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US3619265A Expired / Lapsed US ⏱️ 0.0 years remaining

Rare earth oxide having inert layer thereon and method of making same

Assignee: GTE Sylvania Inc
•
Filing: 1969-02-28
•
Granted: 1971-11-09
•
Expires: 1989-02-28
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Abstract

Abstract A rare earth oxide host phosphor has incorporated thereon an outer layer of chemically combined fluoride ion. The coating increases the adherence properties of the phosphor in slurry application techniques for the manufacture of television screens by preventing poisoning of the phosphor particles by dichromate ions present in the slurry. The phosphor is coated by batching in a .05 molar fluoride bath, in acidic solution, about 400 to 500 grams of phosphor per liter of solution, agitating for about 20 to 30 minutes, and decanting the acidic solution, washing and then filtering and drying the phosphor. The drying temperature should be less than 200* C. to prevent disruption of the coating.

Inventors

  • 👤 Michael J Hammond
  • 👤 Raymond F Herner

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 12:21
CPC Classifications
C; C09; C09K; C09K11/00; C09K11/08; C09K11/77; C09K11/7701

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 17 words
The invention of claim 1 wherein said drying step is carried out at less than 200* C.
Claim 2
Dependent Claim 13 words
The invention of claim 2 wherein said drying temperature is approximately 125* C.
Claim 3
Dependent Claim 10 words
The invention of claim 1 wherein said solution is NH4F.HF.
Claim 4
Dependent Claim 23 words
The invention of claim 1 wherein said phosphor is selected from the group consisting essentially of yttrium oxide, gadolinium oxide, and yttrium-gadolinium oxide.

References Cited (Backward Citations)

US2049765A Cited
US3415757A Cited
US3322682A Cited
US3457184A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-11-08 1975-05-10 1975-11-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-11-08 1979-05-10 1979-11-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-11-08 1983-05-10 1983-11-09 $7700.00 Window Closed / Lapsed

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