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US3627631A Expired / Lapsed US ⏱️ 0.0 years remaining

A method of waterproofing paper using an n{40 -alkyl, n{hd 1{l {40 n{hd 1{l {40 -alkylene-n,n{hd 1{l -bis-urea

Assignee: Sun Chemical Corp
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Filing: 1969-12-08
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Granted: 1971-12-14
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Expires: 1989-12-08
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Abstract

Abstract which is in situ, or subsequently, with the aid of an emulsifying agent dispersed in water. In the formula each R'' is a group such as hydrogen, methyl or ethyl, which are independently selected and which contain from zero to not more than two carbon atoms. R is generally a divalent organic radical, namely an arylene, alkylarylene, arylalkylene, cycloalkylene, or alkylene radical, which may or may not contain ethylenic double bonds. R1 is alkyl, alkenyl, aralkyl, alkylaryl, cycloalkyl or cycloalkenyl and X is independently selected from the same groups or is aryl or hydrogen. The carbon atoms of R, R1 and X combined should total at least eight and preferably not more than 52 carbon atoms. Aqueous paper sizing compositions are prepared by combining an N''-alkyl,N-substituted urea containing an isocyanate group with an alpha, beta-alkylenimine to form an (N''-alkyl),(N1''N1'' -alkylene)-N,N1-bis-urea of the formula Formula I

Inventors

  • 👤 Gerhard Ewald Sprenger

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 09:08
CPC Classifications
D; D21; D21H; D21H17/00; D21H17/03; D21H17/05; D21H17/07

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 23 words
The process of claim 1 wherein the waterproofing compound is the product of the reaction of an alkylurea-substituted isocyanate and an alpha, beta-alkylenimine.
Claim 2
Dependent Claim 28 words
The process of claim 1 wherein the waterproofing dispersion also contains 0.01 to 0.1 percent, based on the weight of the dry paper stock, of a retention aid.

References Cited (Backward Citations)

US2302228A Cited
US3310460A Cited
US3280106A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-12-13 1975-06-14 1975-12-14 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-12-13 1979-06-14 1979-12-14 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-12-13 1983-06-14 1983-12-14 $7700.00 Window Closed / Lapsed

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