US3565408A
Expired / Lapsed
US
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Production of alumina from aluminum hydroxide
Assignee: GEA Group AG
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Filing: 1968-06-03
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Granted: 1971-02-23
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Expires: 1988-06-03
Abstract
Abstract Aluminum hydroxide is first dehydrated in a suspension-type heat exchanger system by hot gas coming from a fluidized bed furnace with material recycling and then introduced into the fluidized bed. Hot alumina taken from the fluidized bed is used in a heat exchanger to preheat fresh air which is used as the fluidizing gas for the fluidized bed. Another portion of air is also heated in the heat exchanger and is introduced into the fluidized bed as secondary air.
Inventors
- 👤 Lothar Reh
- 👤 Karlheinz Rosenthal
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 02:50
CPC Classifications
C; C01; C01F; C01F7/00; C01F7/02; C01F7/44; C01F7/441; C01F7/445
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
376 words
A process for producing anhydrous alumina from moist aluminum hydroxide, comprising the steps of: a. heating dewatered and partially dehydrated aluminum hydroxide particles to a temperature of 600* to 1,200* C. and converting same to anhydrous alumina in a fluidized bed by introducing a fluidizing gas at a temperature of at least 300* C. into said fluidized bed above the bottom thereof and a combustionsustaining fluidizing gas into said bed through the bottom thereof; b. removing from above said fluidized bed a mixture of solids and hot exhaust gas and separating the hot exhaust gas from said solids; c. recirculating at least part of the solids separated in step (b) to the bed of step (a); d. dewatering and partially dehydrating moist aluminum hydroxide at least in part by subjecting the same to direct contact with at least part of the hot exhaust gas separated in step (b) while suspending the moist aluminum hydroxide in said hot exhaust gas, and recovering dewatered and partially dehydrated aluminum hydroxide therefrom; e. feeding the dewatered and partially dehydrated aluminum hydroxide from step (d) to the fluidized bed in step (a); f. recovering anhydrous alumina from said fluidized bed at a temperature of 600 to 1,200* C.; g. cooling the anhydrous alumina recovered in step (f) by fluidizing same with a first portion of cooling air and abstracting heat from the anhydrous alumina with a second portion of cooling air in indirect heat exchange with the hot anhydrous alumina, thereby heating said first and said second portions of said cooling air; h. feeding said first portion of the air heated in step (g) to said fluidized bed in step (a) at a location above said bottom as secondary air, and feeding said second portion of said air heated in step (g) to said bed through said bottom as a fluidizing gas, said location having a height above said bottom between 0.3 and 1.5 times the pressure drop across the fluidized bed in terms of millimeters of a water-column measure of said pressure drop, the volumetric ratio of said second portion to said first portion ranging between 1:2 to 4:1; and i. introducing a combustible fuel into said fluidized bed between said grate and said location to further heat said bed.
Claim 2
Dependent Claim
376 words
A process for producing anhydrous alumina from moist aluminum hydroxide, comprising the steps of: a. heating dewatered and partially dehydrated aluminum hydroxide particles to a temperature of 600* to 1,200* C. and converting same to anhydrous alumina in a fluidized bed by introducing a fluidizing gas at a temperature of at least 300* C. into said fluidized bed above the bottom thereof and a combustionsustaining fluidizing gas into said bed through the bottom thereof; b. removing from above said fluidized bed a mixture of solids and hot exhaust gas and separating the hot exhaust gas from said solids; c. recirculating at least part of the solids separated in step (b) to the bed of step (a); d. dewatering and partially dehydrating moist aluminum hydroxide at least in part by subjecting the same to direct contact with at least part of the hot exhaust gas separated in step (b) while suspending the moist aluminum hydroxide in said hot exhaust gas, and recovering dewatered and partially dehydrated aluminum hydroxide therefrom; e. feeding the dewatered and partially dehydrated aluminum hydroxide from step (d) to the fluidized bed in step (a); f. recovering anhydrous alumina from said fluidized bed at a temperature of 600 to 1,200* C.; g. cooling the anhydrous alumina recovered in step (f) by fluidizing same with a first portion of cooling air and abstracting heat from the anhydrous alumina with a second portion of cooling air in indirect heat exchange with the hot anhydrous alumina, thereby heating said first and said second portions of said cooling air; h. feeding said first portion of the air heated in step (g) to said fluidized bed in step (a) at a location above said bottom as secondary air, and feeding said second portion of said air heated in step (g) to said bed through said bottom as a fluidizing gas, said location having a height above said bottom between 0.3 and 1.5 times the pressure drop across the fluidized bed in terms of millimeters of a water-column measure of said pressure drop, the volumetric ratio of said second portion to said first portion ranging between 1:2 to 4:1; and i. introducing a combustible fuel into said fluidized bed between said grate and said location to further heat said bed.
Claim 3
Dependent Claim
39 words
The process defined in claim 1 wherein the secondary air of step (h) is introduced into said bed at a location spaced above the bottom of said bed by a distance between 0.5 and 0.8 times said pressure drop.
Claim 4
Dependent Claim
31 words
The process defined in claim 1 wherein the moist aluminum hydroxide is dewatered and partially dehydrated in step (d) by passing the moist aluminum hydroxide through a two-stage venturi-type fluid-bed pReheater.
Claim 5
Dependent Claim
64 words
The process defined in claim 1 wherein the anhydrous alumina is cooled in step (g) by passing the same in succession through a plurality of cooling compartments while fluidizing the anhydrous alumina in said compartments with said first portion of cooling air, said second portion of cooling air being passed through said compartments countercurrent to said anhydrous alumina and in indirect heat exchange therewith.
Claim 6
Dependent Claim
33 words
The process defined in claim 1, further comprising the step of passing part of the cooling air heated in step (g) into heat exchanging relationship with the moist aluminum hydroxide in step (d).
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1974-02-22 | 1974-08-24 | 1975-02-23 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1978-02-22 | 1978-08-24 | 1979-02-23 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1982-02-22 | 1982-08-24 | 1983-02-23 | $7700.00 | Window Closed / Lapsed |