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US3607436A Expired / Lapsed US ⏱️ 0.0 years remaining

Sintered beta-alumina bodies and method

Assignee: General Electric Co
•
Filing: 1969-12-17
•
Granted: 1971-09-21
•
Expires: 1989-12-17
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Abstract

Abstract The electrical conductivity of a sintered sodium beta-alumina solid electrolyte can be increased substantially by incorporating small proportions of magnesia and yttria in the powder mixture used to produce the sintered body.

Inventors

  • 👤 Richard J Charles
  • 👤 William J Dondalski
  • 👤 Stephan P Mitoff

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 06:48
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/10; C04B35/111; C04B35/113; C01; C01F; C01F7/00; C01F7/02; C01F7/028; H; H01; H01B; H01B1/00; H01B1/06; H01B1/08; H01M; H01M6/00; H01M6/14; H01M6/18; H01M6/185; C01P; C01P2004/00; C01P2004/60; C01P2004/61; C01P2006/00; C01P2006/40

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 16 words
The ceramic body of claim 1 in which the amount of magnesia is about 2 percent.
Claim 2
Dependent Claim 30 words
The ceramic body of claim 1 in which the amount of magnesia is about 2 percent and the amount of yttria is from about 1 percent to about 3 percent.
Claim 3
Dependent Claim 18 words
The ceramic body of claim 1 in which the body is of substantially uniform thickness approximating 10 mils.
Claim 4
Dependent Claim 15 words
The ceramic body of claim 1 in which the body is approximately 1 millimeter thick.
Claim 5
Dependent Claim 31 words
The ceramic body of claim 1 in which thE amount of magnesia is about 2 percent and the density of the body is greater than about 90 percent of theoretical density.
Claim 6
Independent Claim 120 words
The method of making a ceramic body having density greater than 85 percent of theoretical density and electrical resistivity at 300* C., less than 100 ohm-centimeters and consequently having special utility as a solid electrolyte in a sodium-sulfur battery which includes the steps of preparing a substantially uniform powder mixture of sodium-beta alumina or potassium beta-alumina and a source of from 0.5 percent to 5.0 percent of magnesia and a source of from 0.25 percent to 5.0 percent yttria, subjecting the said powder mixture to compacting pressure and thereby forming a green body, and firing the green body under an atmospheric containing free oxygen at a temperature between 1,600* C. and 1, 900* C. and thereby sintering the green body.
Claim 7
Dependent Claim 63 words
The method of claim 7 in which the powder mixture is mixed with a binder of 10 percent polyvinyl alcohol in water and in which the resulting mixture is extruded to produce the desired green body, and in which the resulting green body is air dried at room temperature and thereafter fired at 1,825* C. for 2 hours in a dry oxygen atmosphere.

References Cited (Backward Citations)

US3298842A Cited
US3311482A Cited
US3458356A Cited
US3432314A Cited
US3499796A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-09-20 1975-03-22 1975-09-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-09-20 1979-03-22 1979-09-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-09-20 1983-03-22 1983-09-21 $7700.00 Window Closed / Lapsed

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