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US3622650A
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Rubber reinforcing compositions
Assignee: Cabot Corp
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Filing: 1969-02-04
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Granted: 1971-11-23
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Expires: 1989-02-04
Abstract
Abstract Superior rubber reinforcing compositions comprising mixtures of carbon black and silica are provided by fluid energy milling of the combined ingredients. Among other attributes the resulting reinforcing composition display improved cut growth resistance characteristics in natural rubber formulations.
Inventors
- 👤 Gregor Berstein
- 👤 Bram B Boonstra
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 01:35
CPC Classifications
C; C08; C08K; C08K3/00; C08K3/02; C08K3/04; C08J; C08J3/00; C08J3/20; C08J3/22; C08K3/34; C08K3/36; C08J2321/00
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
17 words
The process of claim 1 wherein said carbon black provided in step (a) is in pelleted form.
Claim 2
Dependent Claim
14 words
The process of claim 1 wherein step (a) is achieved prior to step (b).
Claim 3
Dependent Claim
15 words
The process of claim 1 wherein step (a) is achieved substantially concomitantly with step (b).
Claim 4
Dependent Claim
21 words
The process of claim 1 wherein said carbon black has a dibutylphthalate absorption factor of greater than about 70 cc./100 grams.
Claim 5
Dependent Claim
23 words
The process of claim 1 wherein said precipitated silica has a BET-N2 surface area of between about 75 and about 150 m.2/ gram.
Claim 6
Dependent Claim
28 words
The process of claim 1 wherein said mixture consists essentially of about 70 weight percent of said carbon black and about 30 weight percent of said precipitated silica.
Claim 7
Dependent Claim
24 words
The process of claim 1 wherein said carbon black/silica mixture is fluid energy milled to an apparent density of less than about 7 lbs./ft.3.
Claim 8
Dependent Claim
18 words
The process of claim 1 wherein, subsequent to step (b), the resulting fluffy carbon black/silica product is pelletized.
Claim 9
Dependent Claim
100 words
A superior rubber reinforcing composition consisting essentially of a mixture of carbon black and precipitated silica, said carbon black having an original apparent density of greater than about 10 lbs./ft.3, a BET-N2 surface area of between about 30 and about 250 m.2/g. and a dibutylphthalate absorption factor of greater than about 50 cc./100 g. and said precipitated silica having an original apparent density of greater than about 10 lbs./ft.3, and a BET-N2 surface area of between about 50 and about 250 m.2/g., and which mixture has been fluid energy milled to an apparent density of less than about 9 lbs./ft.3.
Claim 10
Dependent Claim
37 words
The composition of claim 9 wherein said carbon black has a dibutylphthalate absorption factor greater than about 70 cc./100 g. and said precipitated silica has a BET-N2 surface area of between about 75 and about 150 m.2/g.
Claim 11
Dependent Claim
128 words
A reinforced rubber composition comprising natural rubber and between about 30 and about 85 percent by weight thereof of a carbon black/precipitated silica mixture produced by fluid energy milling a mixture consisting essentially of: a. between about 10 and about 50 weight percent of a precipitated silica having a BET-N2 surface area of between about 50 and about 250 m.2/g. and an apparent density oF above about 10 lbs./ft.3; and b. between about 90 and about 50 weight percent of a carbon black having a BET-N2 surface area of between about 30 and about 150 m.2g., a dibutylphthalate oil absorption factor of greater than about 50 cc./100 g. and an apparent density of greater than about 10 lbs./ft.3 to an apparent density of less than about 9 lbs./ft.3.
References Cited (Backward Citations)
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1974-11-22 | 1975-05-24 | 1975-11-23 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1978-11-22 | 1979-05-24 | 1979-11-23 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1982-11-22 | 1983-05-24 | 1983-11-23 | $7700.00 | Window Closed / Lapsed |