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US3617253A Expired / Lapsed US ⏱️ 0.0 years remaining

Production of metal powders, particularly for use in electrodes and production of electrodes from these products

Assignee: SAFT Societe des Accumulateurs Fixes et de Traction SA
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Filing: 1968-12-13
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Granted: 1971-11-02
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Expires: 1988-12-13
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Abstract

Abstract Process for manufacturing a metal powder having a predetermined structure consisting in chemically reducing to metallic state a solution of a salt of the metal intended to constitute the electrode by the addition thereto of an appropriate reducing agent, while the ''''solution-reducing agent'''' mixture is submitted to a perturbed whirling agitation, so that the concentration of salt and reducing agent are made uniform and so that a great number of metal germs are produced, the agitation being maintained in order to promote an agglomeration in successive concentric layers of particles until the predetermined size of conglomerates is obtained, then separating the conglomerates from the mother-liquid when the required size is reached and finally washing and drying the powder so prepared. The powder so prepared is then formed into electrodes of desired dimensions by compression and, if necessary, followed by subsequent sintering at moderate sintering temperature.

Inventors

  • 👤 Bernard Paul Louis Amiet

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 19:17
CPC Classifications
H; H01; H01M; H01M4/00; H01M4/86; H01M4/90; H01M4/9016; B; B22; B22F; B22F9/00; B22F9/16; B22F9/18; B22F9/24; H01M4/02; H01M4/24; H01M4/34; H01M4/8605; H01M4/861; H01M4/88; H01M4/8875; Y; Y02; Y02E; Y02E60/00; Y02E60/10; Y02E60/30; Y02E60/50

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 24 words
A process according to claim 1, wherein said perturbed whirling agitation is effected by creating a plurality of vortices in the ''''solution-reducing agent'''' mixture.
Claim 2
Dependent Claim 27 words
A process according to claim 1, wherein said perturbed whirling agitation is effected by producing a single vortex in the ''''solution-reducing agent'''' mixture and perturbing said vortex.
Claim 3
Dependent Claim 32 words
A process according to claim 1, wherein the metal salt solution is silver nitrate and the reducing agent is sodium sulfite solution whose molar concentrations are alike and the conglomerate is silver.
Claim 4
Dependent Claim 15 words
A process according to claim 4, wherein the molar concentrations of both solutions are 1M.
Claim 5
Dependent Claim 32 words
A process according to claim 1, wherein said perturbed whirling operation is maintained until the particle size of the conglomerate in the resulting powder have dimensions comprised between 100 and 500 microns.
Claim 6
Dependent Claim 34 words
A process according to claim 6, wherein said dimensions are between 150 and 300 microns, the apparent density of the powder is approximately 0.6 and the specific surface area is approximately from 2,000-3,000 cm2/g.
Claim 7
Dependent Claim 22 words
A process according to claim 1, wherein the resulting dried powder is compressed into the form of an electrode of desired dimensions.
Claim 8
Dependent Claim 23 words
A process according to claim 8, wherein subsequent to compression of the powder sintering is effected at moderate temperature for a limited time.
Claim 9
Dependent Claim 20 words
A process according to claim 9, wherein the temperature is approximately 725* C. and the time is approximately 1 minute.

References Cited (Backward Citations)

US2753257A Cited
US2767082A Cited
US2767083A Cited
US2752237A Cited
US2836485A Cited
US2853374A Cited
US3234007A Cited
US3443933A Cited
US3369886A Cited
US3494760A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-11-01 1975-05-03 1975-11-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-11-01 1979-05-03 1979-11-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-11-01 1983-05-03 1983-11-02 $7700.00 Window Closed / Lapsed

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