapted to generate DC voltage signals proportional to the light received,
Claim 14
Dependent Claim 10 words
a magnet attached along the side of said shaft extension,
Claim 15
Dependent Claim 10 words
a magnet attached along the side of said shaft extension,
Claim 16
Dependent Claim 7 words
reed switch means actuatable by said magnet,
Claim 17
Dependent Claim 7 words
reed switch means actuatable by said magnet,
Claim 18
Dependent Claim 9 words
induction heating power supply means for said RF coil,
Claim 19
Dependent Claim 9 words
induction heating power supply means for said RF coil,
Claim 20
Dependent Claim 10 words
flexible drive shaft means connected to said worm drive means,
Claim 21
Dependent Claim 10 words
flexible drive shaft means connected to said worm drive means,
Claim 22
Dependent Claim 8 words
magnetic reed switch means actuatable by said magnet,
Claim 23
Dependent Claim 8 words
magnetic reed switch means actuatable by said magnet,
Claim 24
Dependent Claim 9 words
induction heating power supply means for said RF coil,
Claim 25
Dependent Claim 9 words
induction heating power supply means for said RF coil,
Claim 26
Dependent Claim 10 words
flexible drive shaft means connected to said worm drive means,
Claim 27
Dependent Claim 10 words
flexible drive shaft means connected to said worm drive means,
Claim 28
Dependent Claim 25 words
An apparatus according to claim 1 wherein said pressuretight enclosure includes external cooling means in the form of coils adapted to circulate a fluid coolant.
Claim 29
Dependent Claim 22 words
An apparatus according to claim 1 wherein said pressuretight enclosure has associated therewith a self-resetting pressure-relief valve and a solenoid-actuated relief valve.
Claim 30
Dependent Claim 23 words
motor means connected through multispeed gear means, first clutch means, bevel gear means and second clutch means to said flexible drive shaft means,
Claim 31
Dependent Claim 23 words
motor means connected through multispeed gear means, first clutch means, bevel gear means and second clutch means to said flexible drive shaft means,
Claim 32
Dependent Claim 15 words
a saturable core reactor adapted to control current input into said power supply means, and
Claim 33
Dependent Claim 15 words
a saturable core reactor adapted to control current input into said power supply means, and
Claim 34
Dependent Claim 5 words
a reversible electromagnetic encounter, and
Claim 35
Dependent Claim 5 words
a reversible electromagnetic encounter, and
Claim 36
Dependent Claim 23 words
motor means connected through multispeed gear means, first clutch means, bevel gear means and second clutch means to said flexible drive shaft means,
Claim 37
Dependent Claim 23 words
motor means connected through multispeed gear means, first clutch means, bevel gear means and second clutch means to said flexible drive shaft means,
Claim 38
Dependent Claim 15 words
a saturable core reactor adapted to control current input into said power supply means, and
Claim 39
Dependent Claim 15 words
a saturable core reactor adapted to control current input into said power supply means, and
Claim 40
Dependent Claim 5 words
a reversible electromagnetic counter, and
Claim 41
Dependent Claim 5 words
a reversible electromagnetic counter, and
Claim 42
Dependent Claim 84 words
switch means connecting said reed switch means and said counter, said switch means being arranged to actuate said counter to register turns of said shaft extension in terms of the exact linear distance the end of said rod is from a fixed reference point; f. RF coil heating means positioned with respect to said rods to heat a load supported by one or both of said rods within said volume, and having temperature monitoring and controlling means associated with said RF coil which comprise
Claim 43
Dependent Claim 84 words
switch means connecting said reed switch means and said counter, said switch means being arranged to actuate said counter to register turns of said shaft extension in terms of the exact linear distance the end of said rod is from a fixed reference point; f. RF coil heating means positioned with respect to said rods to heat a load supported by one or both of said rods within said volume, and having temperature monitoring and controlling means associated with said RF coil which comprise
Claim 44
Dependent Claim 118 words
voltage signal processing means adapted to amplify said voltage signals for transmission to said saturable core whereby said core in controlling said current input controls the temperature developed by said RF coil; g. viewing port means providing for observation of said load and comprising at least one tempered Pyrex window protected within said enclosure by an infrared-reflecting window and having an external rotatably mounted cross-polarizer to control the intensity of the image transmitted through said windows; h. valved-controlled gas inlet means extending through the housing of said viewing port means and positioned to direct incoming gas against the window system in said viewing port means; and i. valved-controlled evacuating means adapted to produce a vacuum within said volume.
