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US3615211A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and apparatus for manufacture of carbon black

Assignee: Ashland LLC
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Filing: 1968-01-12
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Granted: 1971-10-26
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Expires: 1988-01-12
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Abstract

Abstract A method and apparatus for producing carbon black from hydrocarbons in which a hydrocarbon feed stock, such as a liquid hydrocarbon oil, is converted to carbon black in a tunnel-type carbon black furnace, having a combustion zone whose diameter is greater than its axial length, a reaction zone whose diameter is substantially smaller than that of the combustion zone and which is substantially longer in axial length than the combustion zone and a restricted diameter choke, whose diameter is substantially smaller than the diameter of the reaction zone, between the combustion zone and the reaction zone, by burning a combustible mixture, such as a mixture of air and natural gas, in the combustion zone; mixing the flue gases from the burning of the combustible mixture with the feed stock to heat the feed stock prior to its passage through the restricted diameter choke and into the reaction zone; and injecting a quenching fluid, such as low-pressure steam, into the reaction zone, in progressively larger volumes, from the influent end to the effluent end of the reaction zone, including the introduction of a quantity of the quench fluid in the area of the reaction zone adjacent the juncture between the restricted diameter choke and the walls of the reaction zone itself, for example, by introducing the quench fluid at a plurality of points spaced from the juncture of the choke and the walls of the reaction zone to a point in the reaction zone at which the reaction mixture is generally quenched in accordance with the prior art. It is also contemplated that the angle which the injected quench fluid forms with the walls of the reaction zone should progressively increase from the influent to the effluent end of the reaction zone to form an annular veil of quench fluid defining a general cone shape with its base adjacent the influent end and its apex toward the effluent end.

Inventors

  • 👤 James E Lewis

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 11:57
CPC Classifications
C; C09; C09C; C09C1/00; C09C1/44; C09C1/48; C09C1/50; B; B01; B01J; B01J19/00; B01J19/0006

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 18 words
A method in accordance with claim 1 wherein the hydrocarbon feed stock is a liquid hydrocarbon feed stock.
Claim 2
Dependent Claim 24 words
A method in accordance with claim 1 wherein the flue gas is produced by the combustion of a mixture of natural gas and air.
Claim 3
Independent Claim 151 words
A method for producing carbon black from a hydrocarbon feed stock, comprising, passing a mixture of said feed stock and a hot flue gas from the influent end to the effluent end of a generally tubular reaction zone at a velocity and under conditions such that said feed stock is converted to carbon black, and, simultaneously with the passage of said mixture through said reaction zone, injecting a quenching fluid into said mixture from the walls of said reaction zone within a single quadrant angle with respect of said walls of said reaction zone, which angle is progressively greater at each of a plurality of points successively spaced from the influent end toward the effluent end of said reaction zone and in amounts which progressively increase at each of said plurality of successive points from the influent end toward the effluent end of said reaction zone to rapidly cool said mixture.
Claim 4
Dependent Claim 36 words
A method in accordance with claim 4 wherein the quench fluid is introduced in a manner to form a continuous annular curtain of quench fluid along the entire length of the walls of the reaction zone.
Claim 5
Dependent Claim 58 words
A method in accordance with claim 4 wherein the reaction zone has a restricted-diameter choke, having a diameter smaller than the diameter of said reaction zone, located immediately adjacent its influent end and a part of the quench fluid is introduced into said reaction zone adjacent the juncture of said choke and the walls of said reaction zone.
Claim 6
Dependent Claim 18 words
A method in accordance with claim 4 wherein the hydrocarbon feed stock is a liquid hydrocarbon feed stock.
Claim 7
Dependent Claim 24 words
A method in accordance with claim 4 wherein the flue gas is produced by the combustion of a mixture of natural gas and air.
Claim 8
Dependent Claim 15 words
A method in accordance with claim 4 wherein the quench fluid is a low-pressure steam.
Claim 9
Dependent Claim 177 words
In a carbon black reactor system having a generally tubular combustion zone, a generally tubular reaction zone having a substantially smaller diameter than said combustion zone and a substantially gReater length than said combustion zone, and a restricted-diameter choke positioned between said combustion zone and said reaction zone, the improvement comprising, a plurality of quench fluid injection means mounted in said reaction zone at predetermined spaced points from the influent end of said reaction zone toward the effluent end of said reaction zone and means for progressively increasing the amounts of quench fluid introduced by each successive injection means from said influent end to said effluent end of said reaction zone, each successive one of said quench fluid injection means being adapted to spray quench fluid into said reaction zone from the walls of said reaction zone within a single quadrant angle with respect to said walls of said reaction zone, which angle is progressively greater at each of said successive quench fluid injection means from the influent end toward the effluent end of said reaction zone.
Claim 10
Dependent Claim 30 words
A system in accordance with claim 10 wherein at least one of the injection means is located adjacent the juncture between the choke and the walls of the reaction zone.

References Cited (Backward Citations)

US2971822A Cited
US3307911A Cited
US3401020A Cited
US3408165A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-10-25 1975-04-26 1975-10-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-10-25 1979-04-26 1979-10-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-10-25 1983-04-26 1983-10-26 $7700.00 Window Closed / Lapsed

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