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US3624082A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for making 2-hydroxy-3-alkoxy quaternary ammonium propane salts

Assignee: JBS USA LLC
•
Filing: 1966-05-26
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Granted: 1971-11-30
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Expires: 1986-05-26
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Abstract

Abstract Quaternary ammonium salts are produced in substantial yields within a reasonable time by reacting, in the presence of water, a tertiary amine and 1-halo, 2-hydroxy, 3-alkoxy propane or by reacting the corresponding tertiary amine hydrohalide and glycidyl ether. The compositions possess surfactant properties and can be used as emulsifying agents, germicides, etc.

Inventors

  • 👤 Morton Lewis
  • 👤 Thomas W Findley

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 11:55
CPC Classifications
C; C07; C07D; C07D295/00; C07D295/04; C07D295/08; C07D295/084; C07D295/088; C11; C11D; C11D1/00; C11D1/38; C11D1/62

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 21 words
The method of claim 1 wherein the reaction takes place at temperatures of from about 75* C. to about 100* C.
Claim 2
Dependent Claim 15 words
The method of claim 1 wherein the 1-halo, 2-hydroxy, 3-alkoxy propane is a 1-chloro propane.
Claim 3
Dependent Claim 14 words
The method of claim 1 wherein the tertiary amine is a benzyl tertiary amine.
Claim 4
Dependent Claim 48 words
The method of claim 1 wherein the tertiary amine is selected from the group consisting of trialkyl amines having one to four carbon atoms in the alkyl chains, trialkyl amines wherein at least one alkyl group has five to 22 carbon atoms, ditertiary amines and cyclic tertiary amines.
Claim 5
Independent Claim 91 words
A method for the quaternization of tertiary amines with a 1-halo, 2-hydroxy, 3-alkoxy propane comprising: reacting in the liquid phase under reflux conditions, substantially stoichiometric amounts of a tertiary amine and a 1-halo, 2-hydroxy, 3-alkoxy propane wherein the alkyl of the alkoxy group is a carbon chain of from about eight to about 18 carbon atoms, in the presence of a solvent comprising 15-100 percent water and 0-85 percent isopropyl alcohol, said solvent being present in an amount of greater than about 15 percent based upon the weight of the reactants.
Claim 6
Dependent Claim 51 words
The method of claim 6 wherein the teRtiary amine is selected from the group consisting of trialkyl amines having one to four carbon atoms in the alkyl chains, alkyl dimethyl amines wherein the alkyl group has five to 22 carbon atoms, aliphatic ditertiary amines, cyclic ditertiary amines and cyclic tertiary amines.
Claim 7
Dependent Claim 34 words
The method of claim 6 wherein the halogen substituent of the 1-halo, 2-hydroxy, 3-alkoxy propane is chlorine, and wherein said alkoxy propane is the reaction product of a 10-14 carbon fatty alcohol and epichlorohydrin.

References Cited (Backward Citations)

US2548679A Cited
US2680769A Cited
US2775604A Cited
US2946797A Cited
US3326927A Cited
US3412160A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-11-29 1975-05-31 1975-11-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-11-29 1979-05-31 1979-11-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-11-29 1983-05-31 1983-11-30 $7700.00 Window Closed / Lapsed

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