Claim 45
Dependent Claim 118 words
voltage signal processing means adapted to amplify said voltage signals for transmission to said saturable core whereby said core in controlling said current input controls the temperature developed by said RF coil; g. viewing port means providing for observation of said load and comprising at least one tempered Pyrex window protected within said enclosure by an infrared-reflecting window and having an external rotatably mounted cross-polarizer to control the intensity of the image transmitted through said windows; h. valved-controlled gas inlet means extending through the housing of said viewing port means and positioned to direct incoming gas against the window system in said viewing port means; and i. valved-controlled evacuating means adapted to produce a vacuum within said volume.
Claim 46
Dependent Claim 20 words
a high-speed motor connected through said bevel gear means and said second clutch means to said flexible drive shaft means,
Claim 47
Dependent Claim 20 words
a high-speed motor connected through said bevel gear means and said second clutch means to said flexible drive shaft means,
Claim 48
Dependent Claim 44 words
switch means connecting said reed switch means and said counter, said switch means being arranged to actuate said counter to register turns of said shaft extension in terms of the exact linear distance the end of said rod is from a fixed reference point.
Claim 49
Dependent Claim 44 words
switch means connecting said reed switch means and said counter, said switch means being arranged to actuate said counter to register turns of said shaft extension in terms of the exact linear distance the end of said rod is from a fixed reference point.
Claim 50
Dependent Claim 32 words
voltage signal processing means adapted to amplify said voltage signals for transmission to aid saturable core whereby said core in controlling said current input controls the temperature developed by said RF coil.
Claim 51
Dependent Claim 32 words
voltage signal processing means adapted to amplify said voltage signals for transmission to aid saturable core whereby said core in controlling said current input controls the temperature developed by said RF coil.
Claim 52
Dependent Claim 20 words
a high-speed motor connected through said bevel gear means and said second clutch means to said flexible drive shaft means,
Claim 53
Dependent Claim 20 words
a high-speed motor connected through said bevel gear means and said second clutch means to said flexible drive shaft means,
Claim 54
Dependent Claim 22 words
An apparatus according to claim 1 wherein said upper load-bearing rod incorporates fluid channels therein adapted to circulate a fluid coolant therethrough.
Claim 55
Dependent Claim 31 words
An apparatus according to claim 1 wherein said lower load-bearing rod serves as a housing for a thermocouple junction placed internally thereof at its upper end and for thermocouple lead wires.
Claim 56
Dependent Claim 40 words
first clutch-engaging means having energizing means connected to a current supply means common to said high-speed motor through switch means adapted to supply current to either said first clutch-engaging means or said high-speed motor but not to both simultaneously, and
Claim 57
Dependent Claim 40 words
first clutch-engaging means having energizing means connected to a current supply means common to said high-speed motor through switch means adapted to supply current to either said first clutch-engaging means or said high-speed motor but not to both simultaneously, and
Claim 58
Dependent Claim 42 words
first clutch engaging means having energizing means connected to a current supply means common to said high-speed motor through switch means adapted to supply current to either said first clutch engaging means or said high-speed motor but not to both simultaneously, and
Claim 59
Dependent Claim 42 words
first clutch engaging means having energizing means connected to a current supply means common to said high-speed motor through switch means adapted to supply current to either said first clutch engaging means or said high-speed motor but not to both simultaneously, and
Claim 60
Dependent Claim 30 words
second clutch engaging means; e. rod-locating means associated with said translational driving means adapted continuously to indicate the precise position of said rods within said volume and comprising, in combination
Claim 61
Dependent Claim 30 words
second clutch engaging means; e. rod-locating means associated with said translational driving means adapted continuously to indicate the precise position of said rods within said volume and comprising, in combination
Claim 62
Dependent Claim 17 words
second clutch-engaging means. 8. An apparatus according to claim 7, wherein said rod-locating means comprises, in combination
Claim 63
Dependent Claim 18 words
An apparatus according to claim 1 wherein said translational driving means associated with each rod comprises in combination
Claim 64
Dependent Claim 14 words
An apparatus according to claim 1 wherein said heating means is an RF coil.
Claim 65
Dependent Claim 26 words
An apparatus according to claim 1 wherein said heating means is an RF coil and has associated therewith Temperature monitoring and controlling means, comprising in combination
Claim 66
Dependent Claim 42 words
An apparatus according to claim 1 wherein said viewing port means comprises a tempered Pyrex window protected within said enclosure by an infrared-reflecting window and having an external, rotatably mounted cross-polarizer to control the intensity of the image transmitted through said windows.
Claim 67
Dependent Claim 44 words
An apparatus according to claim 1 including valved-controlled gas inlet means extending through the housing of said viewing port means and positioned to direct incoming gas against the window system in said viewing port means thereby to provide means to clean said window system.
Claim 68
Dependent Claim 30 words
An apparatus according to claim 1 including a television camera positioned adjacent one of the windows of said viewing port means and television-receiving means located remotely from said pressuretight enclosure.
Claim 69
Dependent Claim 95 words
A pressure- and temperature-controlled apparatus adapted for growing crystals and the like, comprising in combination a. a pressuretight enclosure defining a working volume therein and having a hinged access port equipped with pressure-relief valve means; b. external cooling means for said pressuretight enclosure adapted to circulate a fluid coolant; c. upper and lower load-bearing rods extending through pressuretight bushing means into said volume and movable therein in both rotational and translational modes; d. upper and lower rotational and translational rod driving means located external of said pressuretight enclosure, said translational driving means comprising, in combination
Claim 70
Dependent Claim 95 words
A pressure- and temperature-controlled apparatus adapted for growing crystals and the like, comprising in combination a. a pressuretight enclosure defining a working volume therein and having a hinged access port equipped with pressure-relief valve means; b. external cooling means for said pressuretight enclosure adapted to circulate a fluid coolant; c. upper and lower load-bearing rods extending through pressuretight bushing means into said volume and movable therein in both rotational and translational modes; d. upper and lower rotational and translational rod driving means located external of said pressuretight enclosure, said translational driving means comprising, in combination
Claim 71
Dependent Claim 22 words
An apparatus according to claim 14 wherein said upper load-bearing rod incorporates fluid channels therein adapted to circulate a fluid coolant therethrough.
Claim 72
Dependent Claim 31 words
An apparatus according to claim 14 wherein said lower load-bearing rod serves as a housing for a thermocouple junction placed internally thereof at its upper end and for thermocouple lead wires.
Claim 73
Dependent Claim 28 words
An apparatus according to claim 14 including a television camera positioned to view the working volume within said enclosure and a television receiving means remote from said camera.
Claim 74
Dependent Claim 21 words
An apparatus according to claim 14 including a self-resetting pressure-relief valve and a solenoid-actuated relief valve associated with said pressuretight enclosure.
Claim 75
Dependent Claim 60 words
An apparatus according to claim 14 wherein control means for said rod driving means, rod-locating means, said RF coil heating means, said valve-controlled gas inlet means and said valve-controlled evacuating means are located remote from said pressuretight enclosure whereby the entire operation performed within said work volume may be monitored and controlled at a location remote from said pressuretight enclosure.
Claim 76
Dependent Claim 35 words
An apparatus according to claim 14 wherein said viewing port means comprises a primary viewing port and an auxiliary viewing port, each of which comprises a tempered Pyrex window, an infrared-reflecting window and a crosspolarizer.

References Cited (Backward Citations)

US2972525A Cited
US2893847A Cited
US3211881A Cited
US3410945A Cited
US3493770A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-01-31 1975-08-02 1976-02-01 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-01-31 1979-08-02 1980-02-01 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-01-31 1983-08-02 1984-02-01 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag